Preparation of Si3N4-BCxN-TiN composite ceramic aerogels via foam-gelcasting
Recently, high-performance ceramic aerogels (CAs) have become a research hotspot because of their multi-functional properties. Compared to their oxide counterparts, non-oxide CAs show better thermal shock resistance and other high-temperature properties, making them suitable for applications in hars...
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| Published in | Journal of the European Ceramic Society Vol. 42; no. 6; pp. 2699 - 2706 |
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| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.06.2022
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| Subjects | |
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| Abstract | Recently, high-performance ceramic aerogels (CAs) have become a research hotspot because of their multi-functional properties. Compared to their oxide counterparts, non-oxide CAs show better thermal shock resistance and other high-temperature properties, making them suitable for applications in harsh environments. In this work, Si3N4-BCxN-TiN ceramic aerogels (SBCNT CAs) with molar ratios of B/C/Si/Ti = 2:1:5:5 were synthesized at 1623 K for 3 h via foam-gelcasting, from Si, Ti, melamine and boron acid raw materials. The prepared SBCNT CAs containing 91.0% porosity exhibited the highest compressive strength up to 1.0 MPa, and thermal conductivity of 0.144 W/(m·K) at 298 K. They also exhibited excellent service performance at 1473 K in Ar, demonstrating their great potential for high-temperature applications.
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| AbstractList | Recently, high-performance ceramic aerogels (CAs) have become a research hotspot because of their multi-functional properties. Compared to their oxide counterparts, non-oxide CAs show better thermal shock resistance and other high-temperature properties, making them suitable for applications in harsh environments. In this work, Si3N4-BCxN-TiN ceramic aerogels (SBCNT CAs) with molar ratios of B/C/Si/Ti = 2:1:5:5 were synthesized at 1623 K for 3 h via foam-gelcasting, from Si, Ti, melamine and boron acid raw materials. The prepared SBCNT CAs containing 91.0% porosity exhibited the highest compressive strength up to 1.0 MPa, and thermal conductivity of 0.144 W/(m·K) at 298 K. They also exhibited excellent service performance at 1473 K in Ar, demonstrating their great potential for high-temperature applications.
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| Author | Dong, Longhao Duan, Hongjuan Li, Guangqiang Han, Lei Zhang, Haijun Li, Faliang Zhang, Shaowei Jia, Quanli |
| Author_xml | – sequence: 1 givenname: Lei surname: Han fullname: Han, Lei organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 2 givenname: Longhao surname: Dong fullname: Dong, Longhao organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 3 givenname: Faliang surname: Li fullname: Li, Faliang organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 4 givenname: Hongjuan surname: Duan fullname: Duan, Hongjuan organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 5 givenname: Haijun surname: Zhang fullname: Zhang, Haijun email: zhanghaijun@wust.edu.cn organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 6 givenname: Guangqiang surname: Li fullname: Li, Guangqiang organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan 430081, China – sequence: 7 givenname: Quanli surname: Jia fullname: Jia, Quanli organization: Henan Key Laboratory of High Temperature Functional Ceramics, Zhengzhou University, Zhengzhou 450052, China – sequence: 8 givenname: Shaowei surname: Zhang fullname: Zhang, Shaowei email: s.zhang@exeter.ac.uk organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter EX4 4QF, UK |
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| Title | Preparation of Si3N4-BCxN-TiN composite ceramic aerogels via foam-gelcasting |
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