Identification of Aspartic Acid Enantiomers Based on Molecularly Imprinted Polyaniline
Affinity sites for L-aspartic acid （L-Asp） in polyaniline （PAn） were created by two successive processes： first, L-Asp was simply added as template molecules during the polymerization of aniline; second, L-Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to...
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| Published in | Chinese journal of chemistry Vol. 29; no. 12; pp. 2659 - 2663 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.12.2011
WILEY‐VCH Verlag Wiley Subscription Services, Inc |
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| ISSN | 1001-604X 1614-7065 |
| DOI | 10.1002/cjoc.201180436 |
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| Abstract | Affinity sites for L-aspartic acid （L-Asp） in polyaniline （PAn） were created by two successive processes： first, L-Asp was simply added as template molecules during the polymerization of aniline; second, L-Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L-Asp template molecules has been utilized for enantioselective recognition of L- and D-Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L-Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L-Asp templates were revealed by Fourier-transform infrared （FTIR） spectrum. |
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| AbstractList | Affinity sites for L‐aspartic acid (L‐Asp) in polyaniline (PAn) were created by two successive processes: first, L‐Asp was simply added as template molecules during the polymerization of aniline; second, L‐Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L‐Asp template molecules has been utilized for enantioselective recognition of L‐ and D‐Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L‐Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L‐Asp templates were revealed by Fourier‐transform infrared (FTIR) spectrum.
Polyaniline, synthesized in the presence of L‐Asp as template molecules with subsequent extraction to create shape complementary cavities, was evaluated as MIP. The higher response and selectivity of the imprinted polyaniline for L‐Asp over D‐Asp can be assigned to the complementary cavities generated during extraction Affinity sites for L ‐aspartic acid ( L ‐Asp) in polyaniline (PAn) were created by two successive processes: first, L ‐Asp was simply added as template molecules during the polymerization of aniline; second, L ‐Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L ‐Asp template molecules has been utilized for enantioselective recognition of L ‐ and D ‐Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L‐ Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L ‐Asp templates were revealed by Fourier‐transform infrared (FTIR) spectrum. Affinity sites for L-aspartic acid (L-Asp) in polyaniline (PAn) were created by two successive processes: first, L-Asp was simply added as template molecules during the polymerization of aniline; second, L-Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L-Asp template molecules has been utilized for enantioselective recognition of L- and D-Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L-Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L-Asp templates were revealed by Fourier-transform infrared (FTIR) spectrum. Affinity sites for L-aspartic acid （L-Asp） in polyaniline （PAn） were created by two successive processes： first, L-Asp was simply added as template molecules during the polymerization of aniline; second, L-Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L-Asp template molecules has been utilized for enantioselective recognition of L- and D-Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L-Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L-Asp templates were revealed by Fourier-transform infrared （FTIR） spectrum. |
| Author | Ni, Junhua Chen, Zhidong Kong, Yong Yao, Chao Zhou, Yongsheng |
| AuthorAffiliation | Institute of Petrochemical Technology, Changzhou University, Changzhou, Jiangsu 213164, China |
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| CitedBy_id | crossref_primary_10_1016_j_msec_2013_05_052 crossref_primary_10_1016_j_cej_2015_08_041 crossref_primary_10_1002_jmr_2347 crossref_primary_10_1016_j_aca_2014_06_011 crossref_primary_10_1016_j_electacta_2012_10_095 crossref_primary_10_1109_JSEN_2014_2298872 crossref_primary_10_1016_j_chroma_2013_01_096 |
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| Notes | polyaniline, aspartic acid, enantioselectivity, molecularly imprinted polymer, IR spectroscopy 31-1547/O6 Affinity sites for L-aspartic acid （L-Asp） in polyaniline （PAn） were created by two successive processes： first, L-Asp was simply added as template molecules during the polymerization of aniline; second, L-Asp incorporated in PAn backbone was extracted by solvent. PAn with cavities complementary to L-Asp template molecules has been utilized for enantioselective recognition of L- and D-Asp. Enantioselectivity of the imprinted PAn could be attributed to the cavities in the imprinted PAn which was complementary to L-Asp templates both in shape and in positioning of groups. Also in this paper, the structural changes before and after extraction of L-Asp templates were revealed by Fourier-transform infrared （FTIR） spectrum. the Priority Academic Program Development of Jiangsu Higher Education Institutions (PAPD) istex:144CEAC9E2AC69E0C2D6A5D6AE8F5FA7BF5E9042 the National Natural Science Foundation of China - No. 20805021 Natural Science Fund for Colleges and Universities in Jiangsu Province - No. 10KJB150004, 09KJA430002 ark:/67375/WNG-FSBWDZD8-W ArticleID:CJOC201180436 ObjectType-Article-1 SourceType-Scholarly Journals-1 ObjectType-Feature-2 content type line 14 |
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| Snippet | Affinity sites for L-aspartic acid （L-Asp） in polyaniline （PAn） were created by two successive processes： first, L-Asp was simply added as template molecules... Affinity sites for L‐aspartic acid (L‐Asp) in polyaniline (PAn) were created by two successive processes: first, L‐Asp was simply added as template molecules... Affinity sites for L ‐aspartic acid ( L ‐Asp) in polyaniline (PAn) were created by two successive processes: first, L ‐Asp was simply added as template... Affinity sites for L-aspartic acid (L-Asp) in polyaniline (PAn) were created by two successive processes: first, L-Asp was simply added as template molecules... |
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| SubjectTerms | aspartic acid enantioselectivity IR spectroscopy molecularly imprinted polymer polyaniline 傅里叶变换红外光谱 分子印迹 天冬氨酸 天门冬氨酸 对映体 模板分子 聚苯胺 选择性识别 |
| Title | Identification of Aspartic Acid Enantiomers Based on Molecularly Imprinted Polyaniline |
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