Phase Composition of Sputtered Film from a Mixture Target of Hydroxyapatite and Strontium-apatite
To obtain an Sr-substituted hydroxyapatite thin film, sputter-coating was performed on a cellulose filter acting as a substrate from the mixture target of hydroxyapatite （HA） and strontium-apatite （SrAp） at an Ar pressure of 0.5-5.0 Pa. The ratio of the SrAp in the mixture target was varied from 25%...
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| Published in | Journal of materials science & technology Vol. 29; no. 1; pp. 1 - 6 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
2013
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| Subjects | |
| Online Access | Get full text |
| ISSN | 1005-0302 1941-1162 |
| DOI | 10.1016/j.jmst.2012.11.014 |
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| Abstract | To obtain an Sr-substituted hydroxyapatite thin film, sputter-coating was performed on a cellulose filter acting as a substrate from the mixture target of hydroxyapatite （HA） and strontium-apatite （SrAp） at an Ar pressure of 0.5-5.0 Pa. The ratio of the SrAp in the mixture target was varied from 25% to 100%. After coating, the films were heated at 700 ℃ to remove the cellulose filter substrate, and the crystalline phases were identified by X-ray diffraction （XRD）. The sputter-coated film was identified as the Sr-substituted /3-tri-calcium phosphate （TCP） and the Sr-substituted/3-calcium pyrophosphate （CPP） as well as the Sr-substituted HA. The weight ratio of the Sr-substituted HA decreased with increasing Ar pressure or with an increasing ratio of SrAp to HA in the target. The average Sr/（Ca ＋ Sr） molar ratio in the film was 1.9%-3.5% slightly lower than the initial SrAp ratio of the target, and the ratio was not influenced by the Ar pressure. In the （Sr ＋ Ca）/P ratio, the ratio decreased while increasing the SrAp ratio in the target. |
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| AbstractList | To obtain an Sr-substituted hydroxyapatite thin film, sputter-coating was performed on a cellulose filter acting as a substrate from the mixture target of hydroxyapatite （HA） and strontium-apatite （SrAp） at an Ar pressure of 0.5-5.0 Pa. The ratio of the SrAp in the mixture target was varied from 25% to 100%. After coating, the films were heated at 700 ℃ to remove the cellulose filter substrate, and the crystalline phases were identified by X-ray diffraction （XRD）. The sputter-coated film was identified as the Sr-substituted /3-tri-calcium phosphate （TCP） and the Sr-substituted/3-calcium pyrophosphate （CPP） as well as the Sr-substituted HA. The weight ratio of the Sr-substituted HA decreased with increasing Ar pressure or with an increasing ratio of SrAp to HA in the target. The average Sr/（Ca ＋ Sr） molar ratio in the film was 1.9%-3.5% slightly lower than the initial SrAp ratio of the target, and the ratio was not influenced by the Ar pressure. In the （Sr ＋ Ca）/P ratio, the ratio decreased while increasing the SrAp ratio in the target. To obtain an Sr-substituted hydroxyapatite thin film, sputter-coating was performed on a cellulose filter acting as a substrate from the mixture target of hydroxyapatite (HA) and strontium-apatite (SrAp) at an Ar pressure of 0.5–5.0 Pa. The ratio of the SrAp in the mixture target was varied from 25% to 100%. After coating, the films were heated at 700 °C to remove the cellulose filter substrate, and the crystalline phases were identified by X-ray diffraction (XRD). The sputter-coated film was identified as the Sr-substituted β-tri-calcium phosphate (TCP) and the Sr-substituted β-calcium pyrophosphate (CPP) as well as the Sr-substituted HA. The weight ratio of the Sr-substituted HA decreased with increasing Ar pressure or with an increasing ratio of SrAp to HA in the target. The average Sr/(Ca + Sr) molar ratio in the film was 1.9%–3.5% slightly lower than the initial SrAp ratio of the target, and the ratio was not influenced by the Ar pressure. In the (Sr + Ca)/P ratio, the ratio decreased while increasing the SrAp ratio in the target. |
| Author | K. Ozeki T. Hoshino H. Aoki T. Masuzawa |
| AuthorAffiliation | Department of Mechanical Engineering, Ibaraki University, 4-12-1, Nakanarusawa, Hitachi, Ibaraki 316-8511, Japan International Apatite Co., Ltd., 20 Kanda-Ogawamachi 3-Chome, Chiyoda-ku, Tokyo 101-0052, Japan |
| Author_xml | – sequence: 1 givenname: K. surname: Ozeki fullname: Ozeki, K. email: ozeki@mx.ibaraki.ac.jp organization: Department of Mechanical Engineering, Ibaraki University, 4-12-1, Nakanarusawa, Hitachi, Ibaraki 316-8511, Japan – sequence: 2 givenname: T. surname: Hoshino fullname: Hoshino, T. organization: Department of Mechanical Engineering, Ibaraki University, 4-12-1, Nakanarusawa, Hitachi, Ibaraki 316-8511, Japan – sequence: 3 givenname: H. surname: Aoki fullname: Aoki, H. organization: International Apatite Co., Ltd., 20 Kanda-Ogawamachi 3-Chome, Chiyoda-ku, Tokyo 101-0052, Japan – sequence: 4 givenname: T. surname: Masuzawa fullname: Masuzawa, T. organization: Department of Mechanical Engineering, Ibaraki University, 4-12-1, Nakanarusawa, Hitachi, Ibaraki 316-8511, Japan |
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| Keywords | Strontium Crystal phase Hydroxyapatite Strontium-apatite Sputtering |
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| Notes | Sputtering; Hydroxyapatite; Strontium; Strontium-apatite; Crystal phase To obtain an Sr-substituted hydroxyapatite thin film, sputter-coating was performed on a cellulose filter acting as a substrate from the mixture target of hydroxyapatite （HA） and strontium-apatite （SrAp） at an Ar pressure of 0.5-5.0 Pa. The ratio of the SrAp in the mixture target was varied from 25% to 100%. After coating, the films were heated at 700 ℃ to remove the cellulose filter substrate, and the crystalline phases were identified by X-ray diffraction （XRD）. The sputter-coated film was identified as the Sr-substituted /3-tri-calcium phosphate （TCP） and the Sr-substituted/3-calcium pyrophosphate （CPP） as well as the Sr-substituted HA. The weight ratio of the Sr-substituted HA decreased with increasing Ar pressure or with an increasing ratio of SrAp to HA in the target. The average Sr/（Ca ＋ Sr） molar ratio in the film was 1.9%-3.5% slightly lower than the initial SrAp ratio of the target, and the ratio was not influenced by the Ar pressure. In the （Sr ＋ Ca）/P ratio, the ratio decreased while increasing the SrAp ratio in the target. 21-1315/TG K. Ozeki, T. Hoshino, H. Aoki, T. Masuzawa 1）Department of Mechanical Engineering, Ibaraki University, 4-12-1, Nakanarusawa, Hitachi, Ibaraki 316-8511, Japan 2） International Apatite Co., Ltd., 20 Kanda-Ogawamachi 3-Chome, Chiyoda-ku, Tokyo 101-0052, Japan |
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| SubjectTerms | Crystal phase Hydroxyapatite Sputtering Strontium Strontium-apatite X-射线衍射 宾夕法尼亚州 混合物 溅射薄膜 相组成 羟基磷灰石 行动方案 锶取代 |
| Title | Phase Composition of Sputtered Film from a Mixture Target of Hydroxyapatite and Strontium-apatite |
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