Defects materials of Institut Lavoisier-125(Ti) materials enhanced photocatalytic activity for toluene and chlorobenzene mixtures degradation: Mechanism study
[Display omitted] •Defects were introduced in MIL-125 to narrow the forbidden band width.•Improved the surface acidity of material for efficient degradation of mixed VOCs.•Revealed the catalytic mechanism using in situ DRIFTS spectroscopy and GC–MS. In this paper, the effect of three monocarboxylic...
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| Published in | Journal of colloid and interface science Vol. 660; pp. 423 - 439 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
Elsevier Inc
15.04.2024
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| Subjects | |
| Online Access | Get full text |
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| Abstract | [Display omitted]
•Defects were introduced in MIL-125 to narrow the forbidden band width.•Improved the surface acidity of material for efficient degradation of mixed VOCs.•Revealed the catalytic mechanism using in situ DRIFTS spectroscopy and GC–MS.
In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption–desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal–organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O2 and H2O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC–MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs. |
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| AbstractList | In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption-desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal-organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O
and H
O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC-MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs. [Display omitted] •Defects were introduced in MIL-125 to narrow the forbidden band width.•Improved the surface acidity of material for efficient degradation of mixed VOCs.•Revealed the catalytic mechanism using in situ DRIFTS spectroscopy and GC–MS. In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption–desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal–organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O2 and H2O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC–MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs. In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption-desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal-organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O2 and H2O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC-MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs.In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption-desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal-organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O2 and H2O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC-MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs. In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray diffractometry (XRD) and nitrogen adsorption–desorption curves indicated that small molecule acids (acetic acid, propionic acid and butyric acid) affected the morphology of MIL-125 and induced lamellar pores and structural defects in the crystals. Thermogravimetric measurements confirmed the presence of acid-regulated defective metal–organic frameworks (MOFs). Electrochemical tests and density function theory calculations indicated that acid modulation could change the forbidden bandwidth of the material. The acid modification strategy effectively promoted the transfer of photogenerated electrons and enhanced the adsorption and activation of O₂ and H₂O molecules, generating reactive radicals. The modified MOFs also showed excellent performance in the removal of mixed toluene and chlorobenzene. The degradation pathways of the mixture were analyzed by in situ infrared (IR) and gas chromatography-mass spectrometry (GC–MS). The mixture was converted to chlorophenolic intermediates in the presence of reactive oxygen species, further decomposed to form ethers and ethanol, and finally formed small molecules such as carbon dioxide and water. A feasible method was provided for the preparation of photocatalysts for the treatment of mixed VOCs. |
| Author | Yue, Ke Zhang, Xiaodong Li, Chenyu Yang, Yiqiong Bi, Fukun Feng, Xiangbo Rao, Renzhi Gao, Bin Wang, Yuxin Xu, Jingcheng |
| Author_xml | – sequence: 1 givenname: Xiaodong orcidid: 0000-0003-2217-6173 surname: Zhang fullname: Zhang, Xiaodong email: zhangxiaodong@usst.edu.cn organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 2 givenname: Bin surname: Gao fullname: Gao, Bin organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 3 givenname: Renzhi surname: Rao fullname: Rao, Renzhi organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 4 givenname: Fukun orcidid: 0000-0003-0115-2826 surname: Bi fullname: Bi, Fukun organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 5 givenname: Chenyu orcidid: 0009-0004-6973-0666 surname: Li fullname: Li, Chenyu organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 6 givenname: Ke surname: Yue fullname: Yue, Ke organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 7 givenname: Yuxin surname: Wang fullname: Wang, Yuxin organization: Institute of Applied Biotechnology, Taizhou Vocation & Technical College, Taizhou, Zhejiang 318000, China – sequence: 8 givenname: Jingcheng surname: Xu fullname: Xu, Jingcheng organization: School of Materials and Chemistry, University of Shanghai for Science and Technology, Shanghai 200093, China – sequence: 9 givenname: Xiangbo surname: Feng fullname: Feng, Xiangbo email: fengxiangbo@xjtu.edu.cn organization: Xi’an Key Laboratory of Advanced Photo-electronics Materials and Energy Conversion Device, School of Electronic Information, Xijing University, Xi’an 710123, Shaanxi, China – sequence: 10 givenname: Yiqiong surname: Yang fullname: Yang, Yiqiong email: yangyiqiong@usst.edu.cn organization: School of Environment and Architecture, University of Shanghai for Science and Technology, Shanghai 200093, China |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/38244508$$D View this record in MEDLINE/PubMed |
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| Keywords | Defect Synergistic mechanism Toluene and chlorobenzene mixtures Photocatalysis Acid regulation |
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•Defects were introduced in MIL-125 to narrow the forbidden band width.•Improved the surface acidity of material for efficient degradation of... In this paper, the effect of three monocarboxylic acids on MIL-125 synthesis was systematically investigated and the results were discussed in detail. X-ray... |
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| SubjectTerms | acetic acid Acid regulation adsorption butyric acid carbon dioxide chlorobenzene Defect electrochemistry ethanol gas chromatography-mass spectrometry nitrogen Photocatalysis photocatalysts propionic acid reactive oxygen species Synergistic mechanism thermogravimetry toluene Toluene and chlorobenzene mixtures X-ray diffraction |
| Title | Defects materials of Institut Lavoisier-125(Ti) materials enhanced photocatalytic activity for toluene and chlorobenzene mixtures degradation: Mechanism study |
| URI | https://dx.doi.org/10.1016/j.jcis.2024.01.012 https://www.ncbi.nlm.nih.gov/pubmed/38244508 https://www.proquest.com/docview/2925035703 https://www.proquest.com/docview/3153205477 |
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