Microwave synthesis of phosphorus-doped graphitic carbon nitride nanosheets with enhanced electrochemiluminescence signals
Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irra...
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| Published in | Journal of materials science Vol. 55; no. 28; pp. 13618 - 13633 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.10.2020
Springer Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0022-2461 1573-4803 |
| DOI | 10.1007/s10853-020-04862-6 |
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| Abstract | Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irradiation. When the melamine precursor is modified with a 5 wt% diammonium hydrogen phosphate, the as-synthesized PCNNs display a very thin thickness (about 2 nm), good dispersibility in water (still stable after 2 weeks), low electron-transfer resistance (7499 Ω) and suitable band gap (2.7 eV). More importantly, the ECL intensity of the optimal PCNNs at low potential (− 1.2 to 0 V) is 26.7 times stronger than that of pure graphitic carbon nitride. The key to the excellent ECL property primarily lies in the more satisfactory sheet-like structure, faster electron transfer and better water affinity. |
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| AbstractList | Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irradiation. When the melamine precursor is modified with a 5 wt% diammonium hydrogen phosphate, the as-synthesized PCNNs display a very thin thickness (about 2 nm), good dispersibility in water (still stable after 2 weeks), low electron-transfer resistance (7499 Ω) and suitable band gap (2.7 eV). More importantly, the ECL intensity of the optimal PCNNs at low potential (- 1.2 to 0 V) is 26.7 times stronger than that of pure graphitic carbon nitride. The key to the excellent ECL property primarily lies in the more satisfactory sheet-like structure, faster electron transfer and better water affinity. Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irradiation. When the melamine precursor is modified with a 5 wt% diammonium hydrogen phosphate, the as-synthesized PCNNs display a very thin thickness (about 2 nm), good dispersibility in water (still stable after 2 weeks), low electron-transfer resistance (7499 Ω) and suitable band gap (2.7 eV). More importantly, the ECL intensity of the optimal PCNNs at low potential (− 1.2 to 0 V) is 26.7 times stronger than that of pure graphitic carbon nitride. The key to the excellent ECL property primarily lies in the more satisfactory sheet-like structure, faster electron transfer and better water affinity. Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we report an efficient bottom-up pathway to synthesize phosphorus-doped graphitic carbon nitride nanosheets (PCNNs) by ultra-rapid microwave irradiation. When the melamine precursor is modified with a 5 wt% diammonium hydrogen phosphate, the as-synthesized PCNNs display a very thin thickness (about 2 nm), good dispersibility in water (still stable after 2 weeks), low electron-transfer resistance (7499 Ω) and suitable band gap (2.7 eV). More importantly, the ECL intensity of the optimal PCNNs at low potential (− 1.2 to 0 V) is 26.7 times stronger than that of pure graphitic carbon nitride. The key to the excellent ECL property primarily lies in the more satisfactory sheet-like structure, faster electron transfer and better water affinity. |
| Audience | Academic |
| Author | Yu, Yongzhi Jiang, Nan Zou, Jingye Wu, Shan Yan, Wenjun Qiao, Kun Cheng, Si Wang, Jigang |
| Author_xml | – sequence: 1 givenname: Jingye surname: Zou fullname: Zou, Jingye organization: Jiangsu Key Laboratory of Advanced Metallic Materials, School of Materials Science and Engineering, Southeast University – sequence: 2 givenname: Yongzhi surname: Yu fullname: Yu, Yongzhi organization: National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen Ceramic Institute – sequence: 3 givenname: Kun surname: Qiao fullname: Qiao, Kun organization: Jiangsu Key Laboratory of Advanced Metallic Materials, School of Materials Science and Engineering, Southeast University – sequence: 4 givenname: Shan surname: Wu fullname: Wu, Shan organization: Jiangsu Key Laboratory of Advanced Metallic Materials, School of Materials Science and Engineering, Southeast University – sequence: 5 givenname: Wenjun surname: Yan fullname: Yan, Wenjun organization: Analytical Instrumentation Center, Institute of Coal Chemistry, Chinese Academy of Sciences – sequence: 6 givenname: Si surname: Cheng fullname: Cheng, Si organization: National Engineering Research Center for Domestic and Building Ceramics, Jingdezhen Ceramic Institute – sequence: 7 givenname: Nan surname: Jiang fullname: Jiang, Nan email: jiangnan@njmu.edu.cn organization: School of Pharmacy, Nanjing Medical University – sequence: 8 givenname: Jigang orcidid: 0000-0001-9220-8076 surname: Wang fullname: Wang, Jigang email: wangjigang@seu.edu.cn organization: Jiangsu Key Laboratory of Advanced Metallic Materials, School of Materials Science and Engineering, Southeast University, Xizang Engineering Laboratory for Water Pollution Control and Ecological Remediation, School of Information Engineering, Xizang Minzu University |
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| Snippet | Efficient and low-cost electrode materials for the electrochemiluminescence (ECL) reaction are highly desired for the future detection technology. Herein, we... |
| SourceID | proquest gale crossref springer |
| SourceType | Aggregation Database Enrichment Source Index Database Publisher |
| StartPage | 13618 |
| SubjectTerms | Boron nitride Carbon Carbon nitride Characterization and Evaluation of Materials Chemical Routes to Materials Chemistry and Materials Science Classical Mechanics Crystallography and Scattering Methods Electrochemiluminescence Electrode materials Electron transfer Electron transport Materials Science Melamine Nanosheets Phosphorus Polymer Sciences Solid Mechanics Synthesis |
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| Title | Microwave synthesis of phosphorus-doped graphitic carbon nitride nanosheets with enhanced electrochemiluminescence signals |
| URI | https://link.springer.com/article/10.1007/s10853-020-04862-6 https://www.proquest.com/docview/2423651920 |
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