CeO2–TiO2 mixed oxide thin films with enhanced photocatalytic degradation of organic pollutants
A series of CeO 2 –TiO 2 mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible spectroscopy, atomic force microscopy, and X-ray photoelectron spectroscopy were used to investigate the characteristics of CeO 2 –TiO 2 sols and...
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| Published in | Journal of sol-gel science and technology Vol. 82; no. 3; pp. 772 - 782 |
|---|---|
| Main Authors | , |
| Format | Journal Article |
| Language | English |
| Published |
New York
Springer US
01.06.2017
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
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| Abstract | A series of CeO
2
–TiO
2
mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible spectroscopy, atomic force microscopy, and X-ray photoelectron spectroscopy were used to investigate the characteristics of CeO
2
–TiO
2
sols and thin films in order to determine the influence of adding CeO
2
to TiO
2
on the photocatalytic degradation of methylene blue aqueous solution under both ultraviolet and visible light irradiation. The pH values of the as-prepared CeO
2
–TiO
2
sols were neutral; the as-prepared sols contained nanocrystals in colloidal suspensions, and there was no subsequent calcination process. It was observed that the highest photocatalytic degradation activities with respect to methylene blue under both UV and visible light irradiation were exhibited for an optimum CeO
2
–TiO
2
weight ratio of 0.05. The high photocatalytic activity was because of changes in the spectral absorption of material, which was attributed to the heterojunction formed by TiO
2
and CeO
2
networks via Ti–O–Ce bonds after addition of CeO
2
. Thus, the presence of CeO
2
in TiO
2
significantly enhanced the photocatalytic activity.
Graphical Abstract |
|---|---|
| AbstractList | A series of CeO2–TiO2 mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible spectroscopy, atomic force microscopy, and X-ray photoelectron spectroscopy were used to investigate the characteristics of CeO2–TiO2 sols and thin films in order to determine the influence of adding CeO2 to TiO2 on the photocatalytic degradation of methylene blue aqueous solution under both ultraviolet and visible light irradiation. The pH values of the as-prepared CeO2–TiO2 sols were neutral; the as-prepared sols contained nanocrystals in colloidal suspensions, and there was no subsequent calcination process. It was observed that the highest photocatalytic degradation activities with respect to methylene blue under both UV and visible light irradiation were exhibited for an optimum CeO2–TiO2 weight ratio of 0.05. The high photocatalytic activity was because of changes in the spectral absorption of material, which was attributed to the heterojunction formed by TiO2 and CeO2 networks via Ti–O–Ce bonds after addition of CeO2. Thus, the presence of CeO2 in TiO2 significantly enhanced the photocatalytic activity. Graphical Abstract [InlineMediaObject not available: see fulltext.] A series of CeO 2 –TiO 2 mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible spectroscopy, atomic force microscopy, and X-ray photoelectron spectroscopy were used to investigate the characteristics of CeO 2 –TiO 2 sols and thin films in order to determine the influence of adding CeO 2 to TiO 2 on the photocatalytic degradation of methylene blue aqueous solution under both ultraviolet and visible light irradiation. The pH values of the as-prepared CeO 2 –TiO 2 sols were neutral; the as-prepared sols contained nanocrystals in colloidal suspensions, and there was no subsequent calcination process. It was observed that the highest photocatalytic degradation activities with respect to methylene blue under both UV and visible light irradiation were exhibited for an optimum CeO 2 –TiO 2 weight ratio of 0.05. The high photocatalytic activity was because of changes in the spectral absorption of material, which was attributed to the heterojunction formed by TiO 2 and CeO 2 networks via Ti–O–Ce bonds after addition of CeO 2 . Thus, the presence of CeO 2 in TiO 2 significantly enhanced the photocatalytic activity. Graphical Abstract |
| Author | Chen, Yu-Wen Moongraksathum, Benjawan |
| Author_xml | – sequence: 1 givenname: Benjawan surname: Moongraksathum fullname: Moongraksathum, Benjawan organization: Department of Chemical and Materials Engineering, National Central University – sequence: 2 givenname: Yu-Wen surname: Chen fullname: Chen, Yu-Wen email: ywchen@cc.ncu.edu.tw organization: Department of Chemical and Materials Engineering, National Central University, Department of Chemistry, Tomsk State University |
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| Keywords | Coating Binary oxide Titania Ceria Peroxo sol–gel Methylene blue |
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mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible... A series of CeO2–TiO2 mixed oxides were prepared by the peroxo sol–gel method. X-ray diffraction, transmission electron microscopy, ultraviolet–visible... |
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| SubjectTerms | Absorption spectra Aqueous solutions Atomic beam spectroscopy Atomic force microscopy Catalytic activity Ceramics Cerium oxides Chemistry and Materials Science Colloiding Composites Glass Heterojunctions Inorganic Chemistry Light irradiation Materials Science Methylene blue Microscopy Mixed oxides Nanocrystals Nanotechnology Natural Materials Optical and Electronic Materials Original Paper: Sol-gel and hybrid materials for catalytic Photocatalysis Photodegradation photoelectrochemical and sensor applications Photoelectrons Pollutants Sol-gel processes Sols Spectrum analysis Thin films Titanium dioxide Transmission electron microscopy Ultraviolet radiation X ray photoelectron spectroscopy X-ray diffraction |
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| Title | CeO2–TiO2 mixed oxide thin films with enhanced photocatalytic degradation of organic pollutants |
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