Synthesis and Characterization of Graphene Oxide (GO) and Reduced Graphene Oxide (rGO) for Gas Sensing Application
In the present investigation, GO was prepared by exfoliation of graphite using modified Hummer's method and then reduced using hydrazine hydrate (reducing agent) to produce rGO. XRD, FESEM, Raman, FTIR spectrophotometer and TGA were used for characterization of GO and rGO. XRD images reveal cry...
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| Published in | Macromolecular symposia. Vol. 376; no. 1 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
Wiley Subscription Services, Inc
01.12.2017
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| Subjects | |
| Online Access | Get full text |
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| Abstract | In the present investigation, GO was prepared by exfoliation of graphite using modified Hummer's method and then reduced using hydrazine hydrate (reducing agent) to produce rGO. XRD, FESEM, Raman, FTIR spectrophotometer and TGA were used for characterization of GO and rGO. XRD images reveal crystalline structure for both GO and rGO. The d‐spacing is observed to be reduced for rGO as compared to that for GO because of removal of oxygen containing functional groups. Raman excitation peaks were obtained for two laser wavelengths 532 and 785 nm. Ratio of intensities of D and G bands (ID/IG) increase for rGO due to increase in order by reduction, implying restoration of the p‐conjugation. The bands are narrower for rGO.TGA thermograms show a higher overall loss of weight for GO in the temperature range 0–1000 °C under N2 flow. Intensity of FTIR peaks of oxide, hydroxyl and alkoxy groups decreases significantly on reduction. FESEM image shows more corrugated surface of rGO as compared to GO. It is expected that this investigation would be useful to develop GO/rGO based gas sensors to detect minute concentration of gases. |
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| AbstractList | In the present investigation, GO was prepared by exfoliation of graphite using modified Hummer's method and then reduced using hydrazine hydrate (reducing agent) to produce rGO. XRD, FESEM, Raman, FTIR spectrophotometer and TGA were used for characterization of GO and rGO. XRD images reveal crystalline structure for both GO and rGO. The d-spacing is observed to be reduced for rGO as compared to that for GO because of removal of oxygen containing functional groups. Raman excitation peaks were obtained for two laser wavelengths 532 and 785nm. Ratio of intensities of D and G bands (ID/IG) increase for rGO due to increase in order by reduction, implying restoration of the p-conjugation. The bands are narrower for rGO.TGA thermograms show a higher overall loss of weight for GO in the temperature range 0-1000°C under N2 flow. Intensity of FTIR peaks of oxide, hydroxyl and alkoxy groups decreases significantly on reduction. FESEM image shows more corrugated surface of rGO as compared to GO. It is expected that this investigation would be useful to develop GO/rGO based gas sensors to detect minute concentration of gases. In the present investigation, GO was prepared by exfoliation of graphite using modified Hummer's method and then reduced using hydrazine hydrate (reducing agent) to produce rGO. XRD, FESEM, Raman, FTIR spectrophotometer and TGA were used for characterization of GO and rGO. XRD images reveal crystalline structure for both GO and rGO. The d‐spacing is observed to be reduced for rGO as compared to that for GO because of removal of oxygen containing functional groups. Raman excitation peaks were obtained for two laser wavelengths 532 and 785 nm. Ratio of intensities of D and G bands (ID/IG) increase for rGO due to increase in order by reduction, implying restoration of the p‐conjugation. The bands are narrower for rGO.TGA thermograms show a higher overall loss of weight for GO in the temperature range 0–1000 °C under N2 flow. Intensity of FTIR peaks of oxide, hydroxyl and alkoxy groups decreases significantly on reduction. FESEM image shows more corrugated surface of rGO as compared to GO. It is expected that this investigation would be useful to develop GO/rGO based gas sensors to detect minute concentration of gases. |
| Author | Sharma, S. K. Gupta, Ragini Sharma, Neeru Kumari, Mitlesh Sharma, Vikas Jain, Yachana Sachdev, K. |
| Author_xml | – sequence: 1 givenname: Neeru surname: Sharma fullname: Sharma, Neeru email: neerupathak93@gmail.com organization: Department of Physics, Malaviya National Institute of Technology – sequence: 2 givenname: Vikas surname: Sharma fullname: Sharma, Vikas organization: Department of Physics, Malaviya National Institute of Technology – sequence: 3 givenname: Yachana surname: Jain fullname: Jain, Yachana organization: Department of Chemistry, Malaviya National Institute of Technology – sequence: 4 givenname: Mitlesh surname: Kumari fullname: Kumari, Mitlesh organization: Department of Chemistry, Malaviya National Institute of Technology – sequence: 5 givenname: Ragini surname: Gupta fullname: Gupta, Ragini organization: Material Research Center, Malaviya National Institute of Technology – sequence: 6 givenname: S. K. surname: Sharma fullname: Sharma, S. K. organization: Department of Physics, Malaviya National Institute of Technology – sequence: 7 givenname: K. surname: Sachdev fullname: Sachdev, K. organization: Material Research Center, Malaviya National Institute of Technology |
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| SubjectTerms | Conjugation FTIR Functional groups Gas sensors Gases Graphene graphene oxide (GO) Hydrazine Immunoglobulins reduced graphene oxide (rGO) Reduction Restoration surface characterization and exfoliation |
| Title | Synthesis and Characterization of Graphene Oxide (GO) and Reduced Graphene Oxide (rGO) for Gas Sensing Application |
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