Innovative Methylcellulose-Polyvinyl Pyrrolidone-Based Solid Polymer Electrolytes Impregnated with Potassium Salt: Ion Conduction and Thermal Properties
In this research, innovative green and sustainable solid polymer electrolytes (SPEs) based on plasticized methylcellulose/polyvinyl pyrrolidone/potassium carbonate (MC/PVP/K2CO3) were examined. The MC/PVP/K2CO3 SPE system with five distinct ethylene carbonate (EC) concentrations as a plasticizer was...
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Published in | Polymers Vol. 14; no. 15; p. 3055 |
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Main Authors | , , , , , , , , , |
Format | Journal Article |
Language | English |
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28.07.2022
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Abstract | In this research, innovative green and sustainable solid polymer electrolytes (SPEs) based on plasticized methylcellulose/polyvinyl pyrrolidone/potassium carbonate (MC/PVP/K2CO3) were examined. The MC/PVP/K2CO3 SPE system with five distinct ethylene carbonate (EC) concentrations as a plasticizer was successfully designed. Frequency-dependent conductivity plots were used to investigate the conduction mechanism of the SPEs. Electrochemical potential window stability and the cation transfer number of the SPEs were studied via linear sweep voltammetry (LSV) and transference number measurement (TNM), respectively. Additionally, the structural behavior of the SPEs was analyzed using Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FESEM), X-ray diffractometry (XRD), and differential scanning calorimetry (DSC) techniques. The SPE film complexed with 15 wt.% EC measured a maximum conductivity of 3.88 × 10−4 Scm−1. According to the results of the transference number examination, cations that record a transference number of 0.949 are the primary charge carriers. An EDLC was fabricated based on the highest conducting sample that recorded a specific capacitance of 54.936 Fg−1 at 5 mVs−1. |
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AbstractList | In this research, innovative green and sustainable solid polymer electrolytes (SPEs) based on plasticized methylcellulose/polyvinyl pyrrolidone/potassium carbonate (MC/PVP/K2CO3) were examined. The MC/PVP/K2CO3 SPE system with five distinct ethylene carbonate (EC) concentrations as a plasticizer was successfully designed. Frequency-dependent conductivity plots were used to investigate the conduction mechanism of the SPEs. Electrochemical potential window stability and the cation transfer number of the SPEs were studied via linear sweep voltammetry (LSV) and transference number measurement (TNM), respectively. Additionally, the structural behavior of the SPEs was analyzed using Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FESEM), X-ray diffractometry (XRD), and differential scanning calorimetry (DSC) techniques. The SPE film complexed with 15 wt.% EC measured a maximum conductivity of 3.88 × 10−4 Scm−1. According to the results of the transference number examination, cations that record a transference number of 0.949 are the primary charge carriers. An EDLC was fabricated based on the highest conducting sample that recorded a specific capacitance of 54.936 Fg−1 at 5 mVs−1. In this research, innovative green and sustainable solid polymer electrolytes (SPEs) based on plasticized methylcellulose/polyvinyl pyrrolidone/potassium carbonate (MC/PVP/K 2 CO 3 ) were examined. The MC/PVP/K 2 CO 3 SPE system with five distinct ethylene carbonate (EC) concentrations as a plasticizer was successfully designed. Frequency-dependent conductivity plots were used to investigate the conduction mechanism of the SPEs. Electrochemical potential window stability and the cation transfer number of the SPEs were studied via linear sweep voltammetry (LSV) and transference number measurement (TNM), respectively. Additionally, the structural behavior of the SPEs was analyzed using Fourier transform infrared spectroscopy (FTIR), field emission scanning electron microscopy (FESEM), X-ray diffractometry (XRD), and differential scanning calorimetry (DSC) techniques. The SPE film complexed with 15 wt.% EC measured a maximum conductivity of 3.88 × 10 −4 Scm −1 . According to the results of the transference number examination, cations that record a transference number of 0.949 are the primary charge carriers. An EDLC was fabricated based on the highest conducting sample that recorded a specific capacitance of 54.936 Fg −1 at 5 mVs −1 . |
Author | Bashir Abdulkadir, Abubakar Abdel All, Naglaa F. M. Dennis, John Ojur Aldaghri, Osamah A. Ali, Mohammed Khalil Mohammed Soleimani, Hassan Shukur, Muhammad Fadhlullah Bin Abd Ibrahem, Moez A. Adam, Abdullahi Abbas Ibnaouf, Khalid Hassan |
AuthorAffiliation | 4 Department of Physics, College of Science, Imam Mohammad Ibn Saud Islamic University (IMSIU), Riyadh 13318, Saudi Arabia; khiahmed@imamu.edu.sa (K.H.I.); odaghri@imamu.edu.sa (O.A.A.); 9@imamm.org (M.A.I.); nfabdelall@imamu.edu.sa (N.F.M.A.A.) 2 Centre of Innovative Nanoscience and Nanotechnology (COINN), Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia 1 Department of Fundamental and Applied Sciences, Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia; jdennis100@gmail.com (J.O.D.); hassan.soleimani@utp.edu.my (H.S.); mfadhlullah.ashukur@utp.edu.my (M.F.B.A.S.); abubakarbashir150@gmail.com (A.B.A.) 3 Department of Physics, Al-Qalam University Katsina, Katsina 820252, Nigeria |
AuthorAffiliation_xml | – name: 2 Centre of Innovative Nanoscience and Nanotechnology (COINN), Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia – name: 4 Department of Physics, College of Science, Imam Mohammad Ibn Saud Islamic University (IMSIU), Riyadh 13318, Saudi Arabia; khiahmed@imamu.edu.sa (K.H.I.); odaghri@imamu.edu.sa (O.A.A.); 9@imamm.org (M.A.I.); nfabdelall@imamu.edu.sa (N.F.M.A.A.) – name: 1 Department of Fundamental and Applied Sciences, Universiti Teknologi PETRONAS, Seri Iskandar 32610, Malaysia; jdennis100@gmail.com (J.O.D.); hassan.soleimani@utp.edu.my (H.S.); mfadhlullah.ashukur@utp.edu.my (M.F.B.A.S.); abubakarbashir150@gmail.com (A.B.A.) – name: 3 Department of Physics, Al-Qalam University Katsina, Katsina 820252, Nigeria |
Author_xml | – sequence: 1 givenname: Abdullahi Abbas orcidid: 0000-0001-7290-4787 surname: Adam fullname: Adam, Abdullahi Abbas – sequence: 2 givenname: Mohammed Khalil Mohammed surname: Ali fullname: Ali, Mohammed Khalil Mohammed – sequence: 3 givenname: John Ojur orcidid: 0000-0002-4489-649X surname: Dennis fullname: Dennis, John Ojur – sequence: 4 givenname: Hassan surname: Soleimani fullname: Soleimani, Hassan – sequence: 5 givenname: Muhammad Fadhlullah Bin Abd surname: Shukur fullname: Shukur, Muhammad Fadhlullah Bin Abd – sequence: 6 givenname: Khalid Hassan orcidid: 0000-0003-1146-9456 surname: Ibnaouf fullname: Ibnaouf, Khalid Hassan – sequence: 7 givenname: Osamah A. orcidid: 0000-0001-7990-6099 surname: Aldaghri fullname: Aldaghri, Osamah A. – sequence: 8 givenname: Moez A. surname: Ibrahem fullname: Ibrahem, Moez A. – sequence: 9 givenname: Naglaa F. M. surname: Abdel All fullname: Abdel All, Naglaa F. M. – sequence: 10 givenname: Abubakar surname: Bashir Abdulkadir fullname: Bashir Abdulkadir, Abubakar |
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CitedBy_id | crossref_primary_10_1007_s13399_022_03202_9 crossref_primary_10_1080_15421406_2022_2160901 crossref_primary_10_1016_j_measurement_2024_114210 crossref_primary_10_1007_s00289_023_04846_x crossref_primary_10_1002_app_54445 crossref_primary_10_1016_j_jelechem_2023_117334 crossref_primary_10_3390_molecules28083461 |
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SubjectTerms | Cations Cellulose Conduction Current carriers Electrochemical potential Electrolytes Emission analysis Field emission microscopy Field emission spectroscopy Fluorides Fourier transforms Infrared analysis Molten salt electrolytes Polymer blends Polymers Polyvinyl alcohol Potassium Potassium carbonate Potassium salts Solid electrolytes Thermodynamic properties Viscosity |
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Title | Innovative Methylcellulose-Polyvinyl Pyrrolidone-Based Solid Polymer Electrolytes Impregnated with Potassium Salt: Ion Conduction and Thermal Properties |
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