One-pot foam-gelcasting/nitridation synthesis of high porosity nano-whiskers based 3D Si3N4 porous ceramics
[Display omitted] •Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) were prepared via a facile one-pot foam-gelcasting/nitridation route at 1423–1523 K.•3D-NWSNPC showed excellent thermal conductivity, and a certain degree of recoverability under cyclic compressive loading.•The sample with s...
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| Published in | Journal of the European Ceramic Society Vol. 41; no. 12; pp. 6070 - 6074 |
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| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier Ltd
01.09.2021
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) were prepared via a facile one-pot foam-gelcasting/nitridation route at 1423–1523 K.•3D-NWSNPC showed excellent thermal conductivity, and a certain degree of recoverability under cyclic compressive loading.•The sample with solid loading of 12.5 wt% exhibited the highest compressive strength of 1.9 MPa, even though its porosity was high up to about 91 %.
Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) with high-porosity (about 91–93 %), low density (0.17–0.25 g/cm3), low thermal conductivity, and a certain degree of recoverability under cyclic compressive loading and reasonably strengths were prepared at 1423–1523 K via a one-pot foam-gelcasting/nitridation route using inexpensive commercial Si powders as starting materials and hexadecyl trimethyl ammonium bromide as foaming agent. After nitridation at 1523 K, the sample with an original solid loading of 12.5 wt% exhibited the highest compressive strength of 1.9 MPa, even though its density was lowered to 0.25 g/cm3. The sample nitrided at 1473 K had a relative density of 7.3 %. Its compressive and specific strength were respectively 1.1 MPa and 5.5 MPa·cm3 g−1, and its thermal conductivity was as low as 0.074 W/(m K) (measured at 323 K). These outstanding properties would make the as-prepared 3D-NWSNPC a promising candidate for applications in catalysis, filtration, thermal insulation and many other important areas. |
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| AbstractList | [Display omitted]
•Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) were prepared via a facile one-pot foam-gelcasting/nitridation route at 1423–1523 K.•3D-NWSNPC showed excellent thermal conductivity, and a certain degree of recoverability under cyclic compressive loading.•The sample with solid loading of 12.5 wt% exhibited the highest compressive strength of 1.9 MPa, even though its porosity was high up to about 91 %.
Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) with high-porosity (about 91–93 %), low density (0.17–0.25 g/cm3), low thermal conductivity, and a certain degree of recoverability under cyclic compressive loading and reasonably strengths were prepared at 1423–1523 K via a one-pot foam-gelcasting/nitridation route using inexpensive commercial Si powders as starting materials and hexadecyl trimethyl ammonium bromide as foaming agent. After nitridation at 1523 K, the sample with an original solid loading of 12.5 wt% exhibited the highest compressive strength of 1.9 MPa, even though its density was lowered to 0.25 g/cm3. The sample nitrided at 1473 K had a relative density of 7.3 %. Its compressive and specific strength were respectively 1.1 MPa and 5.5 MPa·cm3 g−1, and its thermal conductivity was as low as 0.074 W/(m K) (measured at 323 K). These outstanding properties would make the as-prepared 3D-NWSNPC a promising candidate for applications in catalysis, filtration, thermal insulation and many other important areas. |
| Author | Li, Guangqiang Shyng, Tommy Chang, Hong Han, Lei Zhang, Haijun Zhu, Yanqiu Li, Faliang Liu, Cheng Chen, Yu Zhang, Shaowei Jia, Quanli |
| Author_xml | – sequence: 1 givenname: Lei surname: Han fullname: Han, Lei organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan, 430081, China – sequence: 2 givenname: Yu surname: Chen fullname: Chen, Yu organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK – sequence: 3 givenname: Hong surname: Chang fullname: Chang, Hong organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK – sequence: 4 givenname: Faliang surname: Li fullname: Li, Faliang organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan, 430081, China – sequence: 5 givenname: Cheng surname: Liu fullname: Liu, Cheng organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK – sequence: 6 givenname: Tommy surname: Shyng fullname: Shyng, Tommy organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK – sequence: 7 givenname: Yanqiu orcidid: 0000-0003-3659-5643 surname: Zhu fullname: Zhu, Yanqiu organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK – sequence: 8 givenname: Guangqiang orcidid: 0000-0002-4471-7439 surname: Li fullname: Li, Guangqiang organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan, 430081, China – sequence: 9 givenname: Haijun surname: Zhang fullname: Zhang, Haijun email: zhanghaijun@wust.edu.cn organization: The State Key Laboratory of Refractories and Metallurgy, Wuhan University of Science and Technology, Wuhan, 430081, China – sequence: 10 givenname: Quanli surname: Jia fullname: Jia, Quanli organization: Henan Key Laboratory of High Temperature Functional Ceramics, Zhengzhou University, Zhengzhou, 450052, China – sequence: 11 givenname: Shaowei surname: Zhang fullname: Zhang, Shaowei email: s.zhang@exeter.ac.uk organization: College of Engineering, Mathematics and Physical Sciences, University of Exeter, Exeter, EX4 4QF, UK |
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| Keywords | Nano-whiskers One-pot synthesis Si3N4 porous ceramics High porosity Foam-gelcasting/nitridation |
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•Nano-whiskers based 3D Si3N4 porous ceramics (3D-NWSNPC) were prepared via a facile one-pot foam-gelcasting/nitridation route at 1423–1523... |
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| SubjectTerms | Foam-gelcasting/nitridation High porosity Nano-whiskers One-pot synthesis Si3N4 porous ceramics |
| Title | One-pot foam-gelcasting/nitridation synthesis of high porosity nano-whiskers based 3D Si3N4 porous ceramics |
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