Enhanced adsorption and reduction performance of nitrate by Fe–Pd–Fe3O4 embedded multi-walled carbon nanotubes

Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degr...

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Published inChemosphere (Oxford) Vol. 281; p. 130718
Main Authors Wang, Zeyu, Dai, Luyao, Yao, Jiachao, Guo, Tianjiao, Hrynsphan, Dzmitry, Tatsiana, Savitskaya, Chen, Jun
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.10.2021
Subjects
adsorbents
Adsorption
carbon nanotubes
chemical reduction
energy
Fe–Pd–Fe3O4/MWCNTs
nitrates
NO3−-N
Recovery
Reduction
water pollution
Reduction
NO3−-N
Adsorption
Recovery
Fe–Pd–Fe3O4/MWCNTs
Online AccessGet full text
ISSN0045-6535
1879-1298
1879-1298
DOI10.1016/j.chemosphere.2021.130718

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Abstract Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degradation of pollutants. Therefore, the removal process of NO3−-N by Fe–Pd–Fe3O4/MWCNTs was studied, including rapid adsorption of initial pollutants, gradual reduction of intermediate products and re-adsorption of final products. The results showed that Fe–Pd–Fe3O4/MWCNTs completely removed NO3−-N within 2 h, 39% and 25% of which were converted into NO2−-N and NH4+-N. The adsorption efficiency, kinetics, capacity and adsorption energy all followed the order of NH4+-N > NO2−-N > NO3−-N. With the recoverability and reusability of Fe–Pd–Fe3O4/MWCNTs having been confirmed in 5 consecutive cycles, the removal rate of NO3−-N still reached 43%. It has been shown that MWCNTs prolonged the reducing power for NO3−-N, due to avoiding the aggregation of metal particles. The rapid adsorption of initial pollutants, effective stepwise reduction and convenient recovery processes were of great value for the rehabilitation of polluted water. [Display omitted] •50 mg/L Fe–Pd–Fe3O4/MWCNTs completely removed 100 mg/L NO3−-N within 2 h.•36% of adsorbed NO3−-N was converted into N2 or N2O.•The removal efficiency of NO3−-N reached 43% by Fe–Pd–Fe3O4/MWCNTs in 5 cycles.
AbstractList Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degradation of pollutants. Therefore, the removal process of NO₃⁻-N by Fe–Pd–Fe₃O₄/MWCNTs was studied, including rapid adsorption of initial pollutants, gradual reduction of intermediate products and re-adsorption of final products. The results showed that Fe–Pd–Fe₃O₄/MWCNTs completely removed NO₃⁻-N within 2 h, 39% and 25% of which were converted into NO₂⁻-N and NH₄⁺-N. The adsorption efficiency, kinetics, capacity and adsorption energy all followed the order of NH₄⁺-N > NO₂⁻-N > NO₃⁻-N. With the recoverability and reusability of Fe–Pd–Fe₃O₄/MWCNTs having been confirmed in 5 consecutive cycles, the removal rate of NO₃⁻-N still reached 43%. It has been shown that MWCNTs prolonged the reducing power for NO₃⁻-N, due to avoiding the aggregation of metal particles. The rapid adsorption of initial pollutants, effective stepwise reduction and convenient recovery processes were of great value for the rehabilitation of polluted water.
Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degradation of pollutants. Therefore, the removal process of NO3--N by Fe-Pd-Fe3O4/MWCNTs was studied, including rapid adsorption of initial pollutants, gradual reduction of intermediate products and re-adsorption of final products. The results showed that Fe-Pd-Fe3O4/MWCNTs completely removed NO3--N within 2 h, 39% and 25% of which were converted into NO2--N and NH4+-N. The adsorption efficiency, kinetics, capacity and adsorption energy all followed the order of NH4+-N > NO2--N > NO3--N. With the recoverability and reusability of Fe-Pd-Fe3O4/MWCNTs having been confirmed in 5 consecutive cycles, the removal rate of NO3--N still reached 43%. It has been shown that MWCNTs prolonged the reducing power for NO3--N, due to avoiding the aggregation of metal particles. The rapid adsorption of initial pollutants, effective stepwise reduction and convenient recovery processes were of great value for the rehabilitation of polluted water.Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degradation of pollutants. Therefore, the removal process of NO3--N by Fe-Pd-Fe3O4/MWCNTs was studied, including rapid adsorption of initial pollutants, gradual reduction of intermediate products and re-adsorption of final products. The results showed that Fe-Pd-Fe3O4/MWCNTs completely removed NO3--N within 2 h, 39% and 25% of which were converted into NO2--N and NH4+-N. The adsorption efficiency, kinetics, capacity and adsorption energy all followed the order of NH4+-N > NO2--N > NO3--N. With the recoverability and reusability of Fe-Pd-Fe3O4/MWCNTs having been confirmed in 5 consecutive cycles, the removal rate of NO3--N still reached 43%. It has been shown that MWCNTs prolonged the reducing power for NO3--N, due to avoiding the aggregation of metal particles. The rapid adsorption of initial pollutants, effective stepwise reduction and convenient recovery processes were of great value for the rehabilitation of polluted water.
Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal particles on MWCNTs, the chemical reduction ability of adsorbed pollutants could be provided, so as to achieve the purpose of adsorption and degradation of pollutants. Therefore, the removal process of NO3−-N by Fe–Pd–Fe3O4/MWCNTs was studied, including rapid adsorption of initial pollutants, gradual reduction of intermediate products and re-adsorption of final products. The results showed that Fe–Pd–Fe3O4/MWCNTs completely removed NO3−-N within 2 h, 39% and 25% of which were converted into NO2−-N and NH4+-N. The adsorption efficiency, kinetics, capacity and adsorption energy all followed the order of NH4+-N > NO2−-N > NO3−-N. With the recoverability and reusability of Fe–Pd–Fe3O4/MWCNTs having been confirmed in 5 consecutive cycles, the removal rate of NO3−-N still reached 43%. It has been shown that MWCNTs prolonged the reducing power for NO3−-N, due to avoiding the aggregation of metal particles. The rapid adsorption of initial pollutants, effective stepwise reduction and convenient recovery processes were of great value for the rehabilitation of polluted water. [Display omitted] •50 mg/L Fe–Pd–Fe3O4/MWCNTs completely removed 100 mg/L NO3−-N within 2 h.•36% of adsorbed NO3−-N was converted into N2 or N2O.•The removal efficiency of NO3−-N reached 43% by Fe–Pd–Fe3O4/MWCNTs in 5 cycles.
ArticleNumber 130718
Author Dai, Luyao
Yao, Jiachao
Guo, Tianjiao
Hrynsphan, Dzmitry
Tatsiana, Savitskaya
Wang, Zeyu
Chen, Jun
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  surname: Wang
  fullname: Wang, Zeyu
  organization: Interdisciplinary Research Academy, Zhejiang Shuren University, Hangzhou, 310021, PR China
– sequence: 2
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  surname: Dai
  fullname: Dai, Luyao
  organization: College of Environment, Zhejiang University of Technology, Hangzhou, 310032, PR China
– sequence: 3
  givenname: Jiachao
  surname: Yao
  fullname: Yao, Jiachao
  organization: College of Biological and Environmental Engineering, Zhejiang Shuren University, Hangzhou, 310021, PR China
– sequence: 4
  givenname: Tianjiao
  surname: Guo
  fullname: Guo, Tianjiao
  organization: College of Biological and Environmental Engineering, Zhejiang Shuren University, Hangzhou, 310021, PR China
– sequence: 5
  givenname: Dzmitry
  surname: Hrynsphan
  fullname: Hrynsphan, Dzmitry
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  fullname: Tatsiana, Savitskaya
  organization: Research Institute of Physical and Chemical Problems, Belarusian State University, Minsk, 220030, Belarus
– sequence: 7
  givenname: Jun
  surname: Chen
  fullname: Chen, Jun
  email: bec@zjut.edu.cn
  organization: College of Biological and Environmental Engineering, Zhejiang Shuren University, Hangzhou, 310021, PR China
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IsPeerReviewed true
IsScholarly true
Keywords Reduction
NO3−-N
Adsorption
Recovery
Fe–Pd–Fe3O4/MWCNTs
Language English
LinkModel DirectLink
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PQPubID 23479
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crossref_citationtrail_10_1016_j_chemosphere_2021_130718
crossref_primary_10_1016_j_chemosphere_2021_130718
elsevier_sciencedirect_doi_10_1016_j_chemosphere_2021_130718
PublicationCentury 2000
PublicationDate October 2021
2021-10-00
20211001
PublicationDateYYYYMMDD 2021-10-01
PublicationDate_xml – month: 10
  year: 2021
  text: October 2021
PublicationDecade 2020
PublicationTitle Chemosphere (Oxford)
PublicationYear 2021
Publisher Elsevier Ltd
Publisher_xml – name: Elsevier Ltd
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Snippet Multi walled carbon nanotubes (MWCNTs) have attracted more and more attention as adsorbents due to their excellent adsorption properties. By loading metal...
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SubjectTerms adsorbents
Adsorption
carbon nanotubes
chemical reduction
energy
Fe–Pd–Fe3O4/MWCNTs
nitrates
NO3−-N
Recovery
Reduction
water pollution
Title Enhanced adsorption and reduction performance of nitrate by Fe–Pd–Fe3O4 embedded multi-walled carbon nanotubes
URI https://dx.doi.org/10.1016/j.chemosphere.2021.130718
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