X-Ray Diffraction and Cation Distribution Studies in Zinc-Substituted Nickel Ferrite Nanoparticles
Structural and cation distribution studies on Ni 1− x Zn x Fe 2 O 4 (with x =0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction analysis are reported. In this work the Nickel–Zinc ferrites nanoparticles are synthesized by sol–gel auto combustion using respective metal...
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Published in | Journal of superconductivity and novel magnetism Vol. 27; no. 2; pp. 547 - 553 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
Published |
New York
Springer US
01.02.2014
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Abstract | Structural and cation distribution studies on Ni
1−
x
Zn
x
Fe
2
O
4
(with
x
=0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction analysis are reported. In this work the Nickel–Zinc ferrites nanoparticles are synthesized by sol–gel auto combustion using respective metal nitrates and citric acid as fuel for the auto combustion reaction. Formation of ferrite nanoparticles having single-phase spinel structure is evident from the obtained X-ray diffraction patterns. Lattice constant values of the Ni
1−
x
Zn
x
Fe
2
O
4
ferrite system are found to increase with increase of zinc substitution
x
. Broad and intense XRD peaks in the patterns indicate the nanocrystalline nature of the produced ferrite samples. Average particle size calculated from most intense Bragg’s reflection (311) using Debye–Scherrer’s formula is found to be 30 nm. The particle size is found to decrease with increase in zinc substitution
x
. Observed X-ray density is found to decrease with increase in zinc substitution
x
. Bulk density, porosity, and unit cell volume are also calculated from the XRD data. Distribution of metal cations in the spinel structure estimated from X-ray diffraction data show that along with Ni
2+
ions most of the Zn
2+
ions also occupy the octahedral [B] sites, which are attributed to nanosize dimensions of the ferrite samples. |
---|---|
AbstractList | Structural and cation distribution studies on Ni
1−
x
Zn
x
Fe
2
O
4
(with
x
=0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction analysis are reported. In this work the Nickel–Zinc ferrites nanoparticles are synthesized by sol–gel auto combustion using respective metal nitrates and citric acid as fuel for the auto combustion reaction. Formation of ferrite nanoparticles having single-phase spinel structure is evident from the obtained X-ray diffraction patterns. Lattice constant values of the Ni
1−
x
Zn
x
Fe
2
O
4
ferrite system are found to increase with increase of zinc substitution
x
. Broad and intense XRD peaks in the patterns indicate the nanocrystalline nature of the produced ferrite samples. Average particle size calculated from most intense Bragg’s reflection (311) using Debye–Scherrer’s formula is found to be 30 nm. The particle size is found to decrease with increase in zinc substitution
x
. Observed X-ray density is found to decrease with increase in zinc substitution
x
. Bulk density, porosity, and unit cell volume are also calculated from the XRD data. Distribution of metal cations in the spinel structure estimated from X-ray diffraction data show that along with Ni
2+
ions most of the Zn
2+
ions also occupy the octahedral [B] sites, which are attributed to nanosize dimensions of the ferrite samples. Structural and cation distribution studies on Ni1ax Zn x Fe2O4 (with x=0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction analysis are reported. In this work the NickelaZinc ferrites nanoparticles are synthesized by sol-gel auto combustion using respective metal nitrates and citric acid as fuel for the auto combustion reaction. Formation of ferrite nanoparticles having single-phase spinel structure is evident from the obtained X-ray diffraction patterns. Lattice constant values of the Ni1ax Zn x Fe2O4 ferrite system are found to increase with increase of zinc substitution x. Broad and intense XRD peaks in the patterns indicate the nanocrystalline nature of the produced ferrite samples. Average particle size calculated from most intense Braggas reflection (311) using DebyeaScherreras formula is found to be 30 nm. The particle size is found to decrease with increase in zinc substitution x. Observed X-ray density is found to decrease with increase in zinc substitution x. Bulk density, porosity, and unit cell volume are also calculated from the XRD data. Distribution of metal cations in the spinel structure estimated from X-ray diffraction data show that along with Ni2+ ions most of the Zn2+ ions also occupy the octahedral [B] sites, which are attributed to nanosize dimensions of the ferrite samples. |
Author | Kurmude, D. V. Raut, A. V. Jadhav, K. M. Shengule, D. R. Barkule, R. S. |
Author_xml | – sequence: 1 givenname: D. V. surname: Kurmude fullname: Kurmude, D. V. organization: Milind College of Science – sequence: 2 givenname: R. S. surname: Barkule fullname: Barkule, R. S. organization: Department of Physics, Dr. Babasaheb Ambedkar Marathwada University – sequence: 3 givenname: A. V. surname: Raut fullname: Raut, A. V. organization: Department of Physics, Dr. Babasaheb Ambedkar Marathwada University – sequence: 4 givenname: D. R. surname: Shengule fullname: Shengule, D. R. organization: Vivekanand Arts, Sardar Dalipsingh Commerce and Science College – sequence: 5 givenname: K. M. surname: Jadhav fullname: Jadhav, K. M. email: drjadhavkm@gmail.com organization: Department of Physics, Dr. Babasaheb Ambedkar Marathwada University |
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References_xml | – volume-title: The Rietveld Method year: 1993 ident: 2305_CR12 doi: 10.1093/oso/9780198555773.001.0001 contributor: fullname: R.A. Young – volume: 82 start-page: 12 year: 1999 ident: 2305_CR2 publication-title: J. Am. Ceram. Soc. doi: 10.1111/j.1151-2916.1999.tb02241.x contributor: fullname: K.E. Sickafus – ident: 2305_CR17 – ident: 2305_CR27 – start-page: 301 volume-title: Elements of X-Ray Diffraction year: 2000 ident: 2305_CR24 contributor: fullname: B.D. Cullity – volume: 98 year: 2011 ident: 2305_CR10 publication-title: Appl. Phys. Lett. contributor: fullname: G.D. Tang – volume: 36 start-page: 21 year: 2001 ident: 2305_CR3 publication-title: J. Mater. Sci. doi: 10.1023/A:1004866119183 contributor: fullname: Q.M. Wei – ident: 2305_CR33 – ident: 2305_CR41 doi: 10.1007/BF02707350 – ident: 2305_CR36 doi: 10.1107/S0567739476001551 – ident: 2305_CR47 doi: 10.1109/20.489779 – volume: 16 start-page: 4 year: 1981 ident: 2305_CR8 publication-title: Pramana contributor: fullname: V.K. Singh – ident: 2305_CR44 doi: 10.1023/B:JMSC.0000011497.30763.bc – ident: 2305_CR16 doi: 10.1007/s10853-006-0929-3 – ident: 2305_CR22 – volume: 24 issue: 2 year: 2011 ident: 2305_CR21 publication-title: Int. J. Comput. Appl. contributor: fullname: V. Naidu – ident: 2305_CR43 – volume-title: Dielectric Materials for Wireless Communication year: 2008 ident: 2305_CR46 contributor: fullname: M.T. Sebastian – ident: 2305_CR31 doi: 10.1016/j.mseb.2004.12.018 – ident: 2305_CR28 doi: 10.1063/1.1699501 – ident: 2305_CR37 doi: 10.1016/j.jmmm.2011.10.017 – ident: 2305_CR32 – volume-title: Crystal Structure Analysis year: 1960 ident: 2305_CR38 contributor: fullname: M.G. Buerger – ident: 2305_CR51 doi: 10.4314/ijest.v2i8.63832 – ident: 2305_CR25 doi: 10.1016/j.jmmm.2009.05.074 – volume: 111 year: 2012 ident: 2305_CR7 publication-title: J. Appl. Phys. contributor: fullname: S.L. Cheng – ident: 2305_CR48 – ident: 2305_CR29 doi: 10.1103/PhysRevB.8.29 – ident: 2305_CR35 doi: 10.1007/s10853-005-6099-x – ident: 2305_CR40 doi: 10.1143/JPSJ.16.1881 – ident: 2305_CR14 doi: 10.1016/0022-1902(73)80531-7 – volume: 37 start-page: 3 year: 2002 ident: 2305_CR1 publication-title: J. Mater. Sci. doi: 10.1023/A:1013790129045 contributor: fullname: A.K. Nikumbh – ident: 2305_CR20 doi: 10.1016/j.matchemphys.2005.12.012 – ident: 2305_CR18 – start-page: 233 volume-title: Ferrites year: 1959 ident: 2305_CR26 contributor: fullname: J. Smit – ident: 2305_CR45 – ident: 2305_CR50 doi: 10.1016/S1452-3981(23)19503-4 – ident: 2305_CR30 – ident: 2305_CR13 doi: 10.1039/DT9850002155 – volume: 48 start-page: 4 year: 2010 ident: 2305_CR5 publication-title: Chin. J. Phys. contributor: fullname: A.T. Raghavender – ident: 2305_CR15 doi: 10.1016/S0921-4526(00)00286-6 – ident: 2305_CR34 – volume: 30 start-page: 479 year: 1968 ident: 2305_CR49 publication-title: J. Inorg. Nucl. Chem. doi: 10.1016/0022-1902(68)80475-0 contributor: fullname: A. Navrotsky – volume: 64 start-page: 9 year: 1981 ident: 2305_CR9 publication-title: J. Am. Ceram. Soc. doi: 10.1111/j.1151-2916.1981.tb09550.x contributor: fullname: C.C. Wu – ident: 2305_CR23 doi: 10.1021/ef070064w – ident: 2305_CR11 doi: 10.1107/S0021889869006558 – ident: 2305_CR19 doi: 10.1111/j.1551-2916.2005.00098.x – ident: 2305_CR39 doi: 10.1023/A:1014505620254 – ident: 2305_CR42 doi: 10.1016/0022-4596(74)90108-X – ident: 2305_CR6 doi: 10.1016/0041-0101(83)90286-6 – volume: 82 start-page: 11 year: 1960 ident: 2305_CR4 publication-title: J. Am. Chem. Soc. contributor: fullname: C.G. Whinfery |
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Snippet | Structural and cation distribution studies on Ni
1−
x
Zn
x
Fe
2
O
4
(with
x
=0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction... Structural and cation distribution studies on Ni1ax Zn x Fe2O4 (with x=0.0, 0.2, 0.4, 0.6, 0.8, and 1.0) ferrite nanoparticles by using X-ray diffraction... |
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SubjectTerms | Cations Characterization and Evaluation of Materials Condensed Matter Physics Magnetic Materials Magnetism Original Paper Physics Physics and Astronomy Strongly Correlated Systems Superconductivity |
Title | X-Ray Diffraction and Cation Distribution Studies in Zinc-Substituted Nickel Ferrite Nanoparticles |
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