Nanocomposite vacuum-Arc TiC/a-C:H coatings prepared using an additional ionization of acetylene
The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon-acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under wh...
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| Published in | Physics of metals and metallography Vol. 115; no. 7; pp. 723 - 729 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Moscow
Pleiades Publishing
01.07.2014
Springer Springer Nature B.V |
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| Abstract | The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon-acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under which the decomposition of acetylene is provided by the ionization and dissociation of molecules due to electron impacts and by the recharging of molecules through titanium and argon ions with subsequent dissociation should favor the most complete decomposition of acetylene in a wide range of pressures. With increasing acetylene pressure, the structure of the nanocomposite coating changes: the size of TiC crystallites decreases, and the fraction of interfaces (or the fraction of regions with a disordered (amorphous) structure) increases. The application of a bias voltage leads to an increase in the sizes of TiC nanocrystallites. The coatings with a maximum microhardness (∼40 GPa) have been obtained without the action of an electron beam under an acetylene pressure of ∼0.05–0.08 Pa and the atomic ratio Ti: C ∼ 0.9: 1.1 in the coating. |
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| AbstractList | The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon-acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under which the decomposition of acetylene is provided by the ionization and dissociation of molecules due to electron impacts and by the recharging of molecules through titanium and argon ions with subsequent dissociation should favor the most complete decomposition of acetylene in a wide range of pressures. With increasing acetylene pressure, the structure of the nanocomposite coating changes: the size of TiC crystallites decreases, and the fraction of interfaces (or the fraction of regions with a disordered (amorphous) structure) increases. The application of a bias voltage leads to an increase in the sizes of TiC nanocrystallites. The coatings with a maximum microhardness (∼40 GPa) have been obtained without the action of an electron beam under an acetylene pressure of ∼0.05–0.08 Pa and the atomic ratio Ti: C ∼ 0.9: 1.1 in the coating. The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon-acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under which the decomposition of acetylene is provided by the ionization and dissociation of molecules due to electron impacts and by the recharging of molecules through titanium and argon ions with subsequent dissociation should favor the most complete decomposition of acetylene in a wide range of pressures. With increasing acetylene pressure, the structure of the nanocomposite coating changes: the size of TiC crystallites decreases, and the fraction of interfaces (or the fraction of regions with a disordered (amorphous) structure) increases. The application of a bias voltage leads to an increase in the sizes of TiC nanocrystallites. The coatings with a maximum microhardness (40 GPa) have been obtained without the action of an electron beam under an acetylene pressure of 0.05-0.08 Pa and the atomic ratio Ti: C 0.9: 1.1 in the coating. The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon--acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under which the decomposition of acetylene is provided by the ionization and dissociation of molecules due to electron impacts and by the recharging of molecules through titanium and argon ions with subsequent dissociation should favor the most complete decomposition of acetylene in a wide range of pressures. With increasing acetylene pressure, the structure of the nanocomposite coating changes: the size of TiC crystallites decreases, and the fraction of interfaces (or the fraction of regions with a disordered (amorphous) structure) increases. The application of a bias voltage leads to an increase in the sizes of TiC nanocrystallites. The coatings with a maximum microhardness (~40 GPa) have been obtained without the action of an electron beam under an acetylene pressure of ~0.05-0.08 Pa and the atomic ratio Ti : C ~ 0.9 : 1.1 in the coating. Keywords: vacuum-arc deposition, electron beam, ionization of acetylene, nanocomposite TiC/a-C:H coatings, nanocrystalline titanium carbide, nanostructure DOI: 10.1134/S0031918X14070102 The composition, structure, and properties of TiC/a-C:H coatings obtained by simultaneous vacuum-arc deposition of titanium and carbon in a low-pressure argon-acetylene medium additionally activated by a low-energy (a few hundreds of electron-volts) electron beam. The creation of conditions under which the decomposition of acetylene is provided by the ionization and dissociation of molecules due to electron impacts and by the recharging of molecules through titanium and argon ions with subsequent dissociation should favor the most complete decomposition of acetylene in a wide range of pressures. With increasing acetylene pressure, the structure of the nanocomposite coating changes: the size of TiC crystallites decreases, and the fraction of interfaces (or the fraction of regions with a disordered (amorphous) structure) increases. The application of a bias voltage leads to an increase in the sizes of TiC nanocrystallites. The coatings with a maximum microhardness (40 GPa) have been obtained without the action of an electron beam under an acetylene pressure of 0.05-0.08 Pa and the atomic ratio Ti: C 0.9: 1.1 in the coating.[PUBLICATION ABSTRACT] |
| Audience | Academic |
| Author | Rubshtein, A. P. Emlin, D. R. Gavrilov, N. V. Volkova, E. G. Plotnikov, S. A. Trakhtenberg, I. Sh Vladimirov, A. B. |
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| Cites_doi | 10.1088/0022-3727/43/4/043001 10.1016/j.surfcoat.2005.12.007 10.1016/j.msea.2007.10.063 10.1016/j.tsf.2008.09.091 10.1134/S0020441211050046 10.1088/0963-0252/20/1/015003 10.1016/j.surfcoat.2010.05.020 10.1016/j.surfcoat.2008.06.040 10.1134/S102745100903001X |
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| Keywords | vacuum-arc deposition nanostructure electron beam ionization of acetylene nanocrystalline titanium carbide nanocomposite TiC/a-C:H coatings |
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| References | Plotnikov, Emlin, Trakhtenberg, Gavrilov (CR9) 2012; 55 Martínez-Martínez, López-Cartes, Fernández, Sánchez-López (CR4) 2009; 517 Gavrilov, Mamaev, Plotnikov, Rubshtein, Trakhtenberg, Ugov (CR10) 2010; 204 Lyakishev (CR13) 1996 Emlin, Men’shakov, Kuznetsov (CR11) 2013 Benedikt (CR2) 2010; 43 Kuznetsov, Borisov, Shepatkovskii, Veksler, Kozhevnikov (CR6) 2009; 3 Baby, Mahony, Maguire (CR3) 2011; 20 Trakhtepberg, Vladimirov, Rubshtein, Yugov, Kuz’mina, Vykhodets, Kurenykh (CR12) 2003; 96 Vitu, Polcar, Cvrcek, Novak, Macak, Viskocil, Cavaleiro (CR5) 2008; 202 Emlin, Plotnikov, Gavrilov (CR8) 2012; 55 Galvan, Pel, de Hosson (CR14) 2006; 201 Wang, Zhang, Wu (CR1) 2008; 488 Gavrilov, Men’shakov (CR7) 2011; 54 I Sh Trakhtepberg (9783_CR12) 2003; 96 M V Kuznetsov (9783_CR6) 2009; 3 N V Gavrilov (9783_CR10) 2010; 204 D R Emlin (9783_CR11) 2013 (9783_CR13) 1996 S A Plotnikov (9783_CR9) 2012; 55 T Vitu (9783_CR5) 2008; 202 N V Gavrilov (9783_CR7) 2011; 54 J Benedikt (9783_CR2) 2010; 43 D R Emlin (9783_CR8) 2012; 55 A Baby (9783_CR3) 2011; 20 Y Wang (9783_CR1) 2008; 488 D Martínez-Martínez (9783_CR4) 2009; 517 D Galvan (9783_CR14) 2006; 201 |
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Zaved., Fiz. contributor: fullname: S A Plotnikov – volume: 20 start-page: 015003 year: 2011 ident: 9783_CR3 publication-title: Plasma Sources Sci. Technol. doi: 10.1088/0963-0252/20/1/015003 contributor: fullname: A Baby – start-page: 167 volume-title: Proc. 11th Int. Conf. “Films and Coatibgs-2013 year: 2013 ident: 9783_CR11 contributor: fullname: D R Emlin – volume: 201 start-page: 590 year: 2006 ident: 9783_CR14 publication-title: Surf. Coat. Techn. doi: 10.1016/j.surfcoat.2005.12.007 contributor: fullname: D Galvan – volume-title: Phase Diagrams of Binary Metal Systems year: 1996 ident: 9783_CR13 – volume: 43 start-page: 43043001 year: 2010 ident: 9783_CR2 publication-title: J. Phys. D: Appl. Phys. doi: 10.1088/0022-3727/43/4/043001 contributor: fullname: J Benedikt – volume: 202 start-page: 5790 year: 2008 ident: 9783_CR5 publication-title: Surf. Coat. Techn. doi: 10.1016/j.surfcoat.2008.06.040 contributor: fullname: T Vitu |
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| SubjectTerms | Acetylene Chemical properties Chemistry and Materials Science Coatings Coatings industry Decomposition Electron beams Hardness Ionization Materials Science Metallic Materials Nanostructure Strength and Plasticity Titanium Titanium carbide |
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| Title | Nanocomposite vacuum-Arc TiC/a-C:H coatings prepared using an additional ionization of acetylene |
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