Heterogeneous Suzuki cross-coupling reactions over palladium/hydrotalcite catalysts
The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100...
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| Published in | Journal of colloid and interface science Vol. 302; no. 2; pp. 568 - 575 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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San Diego, CA
Elsevier Inc
15.10.2006
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| Abstract | The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100% selectivity at moderate temperatures in the presence of some of the catalysts. The best results were provided by a catalyst consisting of an acetate–pyridine complex of Pd supported on hydrotalcite that gave high conversion values even after three reuses. The reactions conditions were very mild (a temperature of 55 °C and atmospheric pressure). In fact, the catalyst provided conversion and selectivity results surpassing those of existing heterogeneous phase catalysts and most homogeneous phase catalysts for the same purpose. |
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| AbstractList | The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100% selectivity at moderate temperatures in the presence of some of the catalysts. The best results were provided by a catalyst consisting of an acetate-pyridine complex of Pd supported on hydrotalcite that gave high conversion values even after three reuses. The reactions conditions were very mild (a temperature of 55 degrees C and atmospheric pressure). In fact, the catalyst provided conversion and selectivity results surpassing those of existing heterogeneous phase catalysts and most homogeneous phase catalysts for the same purpose.The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100% selectivity at moderate temperatures in the presence of some of the catalysts. The best results were provided by a catalyst consisting of an acetate-pyridine complex of Pd supported on hydrotalcite that gave high conversion values even after three reuses. The reactions conditions were very mild (a temperature of 55 degrees C and atmospheric pressure). In fact, the catalyst provided conversion and selectivity results surpassing those of existing heterogeneous phase catalysts and most homogeneous phase catalysts for the same purpose. The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100% selectivity at moderate temperatures in the presence of some of the catalysts. The best results were provided by a catalyst consisting of an acetate–pyridine complex of Pd supported on hydrotalcite that gave high conversion values even after three reuses. The reactions conditions were very mild (a temperature of 55 °C and atmospheric pressure). In fact, the catalyst provided conversion and selectivity results surpassing those of existing heterogeneous phase catalysts and most homogeneous phase catalysts for the same purpose. The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between bromobenzene and phenylboronic acid was studied. Based on the catalytic activity results, the reaction develops to an acceptable extent with 100% selectivity at moderate temperatures in the presence of some of the catalysts. The best results were provided by a catalyst consisting of an acetate-pyridine complex of Pd supported on hydrotalcite that gave high conversion values even after three reuses. The reactions conditions were very mild (a temperature of 55 degrees C and atmospheric pressure). In fact, the catalyst provided conversion and selectivity results surpassing those of existing heterogeneous phase catalysts and most homogeneous phase catalysts for the same purpose. |
| Author | Jiménez-Sanchidrián, César Mora, Manuel Ruiz, J. Rafael |
| Author_xml | – sequence: 1 givenname: Manuel surname: Mora fullname: Mora, Manuel – sequence: 2 givenname: César surname: Jiménez-Sanchidrián fullname: Jiménez-Sanchidrián, César – sequence: 3 givenname: J. Rafael surname: Ruiz fullname: Ruiz, J. Rafael email: qo1ruarj@uco.es |
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| Keywords | Phenylboronic acid Bromobenzene Hydrotalcite Palladium catalyst Suzuki cross-coupling reaction Acids Transition metal Palladium Platinoid Catalyst |
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| Snippet | The efficiency of various heterogeneous solids consisting of palladium supported on hydrotalcite as catalysts in the Suzuki cross-coupling reaction between... |
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| SubjectTerms | Adsorption Aluminum Hydroxide - chemistry Biphenyl Compounds - chemical synthesis Biphenyl Compounds - chemistry Boronic Acids - chemistry Bromobenzene Bromobenzenes - chemistry Catalysis Chemistry Exact sciences and technology General and physical chemistry Hydrotalcite Magnesium Hydroxide - chemistry Magnetic Resonance Spectroscopy - methods Molecular Structure Organometallic Compounds - chemical synthesis Organometallic Compounds - chemistry Palladium - chemistry Palladium catalyst Particle Size Phenylboronic acid Sensitivity and Specificity Solvents - chemistry Spectrophotometry, Infrared - methods Surface Properties Suzuki cross-coupling reaction Temperature Theory of reactions, general kinetics. Catalysis. Nomenclature, chemical documentation, computer chemistry |
| Title | Heterogeneous Suzuki cross-coupling reactions over palladium/hydrotalcite catalysts |
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