Effect of water on Cu/Zn catalyst for hydrogenation of fatty methyl ester to fatty alcohol

The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave reactor system. The catalysts were characterized by means of XRD, BET, H 2 -TPR, SEM and TEM. The results indicate that catalytic activity de...

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Published in	The Korean journal of chemical engineering Vol. 26; no. 6; pp. 1574 - 1579
Main Authors	Huang, Hui, Cao, Guiping, Fan, Chunling, Wang, Shaohong, Wang, Shujia
Format	Journal Article
Language	English
Published	Boston Springer US 01.11.2009 한국화학공학회
Subjects	Biotechnology Catalysis Chemistry Chemistry and Materials Science Industrial Chemistry Industrial Chemistry/Chemical Engineering Materials Science Reaction Engineering 화학공학 Water Deactivation Fatty Alcohol Cu/Zn Catalyst
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Abstract	The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave reactor system. The catalysts were characterized by means of XRD, BET, H 2 -TPR, SEM and TEM. The results indicate that catalytic activity decreases with increased amount of water in methyl laurate. Correlating with the results from the above characterization, it is found that the main causes for the water deactivation of the Cu/Zn catalyst were the water occlusion of active catalyst sites by the low solubility of water in the substrate and the promotion of crystal growth, as well as the Cu/Zn catalyst agglomeration in the presence of water.
AbstractList	The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave reactor system. The catalysts were characterized by means of XRD, BET, H 2 -TPR, SEM and TEM. The results indicate that catalytic activity decreases with increased amount of water in methyl laurate. Correlating with the results from the above characterization, it is found that the main causes for the water deactivation of the Cu/Zn catalyst were the water occlusion of active catalyst sites by the low solubility of water in the substrate and the promotion of crystal growth, as well as the Cu/Zn catalyst agglomeration in the presence of water. The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave reactor system. The catalysts were characterized by means of XRD, BET, H2-TPR, SEM and TEM. The results indicate that catalytic activity decreases with increased amount of water in methyl laurate. Correlating with the results from the above characterization, it is found that the main causes for the water deactivation of the Cu/Zn catalyst were the water occlusion of active catalyst sites by the low solubility of water in the substrate and the promotion of crystal growth, as well as the Cu/Zn catalyst agglomeration in the presence of water. KCI Citation Count: 16
Author	Wang, Shaohong Wang, Shujia Cao, Guiping Huang, Hui Fan, Chunling
Author_xml	– sequence: 1 givenname: Hui surname: Huang fullname: Huang, Hui organization: UNILAB, State Key Lab of Chemical Engineering, East China University of Science and Technology – sequence: 2 givenname: Guiping surname: Cao fullname: Cao, Guiping email: gpcao@ecust.edu.cn organization: UNILAB, State Key Lab of Chemical Engineering, East China University of Science and Technology – sequence: 3 givenname: Chunling surname: Fan fullname: Fan, Chunling organization: UNILAB, State Key Lab of Chemical Engineering, East China University of Science and Technology – sequence: 4 givenname: Shaohong surname: Wang fullname: Wang, Shaohong organization: Shanghai Zhongyuan Chemical Company Ltd – sequence: 5 givenname: Shujia surname: Wang fullname: Wang, Shujia organization: Shanghai Zhongyuan Chemical Company Ltd
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Snippet	The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave... The effect of water on Cu/Zn catalyst prepared by co-precipitation for hydrogenation of methyl laurate in a slurry phase was studied using a stirred autoclave...
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Title	Effect of water on Cu/Zn catalyst for hydrogenation of fatty methyl ester to fatty alcohol
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