Effective removal of phenol from wastewater by magnetic porous loofah biochar
In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe 3 O 4 . The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In additi...
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| Published in | Carbon Letters Vol. 34; no. 1; pp. 191 - 200 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Singapore
Springer Nature Singapore
01.01.2024
한국탄소학회 Springer Nature B.V |
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| Online Access | Get full text |
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| Abstract | In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe
3
O
4
. The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In addition, the material exhibits outstanding magnetic separation performance (40.01 umg/g) allowing for rapid recovery within just 90 s. The adsorption process of phenol on MPLB was found to be spontaneous and endothermic. The experimental data fit exceptionally well with the pseudo-second-order kinetic model and Langmuir model (
R
2
> 0.99), indicating that the dominant adsorption mechanisms involved monolayer adsorption and chemisorption. These interactions were attributed to host–guest interaction, π–π conjugation, hydrogen bonding, and pore filling. The maximum adsorption capacity calculated using the Langmuir model at 298 K is 39.4 mg/g. Importantly, even after undergoing seven cycles of recycling, MPLB retained 78% of its initial adsorption capacity. In simulated experiments employing MPLB for phenol removal in actual wastewater, an impressive removal rate of 96.4% was achieved. In conclusion, MPLB exhibits significant potential as an effective adsorbent for phenol removal in wastewater.
Graphical abstract |
|---|---|
| AbstractList | In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe3O4. The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In addition, the material exhibits outstanding magnetic separation performance (40.01 umg/g) allowing for rapid recovery within just 90 s. The adsorption process of phenol on MPLB was found to be spontaneous and endothermic. The experimental data fit exceptionally well with the pseudo-second-order kinetic model and Langmuir model (R2 > 0.99), indicating that the dominant adsorption mechanisms involved monolayer adsorption and chemisorption. These interactions were attributed to host–guest interaction, π–π conjugation, hydrogen bonding, and pore filling. The maximum adsorption capacity calculated using the Langmuir model at 298 K is 39.4 mg/g. Importantly, even after undergoing seven cycles of recycling, MPLB retained 78% of its initial adsorption capacity. In simulated experiments employing MPLB for phenol removal in actual wastewater, an impressive removal rate of 96.4% was achieved. In conclusion, MPLB exhibits significant potential as an effective adsorbent for phenol removal in wastewater.
Graphical In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe3O4. The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In addition, the material exhibits outstanding magnetic separation performance (40.01 umg/g) allowing for rapid recovery within just 90 s. The adsorption process of phenol on MPLB was found to be spontaneous and endothermic. The experimental data fit exceptionally well with the pseudo-second-order kinetic model and Langmuir model (R2 > 0.99), indicating that the dominant adsorption mechanisms involved monolayer adsorption and chemisorption. These interactions were attributed to host–guest interaction, π–π conjugation, hydrogen bonding, and pore filling. The maximum adsorption capacity calculated using the Langmuir model at 298 K is 39.4 mg/g. Importantly, even after undergoing seven cycles of recycling, MPLB retained 78% of its initial adsorption capacity. In simulated experiments employing MPLB for phenol removal in actual wastewater, an impressive removal rate of 96.4% was achieved. In conclusion, MPLB exhibits significant potential as an effective adsorbent for phenol removal in wastewater.
Graphical KCI Citation Count: 0 In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe 3 O 4 . The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In addition, the material exhibits outstanding magnetic separation performance (40.01 umg/g) allowing for rapid recovery within just 90 s. The adsorption process of phenol on MPLB was found to be spontaneous and endothermic. The experimental data fit exceptionally well with the pseudo-second-order kinetic model and Langmuir model ( R 2 > 0.99), indicating that the dominant adsorption mechanisms involved monolayer adsorption and chemisorption. These interactions were attributed to host–guest interaction, π–π conjugation, hydrogen bonding, and pore filling. The maximum adsorption capacity calculated using the Langmuir model at 298 K is 39.4 mg/g. Importantly, even after undergoing seven cycles of recycling, MPLB retained 78% of its initial adsorption capacity. In simulated experiments employing MPLB for phenol removal in actual wastewater, an impressive removal rate of 96.4% was achieved. In conclusion, MPLB exhibits significant potential as an effective adsorbent for phenol removal in wastewater. Graphical abstract In this study, a low-cost and easily recyclable porous green adsorbent (magnetic porous loofah biochar, MPLB) was synthesized by modifying the almost zero-cost loofah biochar material with Fe3O4. The successful synthesis of the material was demonstrated by XRD, FTIR, SEM, VSM, and BET. In addition, the material exhibits outstanding magnetic separation performance (40.01 umg/g) allowing for rapid recovery within just 90 s. The adsorption process of phenol on MPLB was found to be spontaneous and endothermic. The experimental data fit exceptionally well with the pseudo-second-order kinetic model and Langmuir model (R2 > 0.99), indicating that the dominant adsorption mechanisms involved monolayer adsorption and chemisorption. These interactions were attributed to host–guest interaction, π–π conjugation, hydrogen bonding, and pore filling. The maximum adsorption capacity calculated using the Langmuir model at 298 K is 39.4 mg/g. Importantly, even after undergoing seven cycles of recycling, MPLB retained 78% of its initial adsorption capacity. In simulated experiments employing MPLB for phenol removal in actual wastewater, an impressive removal rate of 96.4% was achieved. In conclusion, MPLB exhibits significant potential as an effective adsorbent for phenol removal in wastewater. |
| Author | Huang, Mengqin Jiao, Di Wu, Honglin Li, Fu Yang, Jian Shan, Shirui |
| Author_xml | – sequence: 1 givenname: Shirui surname: Shan fullname: Shan, Shirui email: 15520596990@163.com organization: Department of Xuchang Vocational Technical College – sequence: 2 givenname: Honglin surname: Wu fullname: Wu, Honglin organization: Department of Guilin Institute of Information Technology – sequence: 3 givenname: Jian surname: Yang fullname: Yang, Jian organization: Guang’an District, Department of Jinghe Town Junior Middle School – sequence: 4 givenname: Di surname: Jiao fullname: Jiao, Di organization: Department of Tianjin Branch of CNPC Offshore Engineering Co., Ltd – sequence: 5 givenname: Mengqin surname: Huang fullname: Huang, Mengqin organization: Department of Chengdu – sequence: 6 givenname: Fu surname: Li fullname: Li, Fu organization: Department of Weihai Jiamei Chemical Co., Ltd |
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| CitedBy_id | crossref_primary_10_1016_j_jcis_2025_137391 crossref_primary_10_1007_s42823_024_00837_8 crossref_primary_10_1007_s42823_024_00766_6 crossref_primary_10_1016_j_jwpe_2025_107137 |
| Cites_doi | 10.1016/J.JARE.2014.06.001 10.1016/J.JHAZMAT.2013.11.058 10.1016/J.JALLCOM.2020.154942 10.1016/J.ECOENV.2018.12.043 10.1007/S13738-018-1457-1 10.1016/J.MEMSCI.2020.119043 10.1016/J.PSEP.2021.05.015 10.1007/S11164-023-04958-Z 10.1016/J.JECE.2021.106494 10.1021/ACS.EST.1C07457 10.1111/1556-4029.13106 10.1021/ES801297U 10.1016/J.MATLET.2018.06.117 10.3390/W14203203 10.1016/j.powtec.2017.04.021 10.1016/J.JECE.2020.103790 10.1016/J.SEPPUR.2021.119138 10.1007/S10967-021-07782-0 10.1016/J.CEP.2023.109313 10.1007/S42114-017-0004-3 10.1016/J.ENVPOL.2018.10.071 10.2139/ssrn.4401670 10.1016/j.jenvman.2019.109677 10.1016/j.envpol.2019.113822 |
| ContentType | Journal Article |
| Copyright | The Author(s), under exclusive licence to Korean Carbon Society 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
| Copyright_xml | – notice: The Author(s), under exclusive licence to Korean Carbon Society 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law. |
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| SubjectTerms | Adsorbents Adsorption Carbon Characterization and Evaluation of Materials Charcoal Chemisorption Chemistry and Materials Science Conjugation Experiments Fourier transforms Hydrogen bonding Iron oxides Magnetic separation Materials Engineering Materials Science Nanotechnology Original Article Phenols Wastewater Wastewater treatment 자연과학일반 |
| TableOfContents | Effective removal of phenol from wastewater by magnetic porous loofah biochar Abstract Graphical abstract 1 Introduction 2 Experiment 2.1 Reagents 2.2 Synthesis of MPLB 2.3 Adsorption experiment of phenol 2.4 Cycle experiment 2.5 Actual oily wastewater 2.6 Kinetics and isotherm models 2.7 characterization equipment 3 Results and discussion 3.1 Characterization 3.1.1 XRD 3.1.2 VSM and BET 3.1.3 FTIR 3.1.4 SEM 3.2 Effect of pH 3.3 Effect of adsorption time and temperature 3.4 Kinetic studies 3.5 Study on adsorption thermodynamics and adsorption isotherm 3.6 Reuse performance and performance research in actual oily wastewater 3.7 Discussion on adsorption mechanism 4 Conclusions Acknowledgements References |
| Title | Effective removal of phenol from wastewater by magnetic porous loofah biochar |
| URI | https://link.springer.com/article/10.1007/s42823-023-00662-5 http://db.koreascholar.com/Article/Detail/435049 https://www.proquest.com/docview/2933292332 https://www.kci.go.kr/kciportal/ci/sereArticleSearch/ciSereArtiView.kci?sereArticleSearchBean.artiId=ART003060045 |
| Volume | 34 |
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| ispartofPNX | Carbon Letters, 2024, 34(1), , pp.191-200 |
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