Structural evolution, sintering behavior and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9)
Sintering behavior, microstructure and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9) ceramics have been studied in this paper. Continuous solid solution with rock salt structure formed across the entire compositional range. Phase transformed from ordered body-centered cubic phase to...
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| Published in | Journal of the European Ceramic Society Vol. 32; no. 6; pp. 1251 - 1259 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.06.2012
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| Abstract | Sintering behavior, microstructure and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9) ceramics have been studied in this paper. Continuous solid solution with rock salt structure formed across the entire compositional range. Phase transformed from ordered body-centered cubic phase to short range ordered face-centered cubic phase with the addition of LiF. The x>0.4 compositions could be densified at 850°C/2h. The optimized Q×f value for each composition increased with the increase of LiF content and saturated at about 75,000GHz when x≥0.15, whereas the optimized dielectric permittivity decreased with the increase of LiF content. All specimens exhibited negative τf value. The chemical compatibilities with copper (Cu) in the case of x=0.4 composition and silver (Ag) in the case of x=0.5 composition were also investigated, respectively. No chemical reaction has taken place between the matrix phase and Ag or Cu after sintering at 850°C/2h or 950°C/2h, respectively. |
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| AbstractList | The sintering behaviour, microstructure and microwave dielectric properties of (1-x)Li3NbO4-xLiF (x = 0-0.9) ceramics were studied. A continuous solid solution with a rock salt structure formed across the entire compositional range. The phase transformed from an ordered body-centred cubic phase to short range ordered face-centred cubic phase with the addition of LiF. The x > 0.4 compositions could be densified at 850 C/2 h. The optimised Qxf value for each composition increased with increasing LiF content and saturated at about 75000 GHz when x was at least 0.15, whereas the optimised dielectric permittivity decreased with increasing LiF content. All the specimens had negative tauf values. The chemical compatibility with Cu in the case of the x = 0.4 composition and Ag in the case of the x = 0.5 composition were also investigated, respectively. No chemical reaction took place between the matrix phase and Ag or Cu after sintering at 850 C/2 h or 950 C/2 h, respectively. Sintering behavior, microstructure and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9) ceramics have been studied in this paper. Continuous solid solution with rock salt structure formed across the entire compositional range. Phase transformed from ordered body-centered cubic phase to short range ordered face-centered cubic phase with the addition of LiF. The x>0.4 compositions could be densified at 850°C/2h. The optimized Q×f value for each composition increased with the increase of LiF content and saturated at about 75,000GHz when x≥0.15, whereas the optimized dielectric permittivity decreased with the increase of LiF content. All specimens exhibited negative τf value. The chemical compatibilities with copper (Cu) in the case of x=0.4 composition and silver (Ag) in the case of x=0.5 composition were also investigated, respectively. No chemical reaction has taken place between the matrix phase and Ag or Cu after sintering at 850°C/2h or 950°C/2h, respectively. |
| Author | Wu, J.Y. Bian, J.J. Wang, L. |
| Author_xml | – sequence: 1 givenname: J.J. surname: Bian fullname: Bian, J.J. email: jjbian@shu.edu.cn – sequence: 2 givenname: J.Y. surname: Wu fullname: Wu, J.Y. – sequence: 3 givenname: L. surname: Wang fullname: Wang, L. |
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| Snippet | Sintering behavior, microstructure and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9) ceramics have been studied in this paper. Continuous... The sintering behaviour, microstructure and microwave dielectric properties of (1-x)Li3NbO4-xLiF (x = 0-0.9) ceramics were studied. A continuous solid solution... |
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| SubjectTerms | Ceramics Copper Dielectric properties LTCC Microwaves Phase transformations Silver Sintering Solid solutions |
| Title | Structural evolution, sintering behavior and microwave dielectric properties of (1−x)Li3NbO4–xLiF (0≤x≤0.9) |
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