Rapid homogeneous preparation of cellulose graft copolymer in BMIMCL under microwave irradiation
Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′-methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1-butyl-3-methylinidazolium chloride ionic...
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| Published in | Journal of applied polymer science Vol. 118; no. 1; pp. 399 - 404 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Hoboken
Wiley Subscription Services, Inc., A Wiley Company
05.10.2010
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| Abstract | Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′-methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1-butyl-3-methylinidazolium chloride ionic liquid was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of AA onto cellulose. The use of MW resulted in a drastic reduction of reaction time: 3 min irradiation was sufficient, compared with 30 min to 5 h, as conventional heating was used. Investigation was conducted on the effect of reaction parameters, such as monomer concentration, crosslinker dosage, exposure temperature and exposure time. The structure of the graft copolymer was confirmed by IR spectrum, thermogravimetric analyzer, and scanning electron microscope. The results show that the MW irradiation method can increase the reaction rate. And the graft copolymer is also an effective metal ion adsorbent. |
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| AbstractList | Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′-methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1-butyl-3-methylinidazolium chloride ionic liquid was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of AA onto cellulose. The use of MW resulted in a drastic reduction of reaction time: 3 min irradiation was sufficient, compared with 30 min to 5 h, as conventional heating was used. Investigation was conducted on the effect of reaction parameters, such as monomer concentration, crosslinker dosage, exposure temperature and exposure time. The structure of the graft copolymer was confirmed by IR spectrum, thermogravimetric analyzer, and scanning electron microscope. The results show that the MW irradiation method can increase the reaction rate. And the graft copolymer is also an effective metal ion adsorbent. Abstract Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′ ‐methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1‐butyl‐3‐methylinidazolium chloride ionic liquid was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of AA onto cellulose. The use of MW resulted in a drastic reduction of reaction time: 3 min irradiation was sufficient, compared with 30 min to 5 h, as conventional heating was used. Investigation was conducted on the effect of reaction parameters, such as monomer concentration, crosslinker dosage, exposure temperature and exposure time. The structure of the graft copolymer was confirmed by IR spectrum, thermogravimetric analyzer, and scanning electron microscope. The results show that the MW irradiation method can increase the reaction rate. And the graft copolymer is also an effective metal ion adsorbent. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′‐methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1‐butyl‐3‐methylinidazolium chloride ionic liquid was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of AA onto cellulose. The use of MW resulted in a drastic reduction of reaction time: 3 min irradiation was sufficient, compared with 30 min to 5 h, as conventional heating was used. Investigation was conducted on the effect of reaction parameters, such as monomer concentration, crosslinker dosage, exposure temperature and exposure time. The structure of the graft copolymer was confirmed by IR spectrum, thermogravimetric analyzer, and scanning electron microscope. The results show that the MW irradiation method can increase the reaction rate. And the graft copolymer is also an effective metal ion adsorbent. © 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N'-methylenebisacrylamide as a crosslinker under microwave (MW) irradiation. The powerful and highly efficient direct solvent, 1-butyl-3-methylinidazolium chloride ionic liquid was used as the solvent for the dissolution of cellulose and the media for the homogeneous graft polymerization of AA onto cellulose. The use of MW resulted in a drastic reduction of reaction time: 3 min irradiation was sufficient, compared with 30 min to 5 h, as conventional heating was used. Investigation was conducted on the effect of reaction parameters, such as monomer concentration, crosslinker dosage, exposure temperature and exposure time. The structure of the graft copolymer was confirmed by IR spectrum, thermogravimetric analyzer, and scanning electron microscope. The results show that the MW irradiation method can increase the reaction rate. And the graft copolymer is also an effective metal ion adsorbent. [copy 2010 Wiley Periodicals, Inc. J Appl Polym Sci, 2010 |
| Author | Lin, Chun-Xiang Huang, Liang-Hui Fu, Shi-Yu Zhan, Huai-Yu Liu, Ming-Hua |
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| Cites_doi | 10.1111/j.1532-849X.2007.00277.x 10.1016/j.polymer.2005.10.101 10.1016/S0144-8617(02)00004-8 10.1016/S0040-4039(99)00620-6 10.1002/app.1990.070391101 10.1002/mabi.200500039 10.1016/S0040-4020(99)00601-8 10.1016/j.tet.2004.05.100 10.1016/S0014-3057(01)00070-2 10.1016/S0306-2619(03)00016-3 10.1021/ja025790m 10.1021/la9008703 10.1016/j.carbpol.2003.09.008 10.1016/S0141-3910(03)00177-0 10.1002/1521-3927(20001001)21:15<1032::AID-MARC1032>3.0.CO;2-N 10.1016/S0008-6215(97)00185-7 10.1007/s100980050018 10.1016/j.carbpol.2004.04.010 10.1016/S0926-860X(01)00834-1 10.1002/pi.728 10.1002/anie.200460587 10.1021/cr980032t |
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| Keywords | Copper II Imidazole derivatives Molecular structure Adsorption capacity Plant fiber Metal ion Cotton graft compolymerization Grafting Optimization Ionic liquid Crosslinked copolymer Natural fiber Acrylamide copolymer Microwave irradiation acrylic acid microwave Acrylic acid copolymer Iminium compounds Experimental study Organic adsorbent Cellulose graft copolymer Homogeneous reaction cellulose Preparation Cellulose derivatives Kinetics ionic liquids |
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| Snippet | Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′-methylenebisacrylamide as... Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′‐methylenebisacrylamide as... Abstract Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N′... Acrylic acid(AA) was grafted onto cellulose in homogeneous media by using ammonium persulfate as an initiator in the presence of N,N'-methylenebisacrylamide as... |
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| SubjectTerms | acrylic acid Applied sciences Cellulose Cellulose and derivatives Crosslinking Exact sciences and technology graft compolymerization Graft copolymers ionic liquids Irradiation Media microwave Microwaves Natural polymers Physicochemistry of polymers Scanning electron microscopy Solvents |
| Title | Rapid homogeneous preparation of cellulose graft copolymer in BMIMCL under microwave irradiation |
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