Capillary microextraction on sol–gel dendrimer coatings
Sol–gel capillary microextraction (CME) is a new direction in the solventless sample preparation for the preconcentration of trace analytes, and presents significant interest in environmental, pharmaceutical, petrochemical, biomedical, agricultural, food, flavor, and a host of other important areas....
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Published in | Journal of Chromatography A Vol. 1034; no. 1; pp. 1 - 11 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Amsterdam
Elsevier B.V
23.04.2004
Elsevier |
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Abstract | Sol–gel capillary microextraction (CME) is a new direction in the solventless sample preparation for the preconcentration of trace analytes, and presents significant interest in environmental, pharmaceutical, petrochemical, biomedical, agricultural, food, flavor, and a host of other important areas. It utilizes advanced material properties of organic–inorganic hybrid sol–gel polymers to perform efficient extraction and preconcentration of target compounds from a wide variety of matrices. In the present work, a novel benzyl-terminated dendron-based sol–gel coating was developed for CME. A detailed investigation was conducted to evaluate the performance of the newly developed sol–gel dendrimer coatings to perform solventless extraction of a wide range of polar and nonpolar analytes. The characteristic branched architecture of dendrons makes them structurally superior extraction media compared with their traditional linear polymeric counterparts. Sol–gel chemistry was used to chemically immobilize dendritic macromolecules on fused silica capillary inner surface. Due to the strong chemical bonding with the capillary inner walls, sol–gel dendron coatings showed excellent thermal and solvent stability in capillary microextraction in hyphenation with chromatographic analysis. Efficient extraction of a wide range of analytes from their aqueous solutions was accomplished using sol–gel dendron coated fused silica capillaries. Low parts per trillion level detection limits were achieved in CME–GC for both polar and nonpolar analytes including polyaromatic hydrocarbons (PAHs), aldehydes, ketones, phenols, and alcohols. |
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AbstractList | Sol–gel capillary microextraction (CME) is a new direction in the solventless sample preparation for the preconcentration of trace analytes, and presents significant interest in environmental, pharmaceutical, petrochemical, biomedical, agricultural, food, flavor, and a host of other important areas. It utilizes advanced material properties of organic–inorganic hybrid sol–gel polymers to perform efficient extraction and preconcentration of target compounds from a wide variety of matrices. In the present work, a novel benzyl-terminated dendron-based sol–gel coating was developed for CME. A detailed investigation was conducted to evaluate the performance of the newly developed sol–gel dendrimer coatings to perform solventless extraction of a wide range of polar and nonpolar analytes. The characteristic branched architecture of dendrons makes them structurally superior extraction media compared with their traditional linear polymeric counterparts. Sol–gel chemistry was used to chemically immobilize dendritic macromolecules on fused silica capillary inner surface. Due to the strong chemical bonding with the capillary inner walls, sol–gel dendron coatings showed excellent thermal and solvent stability in capillary microextraction in hyphenation with chromatographic analysis. Efficient extraction of a wide range of analytes from their aqueous solutions was accomplished using sol–gel dendron coated fused silica capillaries. Low parts per trillion level detection limits were achieved in CME–GC for both polar and nonpolar analytes including polyaromatic hydrocarbons (PAHs), aldehydes, ketones, phenols, and alcohols. |
Author | Kabir, Abuzar Hamlet, Christina Soo Yoo, Kyung Malik, Abdul Newkome, George R |
Author_xml | – sequence: 1 givenname: Abuzar surname: Kabir fullname: Kabir, Abuzar organization: Department of Chemistry, University of South Florida, 4202 E. Fowler Avenue, Tampa, FL 33620-5250, USA – sequence: 2 givenname: Christina surname: Hamlet fullname: Hamlet, Christina organization: Department of Chemistry, University of South Florida, 4202 E. Fowler Avenue, Tampa, FL 33620-5250, USA – sequence: 3 givenname: Kyung surname: Soo Yoo fullname: Soo Yoo, Kyung organization: Department of Chemistry, University of South Florida, 4202 E. Fowler Avenue, Tampa, FL 33620-5250, USA – sequence: 4 givenname: George R surname: Newkome fullname: Newkome, George R organization: Department of Chemistry, Institute for Polymer Science, The University of Akron, Akron, OH 44325, USA – sequence: 5 givenname: Abdul surname: Malik fullname: Malik, Abdul email: malik@chuma1.cas.usf.edu organization: Department of Chemistry, University of South Florida, 4202 E. Fowler Avenue, Tampa, FL 33620-5250, USA |
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Keywords | Ketones Polynuclear aromatic hydrocarbons Solid-phase microextraction Phenols Sol–gel Aldehydes Capillary microextraction Sol–gel dendrimer coating Alcohols Trace analysis Coating material Hydrocarbon Alcohol Aldehyde Polycyclic aromatic compound Ketone Chemical enrichment Solid phase microextraction Phenol Sample preparation Sol gel process |
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Snippet | Sol–gel capillary microextraction (CME) is a new direction in the solventless sample preparation for the preconcentration of trace analytes, and presents... Sol-gel capillary microextraction (CME) is a new direction in the solventless sample preparation for the preconcentration of trace analytes, and presents... |
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SubjectTerms | Alcohols Aldehydes Analysis Analytical biochemistry: general aspects, technics, instrumentation Analytical chemistry Analytical, structural and metabolic biochemistry Biological and medical sciences Capillary microextraction Chemistry Chromatographic methods and physical methods associated with chromatography Chromatography, Gel - methods Exact sciences and technology Fundamental and applied biological sciences. Psychology Gels General pharmacology Ketones Medical sciences Microscopy, Electron, Scanning Pharmacology. Drug treatments Phenols Polynuclear aromatic hydrocarbons Sensitivity and Specificity Solid-phase microextraction Sol–gel Sol–gel dendrimer coating |
Title | Capillary microextraction on sol–gel dendrimer coatings |
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