Amperometric sensor for the detection of hydrogen stable isotopes based on Pt nanoparticles confined within single-walled carbon nanotubes (SWNTs)
The development of hydrogen-based energy and nuclear energy requires new sensing material and high-performance gas sensor for hydrogen stable isotopes, hydrogen (H2) and deuterium (D2). Amperometric gas sensors based on SWNT-filled Pt composite material (Pt-SWNT-in) to combine the good electronic pr...
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| Published in | Sensors and actuators. B, Chemical Vol. 356; p. 131344 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Lausanne
Elsevier B.V
01.04.2022
Elsevier Science Ltd |
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| Abstract | The development of hydrogen-based energy and nuclear energy requires new sensing material and high-performance gas sensor for hydrogen stable isotopes, hydrogen (H2) and deuterium (D2). Amperometric gas sensors based on SWNT-filled Pt composite material (Pt-SWNT-in) to combine the good electronic properties of SWNTs and space-confined effect of Pt catalyst have been investigated for detecting H2 and D2. The Pt-SWNT-in electrode shows an excellent linear response in a wide range of 160–8000 ppm hydrogen in N2 atmosphere with the correlation coefficient of 0.9993, and compared to the electrode with Pt nanoparticles supported outside of SWNTs, its sensitivity per Pt loading is 3 times, moreover, it gives larger response current for detection of H2 in air and D2 in N2 atmosphere. Additionally, the Pt-SWNT-in electrode provides a response current to deuterium 0.9 times that to hydrogen in N2. The results present the Pt-SWNT-in electrode with superior sensitivity, selectivity, stability and a response variation for detection of hydrogen and deuterium, which would take advantage of the space-confined effect of SWNTs on Pt catalysts to enhance the sensor performance for detecting hydrogen stable isotopes, and provide an approach to discriminate between hydrogen and deuterium.
•Space-confined Pt nanoparticles in SWNTs combine good properties of SWNTs and Pt.•The confinement of Pt in SWNTs enhances sensitivity and response to H2 and D2.•The confinement of Pt in SWNTs enhances selectivity and stability.•Sensor response variation of H2 and D2 allows to discriminate between H2 and D2. |
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| AbstractList | The development of hydrogen-based energy and nuclear energy requires new sensing material and high-performance gas sensor for hydrogen stable isotopes, hydrogen (H2) and deuterium (D2). Amperometric gas sensors based on SWNT-filled Pt composite material (Pt-SWNT-in) to combine the good electronic properties of SWNTs and space-confined effect of Pt catalyst have been investigated for detecting H2 and D2. The Pt-SWNT-in electrode shows an excellent linear response in a wide range of 160–8000 ppm hydrogen in N2 atmosphere with the correlation coefficient of 0.9993, and compared to the electrode with Pt nanoparticles supported outside of SWNTs, its sensitivity per Pt loading is 3 times, moreover, it gives larger response current for detection of H2 in air and D2 in N2 atmosphere. Additionally, the Pt-SWNT-in electrode provides a response current to deuterium 0.9 times that to hydrogen in N2. The results present the Pt-SWNT-in electrode with superior sensitivity, selectivity, stability and a response variation for detection of hydrogen and deuterium, which would take advantage of the space-confined effect of SWNTs on Pt catalysts to enhance the sensor performance for detecting hydrogen stable isotopes, and provide an approach to discriminate between hydrogen and deuterium. The development of hydrogen-based energy and nuclear energy requires new sensing material and high-performance gas sensor for hydrogen stable isotopes, hydrogen (H2) and deuterium (D2). Amperometric gas sensors based on SWNT-filled Pt composite material (Pt-SWNT-in) to combine the good electronic properties of SWNTs and space-confined effect of Pt catalyst have been investigated for detecting H2 and D2. The Pt-SWNT-in electrode shows an excellent linear response in a wide range of 160–8000 ppm hydrogen in N2 atmosphere with the correlation coefficient of 0.9993, and compared to the electrode with Pt nanoparticles supported outside of SWNTs, its sensitivity per Pt loading is 3 times, moreover, it gives larger response current for detection of H2 in air and D2 in N2 atmosphere. Additionally, the Pt-SWNT-in electrode provides a response current to deuterium 0.9 times that to hydrogen in N2. The results present the Pt-SWNT-in electrode with superior sensitivity, selectivity, stability and a response variation for detection of hydrogen and deuterium, which would take advantage of the space-confined effect of SWNTs on Pt catalysts to enhance the sensor performance for detecting hydrogen stable isotopes, and provide an approach to discriminate between hydrogen and deuterium. •Space-confined Pt nanoparticles in SWNTs combine good properties of SWNTs and Pt.•The confinement of Pt in SWNTs enhances sensitivity and response to H2 and D2.•The confinement of Pt in SWNTs enhances selectivity and stability.•Sensor response variation of H2 and D2 allows to discriminate between H2 and D2. |
| ArticleNumber | 131344 |
| Author | Hu, Jiacheng Lv, Chao Sang, Ge Zeng, Ning Xu, Cigang |
| Author_xml | – sequence: 1 givenname: Jiacheng surname: Hu fullname: Hu, Jiacheng – sequence: 2 givenname: Ge surname: Sang fullname: Sang, Ge email: angelsg@163.com – sequence: 3 givenname: Ning surname: Zeng fullname: Zeng, Ning – sequence: 4 givenname: Chao surname: Lv fullname: Lv, Chao – sequence: 5 givenname: Cigang surname: Xu fullname: Xu, Cigang email: georgercgxu@qq.com |
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| CitedBy_id | crossref_primary_10_1109_LSENS_2023_3272779 crossref_primary_10_3390_chemosensors10090363 crossref_primary_10_3390_s24206637 crossref_primary_10_1016_j_ijhydene_2025_02_067 crossref_primary_10_1016_j_ijhydene_2023_02_033 crossref_primary_10_1149_1945_7111_ad22d8 crossref_primary_10_1002_adsr_202200057 crossref_primary_10_1002_cnma_202200355 crossref_primary_10_1039_D4RA08446B crossref_primary_10_1016_S1872_5805_23_60749_8 crossref_primary_10_1007_s10854_023_10386_x crossref_primary_10_1016_j_ijhydene_2023_12_153 crossref_primary_10_1109_JSEN_2022_3221114 crossref_primary_10_1109_JSEN_2024_3374354 |
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| Keywords | Space-confined effect Electrochemical sensor SWNT-filled Pt composite Amperometric gas sensor Hydrogen stable isotope |
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| SubjectTerms | Amperometric gas sensor Catalysts Composite materials Correlation coefficients Deuterium Electrical measurement Electrochemical sensor Electrodes Gas sensors Hydrogen Hydrogen stable isotope Hydrogen-based energy Isotopes Nanoparticles Nuclear energy Nuclear reactors Selectivity Sensitivity Sensors Single wall carbon nanotubes Space-confined effect SWNT-filled Pt composite |
| Title | Amperometric sensor for the detection of hydrogen stable isotopes based on Pt nanoparticles confined within single-walled carbon nanotubes (SWNTs) |
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