Influence of palladium on gas-sensing performance of magnesium ferrite nanoparticles
Commercial ferrites with high densities are mostly used in the electromagnetic devices, which require high temperature synthesis. In this article the gas-sensing characteristics of pure and Pd-doped MgFe 2O 4 powder has been discussed. The synthesis has been carried out by using a simple molten salt...
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| Published in | Materials chemistry and physics Vol. 119; no. 1; pp. 319 - 323 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
15.01.2010
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| Abstract | Commercial ferrites with high densities are mostly used in the electromagnetic devices, which require high temperature synthesis. In this article the gas-sensing characteristics of pure and Pd-doped MgFe
2O
4 powder has been discussed. The synthesis has been carried out by using a simple molten salt method. This method facilitates rapid synthesis at comparatively lower temperature enabling formation of nanostructures, suitable for the gas-sensing application. Various physicochemical techniques have been used for the characterization of samples. X-ray diffraction analysis confirmed the single-phase formation of pure and Pd-doped MgFe
2O
4 having crystallite size 15–20
nm. Pure MgFe
2O
4 showed highest responses towards liquid petroleum gas (LPG) at 350
°C while, on doping with Pd the highest response shifted towards lower operating temperature of ∼200
°C. Pure MgFe
2O
4 exhibited some response towards 200
ppm of LPG which markedly increased on doping of palladium (Pd). The probable mechanism is proposed to explain the selective response towards LPG. |
|---|---|
| AbstractList | The gas-sensing characteristics of pure and Pd-doped MgFe2O4 powders are discussed. The synthesis was carried out using a simple molten salt method. This method facilitated rapid synthesis at comparatively lower temperature, enabling the formation of nanostructures, suitable for gas-sensing applications. XRD analysis confirmed the single-phase formation of pure and Pd-doped MgFe2O4 with a crystallite size of 15-20 nm. Pure MgFe2O4 showed the highest response towards liquid petroleum gas (LPG) at 350 C while, after doping with Pd, the highest response shifted towards a lower operating temperature of about 200 C. Pure MgFe2O4 exhibited some response towards 200 ppm of LPG which increased markedly on doping with Pd. The probable mechanism is proposed to explain the selective response towards LPG. Commercial ferrites with high densities are mostly used in the electromagnetic devices, which require high temperature synthesis. In this article the gas-sensing characteristics of pure and Pd-doped MgFe 2O 4 powder has been discussed. The synthesis has been carried out by using a simple molten salt method. This method facilitates rapid synthesis at comparatively lower temperature enabling formation of nanostructures, suitable for the gas-sensing application. Various physicochemical techniques have been used for the characterization of samples. X-ray diffraction analysis confirmed the single-phase formation of pure and Pd-doped MgFe 2O 4 having crystallite size 15–20 nm. Pure MgFe 2O 4 showed highest responses towards liquid petroleum gas (LPG) at 350 °C while, on doping with Pd the highest response shifted towards lower operating temperature of ∼200 °C. Pure MgFe 2O 4 exhibited some response towards 200 ppm of LPG which markedly increased on doping of palladium (Pd). The probable mechanism is proposed to explain the selective response towards LPG. Commercial ferrites with high densities are mostly used in the electromagnetic devices, which require high temperature synthesis. In this article the gas-sensing characteristics of pure and Pd-doped MgFe(2)O(4) powder has been discussed. The synthesis has been carried out by using a simple molten salt method. This method facilitates rapid synthesis at comparatively lower temperature enabling formation of nanostructures, suitable for the gas-sensing application. Various physicochemical techniques have been used for the characterization of samples. X-ray diffraction analysis confirmed the single-phase formation of pure and Pd-doped MgFe(2)O(4) having crystallite size 15-20nm. Pure MgFe(2)O(4) showed highest responses towards liquid petroleum gas (LPG) at 350(o)C while, on doping with Pd the highest response shifted towards lower operating temperature of ~200(o)C. Pure MgFe(2)O(4) exhibited some response towards 200ppm of LPG which markedly increased on doping of palladium (Pd). The probable mechanism is proposed to explain the selective response towards LPG. |
| Author | Darshane, Sonali Mulla, I.S. |
| Author_xml | – sequence: 1 givenname: Sonali surname: Darshane fullname: Darshane, Sonali organization: Department of Physics, Solapur University, Solapur 413255, India – sequence: 2 givenname: I.S. surname: Mulla fullname: Mulla, I.S. email: is.mulla@ncl.res.in organization: National Chemical Laboratory, Pune 411008, India |
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| Snippet | Commercial ferrites with high densities are mostly used in the electromagnetic devices, which require high temperature synthesis. In this article the... The gas-sensing characteristics of pure and Pd-doped MgFe2O4 powders are discussed. The synthesis was carried out using a simple molten salt method. This... |
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| SubjectTerms | Doping Ferrite Liquids LPG LPG sensor Molten salt synthesis Nanocomposites Nanostructure Nanostructures Operating temperature Palladium Synthesis |
| Title | Influence of palladium on gas-sensing performance of magnesium ferrite nanoparticles |
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