Asymmetric and bi-continuously structured polyethersulfone (PES) membranes with superior water flux for ultrafiltration application
This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/γ-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using non-solvent induced phase separation (NIPS) process. Different amounts of PVP and PES are added into the environmentally friendly solvent, GB...
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| Published in | Journal of polymer research Vol. 29; no. 1 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Dordrecht
Springer Netherlands
01.01.2022
Springer Springer Nature B.V |
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| Abstract | This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/γ-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using non-solvent induced phase separation (NIPS) process. Different amounts of PVP and PES are added into the environmentally friendly solvent, GBL, to form the dope solutions and their effects on the morphological, physical, permeation, and filtration properties of formed membranes are systematically studied. The results demonstrate that the pore size on the top surface and the size of macrovoids in the bulk increase with increasing PVP content and decreasing PES amount in the dope. In the optimal conditions (PVP/PES ratio approaches 1, in particular), the macrovoids disappears and the pores evolve into three-dimensional pore networks in PES matrix. This unique bi-continuous membrane exhibits a remarkable water permeation flux of nearly 1000 L•m
−2
h
−1
and a BSA rejection of 91%. |
|---|---|
| AbstractList | This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/γ-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using non-solvent induced phase separation (NIPS) process. Different amounts of PVP and PES are added into the environmentally friendly solvent, GBL, to form the dope solutions and their effects on the morphological, physical, permeation, and filtration properties of formed membranes are systematically studied. The results demonstrate that the pore size on the top surface and the size of macrovoids in the bulk increase with increasing PVP content and decreasing PES amount in the dope. In the optimal conditions (PVP/PES ratio approaches 1, in particular), the macrovoids disappears and the pores evolve into three-dimensional pore networks in PES matrix. This unique bi-continuous membrane exhibits a remarkable water permeation flux of nearly 1000 L•m−2 h−1 and a BSA rejection of 91%. This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/γ-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using non-solvent induced phase separation (NIPS) process. Different amounts of PVP and PES are added into the environmentally friendly solvent, GBL, to form the dope solutions and their effects on the morphological, physical, permeation, and filtration properties of formed membranes are systematically studied. The results demonstrate that the pore size on the top surface and the size of macrovoids in the bulk increase with increasing PVP content and decreasing PES amount in the dope. In the optimal conditions (PVP/PES ratio approaches 1, in particular), the macrovoids disappears and the pores evolve into three-dimensional pore networks in PES matrix. This unique bi-continuous membrane exhibits a remarkable water permeation flux of nearly 1000 L•m −2 h −1 and a BSA rejection of 91%. This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/[gamma]-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using non-solvent induced phase separation (NIPS) process. Different amounts of PVP and PES are added into the environmentally friendly solvent, GBL, to form the dope solutions and their effects on the morphological, physical, permeation, and filtration properties of formed membranes are systematically studied. The results demonstrate that the pore size on the top surface and the size of macrovoids in the bulk increase with increasing PVP content and decreasing PES amount in the dope. In the optimal conditions (PVP/PES ratio approaches 1, in particular), the macrovoids disappears and the pores evolve into three-dimensional pore networks in PES matrix. This unique bi-continuous membrane exhibits a remarkable water permeation flux of nearly 1000 L*m.sup.-2 h.sup.-1 and a BSA rejection of 91%. |
| ArticleNumber | 23 |
| Audience | Academic |
| Author | Chang, Chao-Ching Cheng, Liao-Ping Yu, Szu-Ting Su, Jenn Fang |
| Author_xml | – sequence: 1 givenname: Chao-Ching surname: Chang fullname: Chang, Chao-Ching organization: Department of Chemical and Materials Engineering, Tamkang University, Energy and Opto-Electronic Materials Research Center, Tamkang University – sequence: 2 givenname: Szu-Ting surname: Yu fullname: Yu, Szu-Ting organization: Department of Chemical and Materials Engineering, Tamkang University – sequence: 3 givenname: Jenn Fang orcidid: 0000-0002-8935-1151 surname: Su fullname: Su, Jenn Fang email: jennfangsu@mail.tku.edu.tw organization: Department of Chemical and Materials Engineering, Tamkang University, Energy and Opto-Electronic Materials Research Center, Tamkang University – sequence: 4 givenname: Liao-Ping surname: Cheng fullname: Cheng, Liao-Ping organization: Department of Chemical and Materials Engineering, Tamkang University, Energy and Opto-Electronic Materials Research Center, Tamkang University |
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| Keywords | Polyethersulfone Membrane Ultrafiltration Water permeation flux Nonsolvent induced phase separation Asymmetric bi-continuous structure |
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| Snippet | This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/γ-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system using... This work reports a fabrication of asymmetric polyethersulfone (PES) membranes from the water/[gamma]-butyllactone (GBL)/polyvinylpyrrolidone (PVP)/PES system... |
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| SubjectTerms | Asymmetry Characterization and Evaluation of Materials Chemistry Chemistry and Materials Science Industrial Chemistry/Chemical Engineering Membranes Original Paper Penetration Phase separation Polyethersulfones Polymer Sciences Polyvinylpyrrolidone Pore size Povidone Solvents Ultrafiltration Water |
| Title | Asymmetric and bi-continuously structured polyethersulfone (PES) membranes with superior water flux for ultrafiltration application |
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