Polyaniline/lignin blends: FTIR, MEV and electrochemical characterization

Blends of polyaniline (emeraldine base) and Eucalyptus grandis kraft lignin were prepared by casting method. The maximum amount of lignin that could be used for blending was 36% (w/w); beyond that, fractile films were produced. The IR spectra of the blends indicated that interactions occurred betwee...

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Published inEuropean polymer journal Vol. 38; no. 11; pp. 2213 - 2217
Main Authors Rodrigues, Paula C, Cantão, Maurı́cio P, Janissek, Paulo, Scarpa, Paulo C.N, Mathias, Alvaro L, Ramos, Luiz P, Gomes, Maria A.B
Format Journal Article
LanguageEnglish
Published Oxford Elsevier Ltd 01.11.2002
Elsevier
Subjects
Applied sciences
Cyclic voltammetry
Electrical, magnetic and optical properties
Exact sciences and technology
FTIR
Kraft lignin
MEV
Organic polymers
Physicochemistry of polymers
Polyaniline
Properties and characterization
Cyclic voltammetry
Polyaniline
FTIR
Kraft lignin
MEV
Intermolecular interaction
Conducting polymers
Solid state
Lignin
Electrochemical properties
Polymer blends
Morphology
Experimental study
Aniline polymer
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Abstract Blends of polyaniline (emeraldine base) and Eucalyptus grandis kraft lignin were prepared by casting method. The maximum amount of lignin that could be used for blending was 36% (w/w); beyond that, fractile films were produced. The IR spectra of the blends indicated that interactions occurred between polyaniline and lignin. Cyclic voltammetry measurements showed peaks that were readily attributed to the oxidation/reduction of polyaniline and a new oxi-reduction peak due to oxidation/reduction of sites created during interaction of two polymers. Scanning electronic microscopy showed that all blends were homogeneous.
AbstractList Blends of polyaniline (emeraldine base) and Eucalyptus grandis kraft lignin were prepared by casting method. The maximum amount of lignin that could be used for blending was 36% (w/w); beyond that, fractile films were produced. The IR spectra of the blends indicated that interactions occurred between polyaniline and lignin. Cyclic voltammetry measurements showed peaks that were readily attributed to the oxidation/reduction of polyaniline and a new oxi-reduction peak due to oxidation/reduction of sites created during interaction of two polymers. Scanning electronic microscopy showed that all blends were homogeneous.
Author Rodrigues, Paula C
Janissek, Paulo
Scarpa, Paulo C.N
Cantão, Maurı́cio P
Gomes, Maria A.B
Mathias, Alvaro L
Ramos, Luiz P
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  organization: Centro de Pesquisa em Quı́mica Aplicada, Departamento de Quı́mica, Universidade Federal do Paraná, P.O. Box 19081, 81531-990 Curitiba, PR, Brazil
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  givenname: Maurı́cio P
  surname: Cantão
  fullname: Cantão, Maurı́cio P
  organization: Instituto de Tecnologia para o Desenvolvimento, LACTEC, P.O. Box 19067, 81531-990 Curitiba, PR, Brazil
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  givenname: Paulo
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  organization: Instituto de Tecnologia para o Desenvolvimento, LACTEC, P.O. Box 19067, 81531-990 Curitiba, PR, Brazil
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  givenname: Paulo C.N
  surname: Scarpa
  fullname: Scarpa, Paulo C.N
  organization: Instituto de Tecnologia para o Desenvolvimento, LACTEC, P.O. Box 19067, 81531-990 Curitiba, PR, Brazil
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  givenname: Alvaro L
  surname: Mathias
  fullname: Mathias, Alvaro L
  organization: Departamento de Engenharia Quı́mica, Universidade Federal do Paraná, P.O. Box 19081, 81531-990 Curitiba, PR, Brazil
– sequence: 6
  givenname: Luiz P
  surname: Ramos
  fullname: Ramos, Luiz P
  organization: Centro de Pesquisa em Quı́mica Aplicada, Departamento de Quı́mica, Universidade Federal do Paraná, P.O. Box 19081, 81531-990 Curitiba, PR, Brazil
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  givenname: Maria A.B
  surname: Gomes
  fullname: Gomes, Maria A.B
  email: gomes@quimica.ufpr.br
  organization: Centro de Pesquisa em Quı́mica Aplicada, Departamento de Quı́mica, Universidade Federal do Paraná, P.O. Box 19081, 81531-990 Curitiba, PR, Brazil
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Issue 11
Keywords Cyclic voltammetry
Polyaniline
FTIR
Kraft lignin
MEV
Intermolecular interaction
Conducting polymers
Solid state
Lignin
Electrochemical properties
Polymer blends
Morphology
Experimental study
Aniline polymer
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Snippet Blends of polyaniline (emeraldine base) and Eucalyptus grandis kraft lignin were prepared by casting method. The maximum amount of lignin that could be used...
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SubjectTerms Applied sciences
Cyclic voltammetry
Electrical, magnetic and optical properties
Exact sciences and technology
FTIR
Kraft lignin
MEV
Organic polymers
Physicochemistry of polymers
Polyaniline
Properties and characterization
Title Polyaniline/lignin blends: FTIR, MEV and electrochemical characterization
URI https://dx.doi.org/10.1016/S0014-3057(02)00114-3
Volume 38
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