Comparative Study on Total Lipid Determination using Soxhlet, Roese-Gottlieb, Bligh & Dyer, and Modified Bligh & Dyer Extraction Methods
Soxhlet method was used in hot and standard extraction mode and compared with liquid–liquid extraction methods for lipid determination in food samples. Several solvent mixtures were investigated and Soxhlet extraction time was optimized. Soxhlet extraction was convenient only for solid samples. Exce...
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| Published in | Journal of food composition and analysis Vol. 14; no. 1; pp. 93 - 100 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
New York, NY
Elsevier Inc
01.02.2001
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | Soxhlet method was used in hot and standard extraction mode and compared with liquid–liquid extraction methods for lipid determination in food samples. Several solvent mixtures were investigated and Soxhlet extraction time was optimized. Soxhlet extraction was convenient only for solid samples. Except Roese–Gottlieb method, other liquid–liquid extraction methods were suitable for lipid extraction from all samples analysed. Even if the precision of each method was good (R.S.D.<3.5%), the comparison of extracted lipid amounts showed that, depending on the type of sample, some methods present serious limitations. |
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| AbstractList | Soxhlet method was used in hot and standard extraction mode and compared with liquid–liquid extraction methods for lipid determination in food samples. Several solvent mixtures were investigated and Soxhlet extraction time was optimized. Soxhlet extraction was convenient only for solid samples. Except Roese–Gottlieb method, other liquid–liquid extraction methods were suitable for lipid extraction from all samples analysed. Even if the precision of each method was good (R.S.D.<3.5%), the comparison of extracted lipid amounts showed that, depending on the type of sample, some methods present serious limitations. |
| Author | Covaci, A Manirakiza, P Schepens, P |
| Author_xml | – sequence: 1 givenname: P surname: Manirakiza fullname: Manirakiza, P – sequence: 2 givenname: A surname: Covaci fullname: Covaci, A – sequence: 3 givenname: P surname: Schepens fullname: Schepens, P |
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| Cites_doi | 10.1139/o59-099 10.1080/03067319808032622 10.1016/S0025-326X(98)00170-2 10.1007/BF00205141 10.1080/03067319508033120 10.1039/a905904k 10.1002/etc.5620101108 10.1016/S0165-9936(97)00080-0 10.1016/0045-6535(88)90108-7 10.4319/lo.1985.30.5.1099 |
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| Snippet | Soxhlet method was used in hot and standard extraction mode and compared with liquid–liquid extraction methods for lipid determination in food samples. Several... |
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| SubjectTerms | Applied sciences Biological and medical sciences Chemical engineering Exact sciences and technology extraction Food industries Fundamental and applied biological sciences. Psychology General aspects lipids Liquid-liquid extraction liquid–liquid Methods of analysis, processing and quality control, regulation, standards Soxhlet |
| Title | Comparative Study on Total Lipid Determination using Soxhlet, Roese-Gottlieb, Bligh & Dyer, and Modified Bligh & Dyer Extraction Methods |
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