Facile Synthesis of Multi-Branched Gold Nanostructures through a TBAB-Assisted Route in Aqueous Solution and Their SERS Property
Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide （TBAB） as a capping agent is described. The reaction is carried out in a one-step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are...
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| Published in | Chinese journal of chemistry Vol. 29; no. 1; pp. 185 - 190 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
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Weinheim
WILEY-VCH Verlag
2011
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
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| Abstract | Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide （TBAB） as a capping agent is described. The reaction is carried out in a one-step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are synthesized in high yield. It is proposed that the relative weak adsorption capacity of TBAB leads to the incompletely covered gold surface and the growth of nanoparticles occurs on the uncovered gold surface, and therefore short branches appear consequently. Then positively charged TBAB layers on the gold surfaces prevent the branches from aggregating with each other which stimulates the branch growth. The prepared branched gold nanoparticles show efficient surface-enhanced Raman scattering （SERS） properties. Low temperature （4 ℃） is unfavorable to the formation of multi-branched gold nanostructures, and only thin small irregular plate-like nanoparticles are produced. The addition of SDS in TBAB aqueous solution results in forming SDS micelles at much lower concentration of SDS （0.4 mmol/L） as compared to that in pure water, and short branched gold nanoparticles are obtained in the SDS-TBAB system. |
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| AbstractList | Abstract
Facile synthesis of multi‐branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction is carried out in a one‐step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are synthesized in high yield. It is proposed that the relative weak adsorption capacity of TBAB leads to the incompletely covered gold surface and the growth of nanoparticles occurs on the uncovered gold surface, and therefore short branches appear consequently. Then positively charged TBAB layers on the gold surfaces prevent the branches from aggregating with each other which stimulates the branch growth. The prepared branched gold nanoparticles show efficient surface‐enhanced Raman scattering (SERS) properties. Low temperature (4°C) is unfavorable to the formation of multi‐branched gold nanostructures, and only thin small irregular plate‐like nanoparticles are produced. The addition of SDS in TBAB aqueous solution results in forming SDS micelles at much lower concentration of SDS (0.4 mmol/L) as compared to that in pure water, and short branched gold nanoparticles are obtained in the SDS‐TBAB system. Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction is carried out in a one-step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are synthesized in high yield. It is proposed that the relative weak adsorption capacity of TBAB leads to the incompletely covered gold surface and the growth of nanoparticles occurs on the uncovered gold surface, and therefore short branches appear consequently. Then positively charged TBAB layers on the gold surfaces prevent the branches from aggregating with each other which stimulates the branch growth. The prepared branched gold nanoparticles show efficient surface-enhanced Raman scattering (SERS) properties. Low temperature (4°C) is unfavorable to the formation of multi-branched gold nanostructures, and only thin small irregular plate-like nanoparticles are produced. The addition of SDS in TBAB aqueous solution results in forming SDS micelles at much lower concentration of SDS (0.4 mmol/L) as compared to that in pure water, and short branched gold nanoparticles are obtained in the SDS-TBAB system. Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide （TBAB） as a capping agent is described. The reaction is carried out in a one-step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are synthesized in high yield. It is proposed that the relative weak adsorption capacity of TBAB leads to the incompletely covered gold surface and the growth of nanoparticles occurs on the uncovered gold surface, and therefore short branches appear consequently. Then positively charged TBAB layers on the gold surfaces prevent the branches from aggregating with each other which stimulates the branch growth. The prepared branched gold nanoparticles show efficient surface-enhanced Raman scattering （SERS） properties. Low temperature （4 ℃） is unfavorable to the formation of multi-branched gold nanostructures, and only thin small irregular plate-like nanoparticles are produced. The addition of SDS in TBAB aqueous solution results in forming SDS micelles at much lower concentration of SDS （0.4 mmol/L） as compared to that in pure water, and short branched gold nanoparticles are obtained in the SDS-TBAB system. Facile synthesis of multi‐branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction is carried out in a one‐step process at mild temperature. Gold nanostructures with more than six sharp branches ranging from 70 to 130 nm in length are synthesized in high yield. It is proposed that the relative weak adsorption capacity of TBAB leads to the incompletely covered gold surface and the growth of nanoparticles occurs on the uncovered gold surface, and therefore short branches appear consequently. Then positively charged TBAB layers on the gold surfaces prevent the branches from aggregating with each other which stimulates the branch growth. The prepared branched gold nanoparticles show efficient surface‐enhanced Raman scattering (SERS) properties. Low temperature (4°C) is unfavorable to the formation of multi‐branched gold nanostructures, and only thin small irregular plate‐like nanoparticles are produced. The addition of SDS in TBAB aqueous solution results in forming SDS micelles at much lower concentration of SDS (0.4 mmol/L) as compared to that in pure water, and short branched gold nanoparticles are obtained in the SDS‐TBAB system. Multi‐branched gold nanoparticles with relatively long branches are synthesized in high yield (practically 100% of the particles have numerous branches) by using TBAB (1.4 mmol/L) as the capping agent in aqueous solutions at mild temperature. |
| Author | Li, Xiaonan Wu, Zhiyan Wu, Xinzhou Wang, Luyan Pei, Meishan Tao, Xutang |
| AuthorAffiliation | School of Chemistry and Chemical Engineering, University ofJinan, Shandong Provincial Key Laboratory of Fluorine Chemistry and Chemical Materials, Jinan, Shandong 250022, China State Key Laboratory of Crystal Materials, （Shandong University）, Jinan, Shandong 250100, China |
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| Snippet | Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide （TBAB） as a capping agent is described. The reaction is carried... Facile synthesis of multi‐branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction is carried... Abstract Facile synthesis of multi‐branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction... Facile synthesis of multi-branched gold nanostructures by using the tetrabutyl ammonium bromide (TBAB) as a capping agent is described. The reaction is carried... |
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| StartPage | 185 |
| SubjectTerms | gold multi-branched nanostructures SERS surface-enhanced Raman scattering TBAB tetrabutyl ammonium bromide 水溶液 简便合成 纳米结构材料 表面增强拉曼散射 辅助线 |
| Title | Facile Synthesis of Multi-Branched Gold Nanostructures through a TBAB-Assisted Route in Aqueous Solution and Their SERS Property |
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