Fracture of polycrystalline graphene membranes by in situ nanoindentation in a scanning electron microscope
Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene membranes were subject to central point loads using a nanomanipulator combined with an atomic force microscope cantilever as a force sensor....
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| Published in | Physica status solidi. PSS-RRL. Rapid research letters Vol. 9; no. 10; pp. 564 - 569 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
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Berlin
WILEY-VCH Verlag Berlin GmbH
01.10.2015
WILEY‐VCH Verlag Berlin GmbH Wiley Subscription Services, Inc |
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| Abstract | Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene membranes were subject to central point loads using a nanomanipulator combined with an atomic force microscope cantilever as a force sensor. The grain boundaries of the polycrystalline graphene were visualized by Raman spectroscopy coupled with a carbon isotope labeling technique. Graphene membranes without any grain boundary had a failure strength of 45.4 ± 10.4 GPa, compared to 16.4 ± 5.1 GPa for those with grain boundaries when a Young's modulus was assumed to be 1 TPa. (© 2015 WILEY‐VCH Verlag GmbH &Co. KGaA, Weinheim)
The failure strength of polycrystalline monolayer graphene grown by chemical vapor deposition is investigated by in situ nanoindentation in a scanning electron microscope. By visualizing the grain boundaries with carbon isotope labeling and Raman mapping techniques, the mechanical property of monolayer graphene is correlated with the grain boundary density. |
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| AbstractList | Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene membranes were subject to central point loads using a nanomanipulator combined with an atomic force microscope cantilever as a force sensor. The grain boundaries of the polycrystalline graphene were visualized by Raman spectroscopy coupled with a carbon isotope labeling technique. Graphene membranes without any grain boundary had a failure strength of 45.4 ± 10.4 GPa, compared to 16.4 ± 5.1 GPa for those with grain boundaries when a Young's modulus was assumed to be 1 TPa. (© 2015 WILEY‐VCH Verlag GmbH &Co. KGaA, Weinheim) Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene membranes were subject to central point loads using a nanomanipulator combined with an atomic force microscope cantilever as a force sensor. The grain boundaries of the polycrystalline graphene were visualized by Raman spectroscopy coupled with a carbon isotope labeling technique. Graphene membranes without any grain boundary had a failure strength of 45.4 ± 10.4 GPa, compared to 16.4 ± 5.1 GPa for those with grain boundaries when a Young's modulus was assumed to be 1 TPa. (© 2015 WILEY‐VCH Verlag GmbH &Co. KGaA, Weinheim) The failure strength of polycrystalline monolayer graphene grown by chemical vapor deposition is investigated by in situ nanoindentation in a scanning electron microscope. By visualizing the grain boundaries with carbon isotope labeling and Raman mapping techniques, the mechanical property of monolayer graphene is correlated with the grain boundary density. Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene membranes were subject to central point loads using a nanomanipulator combined with an atomic force microscope cantilever as a force sensor. The grain boundaries of the polycrystalline graphene were visualized by Raman spectroscopy coupled with a carbon isotope labeling technique. Graphene membranes without any grain boundary had a failure strength of 45.4 plus or minus 10.4 GPa, compared to 16.4 plus or minus 5.1 GPa for those with grain boundaries when a Young's modulus was assumed to be 1 TPa. ( copyright 2015 WILEY-VCH Verlag GmbH &Co. KGaA, Weinheim) The failure strength of polycrystalline monolayer graphene grown by chemical vapor deposition is investigated by in situ nanoindentation in a scanning electron microscope. By visualizing the grain boundaries with carbon isotope labeling and Raman mapping techniques, the mechanical property of monolayer graphene is correlated with the grain boundary density. |
| Author | Suk, Ji Won Hao, Yufeng Mancevski, Vladimir Liechti, Kenneth M. Ruoff, Rodney S. |
| Author_xml | – sequence: 1 givenname: Ji Won surname: Suk fullname: Suk, Ji Won email: jwsuk@skku.edu organization: School of Mechanical Engineering, Sungkyunkwan University, 440-746, Suwon, Republic of Korea – sequence: 2 givenname: Vladimir surname: Mancevski fullname: Mancevski, Vladimir organization: Xidex Corporation, 78754, Austin, Texas, USA – sequence: 3 givenname: Yufeng surname: Hao fullname: Hao, Yufeng organization: Department of Mechanical Engineering and the Materials Science and Engineering Program, The University of Texas at Austin, 78712, Austin, Texas, USA – sequence: 4 givenname: Kenneth M. surname: Liechti fullname: Liechti, Kenneth M. organization: Department of Aerospace Engineering and Engineering Mechanics, The University of Texas at Austin, 78712, Austin, Texas, USA – sequence: 5 givenname: Rodney S. surname: Ruoff fullname: Ruoff, Rodney S. organization: Institute of Basic Sciences Center for Multidimensional Carbon Materials &Department of Chemistry and School of Materials Science and Engineering, Ulsan National Institute of Science and Technology, 689-798, Ulsan, Republic of Korea |
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| Snippet | Failure of polycrystalline graphene grown by chemical vapor deposition was investigated by nanoindentation in a scanning electron microscope. Circular graphene... |
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| SubjectTerms | Chemical vapor deposition Crystallization Failure Grain boundaries Graphene Marking Membranes Nanoindentation Scanning electron microscopy |
| Title | Fracture of polycrystalline graphene membranes by in situ nanoindentation in a scanning electron microscope |
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