Hydrate seeding effect on the metastability of CH4 hydrate
Cyclopentane (CP) hydrate seeds can lead to nucleation of CH 4 hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate the metastable zone width (MSZW) of CH 4 hydrate. To verify the crystal structure of CH 4 hydrate formed from the CP hydrate seeds, the hyd...
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| Published in | The Korean journal of chemical engineering Vol. 37; no. 2; pp. 341 - 349 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.02.2020
Springer Nature B.V 한국화학공학회 |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0256-1115 1975-7220 |
| DOI | 10.1007/s11814-019-0451-3 |
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| Abstract | Cyclopentane (CP) hydrate seeds can lead to nucleation of CH
4
hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate the metastable zone width (MSZW) of CH
4
hydrate. To verify the crystal structure of CH
4
hydrate formed from the CP hydrate seeds, the hydrate samples were analyzed by high resolution powder diffraction (HRPD). 1 wt% of CP hydrates in the system reduced the MSZW of CH
4
hydrate from 3.39 K to 1.32 K, and showed synergetic performance with sodium dodecyl sulfate (SDS). From the hydrate nucleation theory, SDS is able to decrease the effective surface energy for heterogeneous nucleation on the stainless steel wall, but the CP hydrate seeds provide new nucleation sites with even lower surface energy than that of the stainless steel wall. Hence, the nucleation rate depends on the amount of CP hydrate seeds, and the kinetic parameter can be estimated from the concentration of nucleation sites on the CP hydrate seeds. Also, the MSZW of CH
4
hydrate was satisfactorily correlated with the amount of CP hydrate seeds by the cumulative nucleation potentials using estimated kinetic parameters. |
|---|---|
| AbstractList | Cyclopentane (CP) hydrate seeds can lead to nucleation of CH4 hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate the metastable zone width (MSZW) of CH4 hydrate. To verify the crystal structure of CH4 hydrate formed from the CP hydrate seeds, the hydrate samples were analyzed by high resolution powder diffraction (HRPD). 1wt% of CP hydrates in the system reduced the MSZW of CH4 hydrate from 3.39 K to 1.32 K, and showed synergetic performance with sodium dodecyl sulfate (SDS). From the hydrate nucleation theory, SDS is able to decrease the effective surface energy for heterogeneous nucleation on the stainless steel wall, but the CP hydrate seeds provide new nucleation sites with even lower surface energy than that of the stainless steel wall. Hence, the nucleation rate depends on the amount of CP hydrate seeds, and the kinetic parameter can be estimated from the concentration of nucleation sites on the CP hydrate seeds. Also, the MSZW of CH4 hydrate was satisfactorily correlated with the amount of CP hydrate seeds by the cumulative nucleation potentials using estimated kinetic parameters. KCI Citation Count: 8 Cyclopentane (CP) hydrate seeds can lead to nucleation of CH 4 hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate the metastable zone width (MSZW) of CH 4 hydrate. To verify the crystal structure of CH 4 hydrate formed from the CP hydrate seeds, the hydrate samples were analyzed by high resolution powder diffraction (HRPD). 1 wt% of CP hydrates in the system reduced the MSZW of CH 4 hydrate from 3.39 K to 1.32 K, and showed synergetic performance with sodium dodecyl sulfate (SDS). From the hydrate nucleation theory, SDS is able to decrease the effective surface energy for heterogeneous nucleation on the stainless steel wall, but the CP hydrate seeds provide new nucleation sites with even lower surface energy than that of the stainless steel wall. Hence, the nucleation rate depends on the amount of CP hydrate seeds, and the kinetic parameter can be estimated from the concentration of nucleation sites on the CP hydrate seeds. Also, the MSZW of CH 4 hydrate was satisfactorily correlated with the amount of CP hydrate seeds by the cumulative nucleation potentials using estimated kinetic parameters. Cyclopentane (CP) hydrate seeds can lead to nucleation of CH4 hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate the metastable zone width (MSZW) of CH4 hydrate. To verify the crystal structure of CH4 hydrate formed from the CP hydrate seeds, the hydrate samples were analyzed by high resolution powder diffraction (HRPD). 1 wt% of CP hydrates in the system reduced the MSZW of CH4 hydrate from 3.39 K to 1.32 K, and showed synergetic performance with sodium dodecyl sulfate (SDS). From the hydrate nucleation theory, SDS is able to decrease the effective surface energy for heterogeneous nucleation on the stainless steel wall, but the CP hydrate seeds provide new nucleation sites with even lower surface energy than that of the stainless steel wall. Hence, the nucleation rate depends on the amount of CP hydrate seeds, and the kinetic parameter can be estimated from the concentration of nucleation sites on the CP hydrate seeds. Also, the MSZW of CH4 hydrate was satisfactorily correlated with the amount of CP hydrate seeds by the cumulative nucleation potentials using estimated kinetic parameters. |
| Author | Ahn, Yun-Ho Baek, Seungjun Lee, Wonhyeong Lee, Jae W. Min, Juwon Kang, Dong Woo |
| Author_xml | – sequence: 1 givenname: Seungjun surname: Baek fullname: Baek, Seungjun organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) – sequence: 2 givenname: Wonhyeong surname: Lee fullname: Lee, Wonhyeong organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) – sequence: 3 givenname: Juwon surname: Min fullname: Min, Juwon organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) – sequence: 4 givenname: Yun-Ho surname: Ahn fullname: Ahn, Yun-Ho organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) – sequence: 5 givenname: Dong Woo surname: Kang fullname: Kang, Dong Woo organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) – sequence: 6 givenname: Jae W. surname: Lee fullname: Lee, Jae W. email: jaewlee@kaist.ac.kr organization: Department of Chemical and Biomolecular Engineering, Korea Advanced Institute of Science and Technology (KAIST) |
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| Keywords | Methane Hydrates Hydrate Seed Crystals Hydrate Nucleation Metastable Zone Width Cyclopentane Hydrates |
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| Snippet | Cyclopentane (CP) hydrate seeds can lead to nucleation of CH
4
hydrate with a lower supersaturation; the concept of nucleation potential was applied to... Cyclopentane (CP) hydrate seeds can lead to nucleation of CH4 hydrate with a lower supersaturation; the concept of nucleation potential was applied to estimate... |
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| SubjectTerms | Biotechnology Catalysis Chemistry Chemistry and Materials Science Crystal structure Industrial Chemistry/Chemical Engineering Materials Science Methane hydrates Nucleation Parameter estimation Separation Technology Sodium dodecyl sulfate Stainless steel Stainless steels Steel structures Supersaturation Surface energy Thermodynamics Walls 화학공학 |
| Title | Hydrate seeding effect on the metastability of CH4 hydrate |
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