High-pressure and high-temperature sintering of nanostructured bulk NiAl materials
Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0–5.0 GPa and 600–1500 °C, respectively). The sintered samples were characterized by x-ray diffraction, scanning electron microscope, density, and indentation hardness measurements. The results show that NiAl nanopart...
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| Published in | Journal of materials research Vol. 24; no. 6; pp. 2089 - 2096 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
New York, USA
Cambridge University Press
01.06.2009
Springer International Publishing |
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| Abstract | Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0–5.0 GPa and 600–1500 °C, respectively). The sintered samples were characterized by x-ray diffraction, scanning electron microscope, density, and indentation hardness measurements. The results show that NiAl nanoparticles may have a compressed surface shell, which may be the reason why NiAl nanomaterials were difficult to densify sintering using conventional methods and why high-pressure sintering was an effective approach. We also observed that B2-structured NiAl could undergo a temperature-dependent phase transition and could be transformed into Al0.9Ni4.22 below 1000 °C for the first time. It is interesting to note that Vickers hardness decreased as grain size decreased below ∼30 nm, indicating that the inverse Hall-Petch effect may be observed in nano-polycrystalline NiAl (n-NiAl) samples. Moreover, a tentative interpretation was developed for high-pressure nanosintering, based on the shell-core model of nanoparticles. |
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| AbstractList | Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0-5.0 GPa and 600-1500 deg C, respectively). The sintered samples were characterized by x-ray diffraction, scanning electron microscope, density, and indentation hardness measurements. The results show that NiAl nanoparticles may have a compressed surface shell, which may be the reason why NiAl nanomaterials were difficult to densify sintering using conventional methods and why high-pressure sintering was an effective approach. We also observed that B2-structured NiAl could undergo a temperature-dependent phase transition and could be transformed into Al(0.9)Ni(4.22) below 1000 deg C for the first time. It was interesting to note that Vickers hardness decreased as grain size decreased below ~30 run, indicating that the inverse Hall-Petch effect may be observed in nano-polycrystalline NiAl (n-NiAl) samples. Moreover, a tentative interpretation was developed for high-pressure nanosintering, based on the shell-core model of nanoparticles. Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0–5.0 GPa and 600–1500 °C, respectively). The sintered samples were characterized by x-ray diffraction, scanning electron microscope, density, and indentation hardness measurements. The results show that NiAl nanoparticles may have a compressed surface shell, which may be the reason why NiAl nanomaterials were difficult to densify sintering using conventional methods and why high-pressure sintering was an effective approach. We also observed that B2-structured NiAl could undergo a temperature-dependent phase transition and could be transformed into Al 0.9 Ni 4.22 below 1000 °C for the first time. It is interesting to note that Vickers hardness decreased as grain size decreased below ∼30 nm, indicating that the inverse Hall-Petch effect may be observed in nano-polycrystalline NiAl (n-NiAl) samples. Moreover, a tentative interpretation was developed for high-pressure nanosintering, based on the shell-core model of nanoparticles. Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0–5.0 GPa and 600–1500 °C, respectively). The sintered samples were characterized by x-ray diffraction, scanning electron microscope, density, and indentation hardness measurements. The results show that NiAl nanoparticles may have a compressed surface shell, which may be the reason why NiAl nanomaterials were difficult to densify sintering using conventional methods and why high-pressure sintering was an effective approach. We also observed that B2-structured NiAl could undergo a temperature-dependent phase transition and could be transformed into Al0.9Ni4.22 below 1000 °C for the first time. It is interesting to note that Vickers hardness decreased as grain size decreased below ∼30 nm, indicating that the inverse Hall-Petch effect may be observed in nano-polycrystalline NiAl (n-NiAl) samples. Moreover, a tentative interpretation was developed for high-pressure nanosintering, based on the shell-core model of nanoparticles. |
| Author | Wang, Shanmin He, Duanwei Li, Yongjun Zou, Yongtao Wang, Jianghua Wang, Wendan Kou, Zili Wei, Jianjun Lei, Li |
| Author_xml | – sequence: 1 givenname: Shanmin surname: Wang fullname: Wang, Shanmin – sequence: 2 givenname: Duanwei surname: He fullname: He, Duanwei email: duanweihe@yahoo.com organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, People's Republic of China – sequence: 3 givenname: Yongtao surname: Zou fullname: Zou, Yongtao – sequence: 4 givenname: Jianjun surname: Wei fullname: Wei, Jianjun – sequence: 5 givenname: Li surname: Lei fullname: Lei, Li – sequence: 6 givenname: Yongjun surname: Li fullname: Li, Yongjun – sequence: 7 givenname: Jianghua surname: Wang fullname: Wang, Jianghua – sequence: 8 givenname: Wendan surname: Wang fullname: Wang, Wendan – sequence: 9 givenname: Zili surname: Kou fullname: Kou, Zili organization: Institute of Atomic and Molecular Physics, Sichuan University, Chengdu 610065, People's Republic of China |
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| Snippet | Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0–5.0 GPa and 600–1500 °C, respectively). The sintered samples were... Nanostructured bulk NiAl materials were prepared at high pressure and temperature (0-5.0 GPa and 600-1500 deg C, respectively). The sintered samples were... |
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| SubjectTerms | Applied and Technical Physics Biomaterials Grain size Inorganic Chemistry Materials Engineering Materials Science Nanostructure Nanotechnology Sintering |
| Title | High-pressure and high-temperature sintering of nanostructured bulk NiAl materials |
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