Determination of epichlorohydrin by sulfite derivatization and ion chromatography: characterization of the sulfite derivatives by ion chromatography–mass spectrometry

• Published in: Journal of Chromatography A Vol. 1034; no. 1; pp. 243 - 247
• Main Authors: Bruzzoniti, Maria Concetta, Andrensek, Samo, Novic, Milko, Perrachon, Daniela, Sarzanini, Corrado
• Format: Journal Article
• Language: English
• Published: Amsterdam Elsevier B.V 23.04.2004; Elsevier
• Subjects: Analysis; Analytical biochemistry: general aspects, technics, instrumentation; Analytical chemistry; Analytical, structural and metabolic biochemistry; Biological and medical sciences; Chemistry; Chromatographic methods and physical methods associated with chromatography; Chromatography, Liquid - methods; Derivatization, LC; Epichlorohydrin; Epichlorohydrin - analysis; Exact sciences and technology; Fundamental and applied biological sciences. Psychology; General pharmacology; Medical sciences; Pharmacology. Drug treatments; Spectrometry, Mass, Electrospray Ionization - methods; Sulfite; Sulfites - chemistry; Sulfite; Epichlorohydrin; Derivatization, LC; Sulfites; Ion chromatography; Inorganic anion; Analysis; Liquid chromatography; Derivatization; Mass spectrometry

This work is an upgrade of a previously developed method [J. Chromatogr. A 884 (2000) 251] for epichlorohydrin determination by ion chromatography (IC) and conductivity detection. Here, an ion chromatography–mass spectrometry (IC–MS) coupling has been employed for the separation and the identificati...