Simultaneous ion-exclusion/cation-exchange chromatography of anions and cations in acid rain waters on a weakly acidic cation-exchange resin by elution with sulfosalicylic acid
A simple, selective, and sensitive method for the simultaneous determination of anions (sulfate, nitrate, and chloride) and cations (sodium, ammonium, potassium, magnesium, and calcium) in acid rain waters was developed using ion-exclusion/cation-exchange chromatography with conductimetric detection...
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Published in | Journal of Chromatography A Vol. 884; no. 1; pp. 167 - 174 |
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Main Authors | , , , , , , |
Format | Journal Article Conference Proceeding |
Language | English |
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Amsterdam
Elsevier B.V
07.07.2000
Elsevier |
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Abstract | A simple, selective, and sensitive method for the simultaneous determination of anions (sulfate, nitrate, and chloride) and cations (sodium, ammonium, potassium, magnesium, and calcium) in acid rain waters was developed using ion-exclusion/cation-exchange chromatography with conductimetric detection. A weakly acidic cation-exchange resin column (Tosho TSKgel OA-PAK-A) and a sulfosalicylic acid–methanol–water eluent was used. With a mobile phase comprising 1.25 m
M sulfosalicylic acid in methanol–water (7.5:92.5) at 1.2 ml/min, simultaneous separation and detection of the above anions and cations was achieved in about 30 min. Linear calibration plots of peak area versus concentration were obtained over the concentration ranges 0–1.0 m
M for anions (
R=0.9991) and 0–0.5 m
M for cations (
R=0.9994). Detection limits calculated at
S/N=3 ranged from 4.2 to 14.8 ppb for the anions and from 2.4 to 12.1 ppb for the cations. The reproducibility of retention times was 0.14–0.15% relative standard deviation (RSD) for anions and 0.18–0.31% for cations, and reproducibility of chromatographic peak areas was 1.22–1.75% RSD for anions and 1.81–2.10% for cations. The method was applied successfully to the simultaneous determination of anions and cations in aerosols transported from mainland China to central Japan, as determined by a meteorological satellite data analyzer. |
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AbstractList | A simple, selective, and sensitive method for the simultaneous determination of anions (sulfate, nitrate, and chloride) and cations (sodium, ammonium, potassium, magnesium, and calcium) in acid rain waters was developed using ion-exclusion/cation-exchange chromatography with conductimetric detection. A weakly acidic cation-exchange resin column (Tosho TSKgel OA-PAK-A) and a sulfosalicylic acid–methanol–water eluent was used. With a mobile phase comprising 1.25 m
M sulfosalicylic acid in methanol–water (7.5:92.5) at 1.2 ml/min, simultaneous separation and detection of the above anions and cations was achieved in about 30 min. Linear calibration plots of peak area versus concentration were obtained over the concentration ranges 0–1.0 m
M for anions (
R=0.9991) and 0–0.5 m
M for cations (
R=0.9994). Detection limits calculated at
S/N=3 ranged from 4.2 to 14.8 ppb for the anions and from 2.4 to 12.1 ppb for the cations. The reproducibility of retention times was 0.14–0.15% relative standard deviation (RSD) for anions and 0.18–0.31% for cations, and reproducibility of chromatographic peak areas was 1.22–1.75% RSD for anions and 1.81–2.10% for cations. The method was applied successfully to the simultaneous determination of anions and cations in aerosols transported from mainland China to central Japan, as determined by a meteorological satellite data analyzer. A simple, selective, and sensitive method for the simultaneous determination of anions (sulfate, nitrate, and chloride) and cations (sodium, ammonium, potassium, magnesium, and calcium) in acid rain waters was developed using ion-exclusion/ cation-exchange chromatography with conductimetric detection. A weakly acidic cation-exchange resin column (Tosho TSKgel OA-PAK-A) and a sulfosalicylic acid-methanol-water eluent was used. With a mobile phase comprising 1.25 mM sulfosalicylic acid in methanol-water (7.5:92.5) at 1.2 ml/min, simultaneous separation and detection of the above anions and cations was achieved in about 30 min. Linear calibration plots of peak area versus concentration were obtained over the concentration ranges 0-1.0 mM for anions (R=0.9991) and 0-0.5 mM for cations (R=0.9994). Detection limits calculated at S/N=3 ranged from 4.2 to 14.8 ppb for the anions and from 2.4 to 12.1 ppb for the cations. The reproducibility of retention times was 0.14-0.15% relative standard deviation (RSD) for anions and 0.18-0.31% for cations, and reproducibility of chromatographic peak areas was 1.22-1.75% RSD for anions and 1.81-2.10% for cations. The method was applied successfully to the simultaneous determination of anions and cations in aerosols transported from mainland China to central Japan, as determined by a meteorological satellite data analyzer. |
Author | Miyanaga, Akiyoshi Hasebe, Kiyoshi Haddad, Paul R Fritz, James S Ohta, Kazutoku Tanaka, Kazuhiko Hu, Wenzhi |
Author_xml | – sequence: 1 givenname: Kazuhiko surname: Tanaka fullname: Tanaka, Kazuhiko email: ktanaka@nirin.go.jp organization: National Industrial Research Institute of Nagoya, Nagoya 462-8510, Japan – sequence: 2 givenname: Kazutoku surname: Ohta fullname: Ohta, Kazutoku organization: National Industrial Research Institute of Nagoya, Nagoya 462-8510, Japan – sequence: 3 givenname: Paul R surname: Haddad fullname: Haddad, Paul R organization: School of Chemistry, University of Tasmania, GPO Box 252-75, Hobart 7001, Australia – sequence: 4 givenname: James S surname: Fritz fullname: Fritz, James S organization: Iowa State University, Ames IA 50011, USA – sequence: 5 givenname: Akiyoshi surname: Miyanaga fullname: Miyanaga, Akiyoshi organization: Tosoh Corporation, Ayase 252, Japan – sequence: 6 givenname: Wenzhi surname: Hu fullname: Hu, Wenzhi organization: Hokkaido University, Sapporo 060, Japan – sequence: 7 givenname: Kiyoshi surname: Hasebe fullname: Hasebe, Kiyoshi organization: Hokkaido University, Sapporo 060, Japan |
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Cites_doi | 10.1016/S0021-9673(99)00286-1 10.1016/S0021-9673(98)00031-4 10.1016/S0021-9673(01)86902-8 10.1016/0021-9673(94)80245-9 10.1016/S0021-9673(97)00523-2 10.1016/S0021-9673(01)86803-5 10.1016/S0021-9673(00)83880-7 10.1016/S0021-9673(99)00232-0 10.1016/0021-9673(96)00213-0 |
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Keywords | Ion-exclusion/cation-exchange chromatography Sulfosalicylic acid Water analysis Mobile phase composition Inorganic anions Inorganic cations Environmental analysis Sodium Ions Ammonium Chemical analysis Cationic resin Phase composition Acid rain Nitrates Calcium Ions Mobile phase Sulfates Potassium Ions Gel permeation chromatography Ion exchange chromatography Electrochemical detector Inorganic cation Multicomponent analysis Inorganic anion Conductometry Chlorides Simultaneous measurement Rain water Magnesium Ions |
Language | English |
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References | Tanaka, Fritz (BIB10) 1986; 361 Tanaka, Ohta, Haddad, Fritz, Lee, Hasebe, Ieuji, Miyanaga (BIB5) 1999; 850 Tanaka, Chikara, Hu, Hasebe (BIB9) 1999; 850 Haddad, Jackson (BIB6) 1990 Ohta, Tanaka, Haddad (BIB13) 1996; 739 Tanaka, Haddad (BIB4) 1996; 15 Ohta, Tanaka, Haddad (BIB14) 1997; 782 M. Stumm, J.J. Morgan, Aquatic Chemistry; An Introduction Emphasizing Chemical Equilibria in Natural Water, Wiley, New York, 2nd ed., 1981. Tanaka, Ohta, Haddad, Fritz (BIB8) 1998; 804 Tanaka, Ohta, Fritz, Matsushita, Miyanaga (BIB2) 1994; 671 Gjerde, Fritz (BIB7) 1987 Tanaka, Fritz (BIB11) 1987; 409 Tanaka, Fritz (BIB3) 1995; 7 Waki, Tokunaga (BIB12) 1980; 201 Tanaka (10.1016/S0021-9673(00)00202-8_BIB4) 1996; 15 10.1016/S0021-9673(00)00202-8_BIB1 Ohta (10.1016/S0021-9673(00)00202-8_BIB14) 1997; 782 Haddad (10.1016/S0021-9673(00)00202-8_BIB6) 1990 Tanaka (10.1016/S0021-9673(00)00202-8_BIB3) 1995; 7 Tanaka (10.1016/S0021-9673(00)00202-8_BIB10) 1986; 361 Ohta (10.1016/S0021-9673(00)00202-8_BIB13) 1996; 739 Tanaka (10.1016/S0021-9673(00)00202-8_BIB2) 1994; 671 Tanaka (10.1016/S0021-9673(00)00202-8_BIB5) 1999; 850 Waki (10.1016/S0021-9673(00)00202-8_BIB12) 1980; 201 Tanaka (10.1016/S0021-9673(00)00202-8_BIB8) 1998; 804 Tanaka (10.1016/S0021-9673(00)00202-8_BIB9) 1999; 850 Gjerde (10.1016/S0021-9673(00)00202-8_BIB7) 1987 Tanaka (10.1016/S0021-9673(00)00202-8_BIB11) 1987; 409 |
References_xml | – volume: 850 start-page: 311 year: 1999 ident: BIB5 publication-title: J. Chromatogr. A contributor: fullname: Miyanaga – volume: 804 start-page: 179 year: 1998 ident: BIB8 publication-title: J. Chromatogr. A contributor: fullname: Fritz – volume: 15 start-page: 266 year: 1996 ident: BIB4 publication-title: Trends Anal. Chem. contributor: fullname: Haddad – volume: 361 start-page: 151 year: 1986 ident: BIB10 publication-title: J. Chromatogr. contributor: fullname: Fritz – volume: 671 start-page: 239 year: 1994 ident: BIB2 publication-title: J. Chromatogr. A contributor: fullname: Miyanaga – volume: 201 start-page: 259 year: 1980 ident: BIB12 publication-title: J. Chromatogr. contributor: fullname: Tokunaga – volume: 409 start-page: 271 year: 1987 ident: BIB11 publication-title: J. Chromatogr. contributor: fullname: Fritz – volume: 7 start-page: 30 year: 1995 ident: BIB3 publication-title: Am. Environ. Lab. contributor: fullname: Fritz – year: 1990 ident: BIB6 publication-title: Ion Chromatography — Principles and Applications contributor: fullname: Jackson – year: 1987 ident: BIB7 publication-title: Ion Chromatography contributor: fullname: Fritz – volume: 782 start-page: 331 year: 1997 ident: BIB14 publication-title: J. Chromatogr. A contributor: fullname: Haddad – volume: 850 start-page: 187 year: 1999 ident: BIB9 publication-title: J. Chromatogr. A contributor: fullname: Hasebe – volume: 739 start-page: 359 year: 1996 ident: BIB13 publication-title: J. Chromatogr. A contributor: fullname: Haddad – volume: 850 start-page: 311 year: 1999 ident: 10.1016/S0021-9673(00)00202-8_BIB5 publication-title: J. Chromatogr. A doi: 10.1016/S0021-9673(99)00286-1 contributor: fullname: Tanaka – year: 1987 ident: 10.1016/S0021-9673(00)00202-8_BIB7 contributor: fullname: Gjerde – volume: 7 start-page: 30 year: 1995 ident: 10.1016/S0021-9673(00)00202-8_BIB3 publication-title: Am. Environ. Lab. contributor: fullname: Tanaka – volume: 804 start-page: 179 year: 1998 ident: 10.1016/S0021-9673(00)00202-8_BIB8 publication-title: J. Chromatogr. A doi: 10.1016/S0021-9673(98)00031-4 contributor: fullname: Tanaka – volume: 361 start-page: 151 year: 1986 ident: 10.1016/S0021-9673(00)00202-8_BIB10 publication-title: J. Chromatogr. doi: 10.1016/S0021-9673(01)86902-8 contributor: fullname: Tanaka – volume: 671 start-page: 239 year: 1994 ident: 10.1016/S0021-9673(00)00202-8_BIB2 publication-title: J. Chromatogr. A doi: 10.1016/0021-9673(94)80245-9 contributor: fullname: Tanaka – volume: 782 start-page: 331 year: 1997 ident: 10.1016/S0021-9673(00)00202-8_BIB14 publication-title: J. Chromatogr. A doi: 10.1016/S0021-9673(97)00523-2 contributor: fullname: Ohta – volume: 15 start-page: 266 year: 1996 ident: 10.1016/S0021-9673(00)00202-8_BIB4 publication-title: Trends Anal. Chem. contributor: fullname: Tanaka – volume: 409 start-page: 271 year: 1987 ident: 10.1016/S0021-9673(00)00202-8_BIB11 publication-title: J. Chromatogr. doi: 10.1016/S0021-9673(01)86803-5 contributor: fullname: Tanaka – volume: 201 start-page: 259 year: 1980 ident: 10.1016/S0021-9673(00)00202-8_BIB12 publication-title: J. Chromatogr. doi: 10.1016/S0021-9673(00)83880-7 contributor: fullname: Waki – volume: 850 start-page: 187 year: 1999 ident: 10.1016/S0021-9673(00)00202-8_BIB9 publication-title: J. Chromatogr. A doi: 10.1016/S0021-9673(99)00232-0 contributor: fullname: Tanaka – volume: 739 start-page: 359 year: 1996 ident: 10.1016/S0021-9673(00)00202-8_BIB13 publication-title: J. Chromatogr. A doi: 10.1016/0021-9673(96)00213-0 contributor: fullname: Ohta – ident: 10.1016/S0021-9673(00)00202-8_BIB1 – year: 1990 ident: 10.1016/S0021-9673(00)00202-8_BIB6 contributor: fullname: Haddad |
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SubjectTerms | Analytical chemistry Anions - analysis Benzenesulfonates Cation Exchange Resins Cations - analysis Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Ion Exchange - methods Earth, ocean, space Exact sciences and technology External geophysics Hydrogen-Ion Concentration Inorganic anions Inorganic cations Meteorology Other chromatographic methods Reproducibility of Results Salicylates - chemistry Sensitivity and Specificity Sulfosalicylic acid Water in the atmosphere (humidity, clouds, evaporation, precipitation) |
Title | Simultaneous ion-exclusion/cation-exchange chromatography of anions and cations in acid rain waters on a weakly acidic cation-exchange resin by elution with sulfosalicylic acid |
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