Ibuprofen-Based Ionic Liquids as Additives for Enhancing the Lubricity and Antiwear of Water–Ethylene Glycol Liquid

Ibuprofen-based (L-Ibu) halogen-free ionic liquids (ILs) were synthesized and evaluated as water-based lubricant additive. In contrast to the conventional ILs with fluoro-containing anions, the present L-Ibu ILs have no corrosive attack to steel and cast iron even in the water environment and exhibi...

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Published in	Tribology letters Vol. 65; no. 2; pp. 1 - 13
Main Authors	Wang, Yurong, Yu, Qiangliang, Cai, Meirong, Shi, Lei, Zhou, Feng, Liu, Weimin
Format	Journal Article
Language	English
Published	New York Springer US 01.06.2017 Springer Nature B.V
Subjects	Additives Cast iron Chemistry and Materials Science Contact resistance Corrosion and Coatings Electric contacts Ethylene glycol Friction reduction Hydraulic fluids Ibuprofen Ionic liquids Ions Lubricants Lubricants & lubrication Lubrication Lubricity Materials Science Microbalances Nanotechnology Nonsteroidal anti-inflammatory drugs Original Paper Photoelectrons Physical Chemistry Protective coatings Quartz crystals Surfaces and Interfaces Theoretical and Applied Mechanics Thin Films Tribology Ionic liquids Aqueous lubrication Additives Antiwear
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Abstract	Ibuprofen-based (L-Ibu) halogen-free ionic liquids (ILs) were synthesized and evaluated as water-based lubricant additive. In contrast to the conventional ILs with fluoro-containing anions, the present L-Ibu ILs have no corrosive attack to steel and cast iron even in the water environment and exhibit extremely stable hydrolytic stability in water–ethylene glycol (W–EG) system. In addition, the Ibuprofen ILs as the water-based lubricant additives have better friction-reducing, extreme-pressure and antiwear properties than a commercial antiwear water-based lubricant additive of Hostagliss L4. The mechanism for excellent lubricating characteristics is investigated by combining electrical contact resistance measurement, X-ray photoelectron spectroscopy and interfacial adsorption behaviour by quartz crystal microbalance. The results indicate that a formed protective film on the contact surface prevents the direct contact of sliding pairs and contributes to the friction reduction and antiwear properties. More importantly, the prepared ILs provide a comparatively green alternative to the traditional halogenated ILs for the water-based lubrication application owing to halogen-, sulphur-, and phosphorus-free. So, these ILs are expected to develop into a highly efficient lubricant additive applied in water-based hydraulic fluids. Graphical Abstract
AbstractList	Ibuprofen-based (L-Ibu) halogen-free ionic liquids (ILs) were synthesized and evaluated as water-based lubricant additive. In contrast to the conventional ILs with fluoro-containing anions, the present L-Ibu ILs have no corrosive attack to steel and cast iron even in the water environment and exhibit extremely stable hydrolytic stability in water–ethylene glycol (W–EG) system. In addition, the Ibuprofen ILs as the water-based lubricant additives have better friction-reducing, extreme-pressure and antiwear properties than a commercial antiwear water-based lubricant additive of Hostagliss L4. The mechanism for excellent lubricating characteristics is investigated by combining electrical contact resistance measurement, X-ray photoelectron spectroscopy and interfacial adsorption behaviour by quartz crystal microbalance. The results indicate that a formed protective film on the contact surface prevents the direct contact of sliding pairs and contributes to the friction reduction and antiwear properties. More importantly, the prepared ILs provide a comparatively green alternative to the traditional halogenated ILs for the water-based lubrication application owing to halogen-, sulphur-, and phosphorus-free. So, these ILs are expected to develop into a highly efficient lubricant additive applied in water-based hydraulic fluids. Graphical Abstract Ibuprofen-based (L-Ibu) halogen-free ionic liquids (ILs) were synthesized and evaluated as water-based lubricant additive. In contrast to the conventional ILs with fluoro-containing anions, the present L-Ibu ILs have no corrosive attack to steel and cast iron even in the water environment and exhibit extremely stable hydrolytic stability in water–ethylene glycol (W–EG) system. In addition, the Ibuprofen ILs as the water-based lubricant additives have better friction-reducing, extreme-pressure and antiwear properties than a commercial antiwear water-based lubricant additive of Hostagliss L4. The mechanism for excellent lubricating characteristics is investigated by combining electrical contact resistance measurement, X-ray photoelectron spectroscopy and interfacial adsorption behaviour by quartz crystal microbalance. The results indicate that a formed protective film on the contact surface prevents the direct contact of sliding pairs and contributes to the friction reduction and antiwear properties. More importantly, the prepared ILs provide a comparatively green alternative to the traditional halogenated ILs for the water-based lubrication application owing to halogen-, sulphur-, and phosphorus-free. So, these ILs are expected to develop into a highly efficient lubricant additive applied in water-based hydraulic fluids.Graphical Abstract
ArticleNumber	55
Author	Shi, Lei Zhou, Feng Yu, Qiangliang Cai, Meirong Wang, Yurong Liu, Weimin
Author_xml	– sequence: 1 givenname: Yurong surname: Wang fullname: Wang, Yurong organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences, University of Chinese Academy of Sciences – sequence: 2 givenname: Qiangliang surname: Yu fullname: Yu, Qiangliang organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 3 givenname: Meirong surname: Cai fullname: Cai, Meirong email: caimr@licp.cas.cn organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 4 givenname: Lei surname: Shi fullname: Shi, Lei organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 5 givenname: Feng surname: Zhou fullname: Zhou, Feng email: zhouf@licp.cas.cn organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences – sequence: 6 givenname: Weimin surname: Liu fullname: Liu, Weimin organization: State Key Laboratory of Solid Lubrication, Lanzhou Institute of Chemical Physics, Chinese Academy of Sciences
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Snippet	Ibuprofen-based (L-Ibu) halogen-free ionic liquids (ILs) were synthesized and evaluated as water-based lubricant additive. In contrast to the conventional ILs...
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SubjectTerms	Additives Cast iron Chemistry and Materials Science Contact resistance Corrosion and Coatings Electric contacts Ethylene glycol Friction reduction Hydraulic fluids Ibuprofen Ionic liquids Ions Lubricants Lubricants & lubrication Lubrication Lubricity Materials Science Microbalances Nanotechnology Nonsteroidal anti-inflammatory drugs Original Paper Photoelectrons Physical Chemistry Protective coatings Quartz crystals Surfaces and Interfaces Theoretical and Applied Mechanics Thin Films Tribology
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Title	Ibuprofen-Based Ionic Liquids as Additives for Enhancing the Lubricity and Antiwear of Water–Ethylene Glycol Liquid
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