Synthesis, Characterization, Optical and Electrochemical Properties of Fulleropyrrolidines Containing Trifluoromethyl Group
Four novel [60]fullerene pyrrolidines containing trifluoromethyl （--CF3） group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been characterized by UV-Vis spectroscopy, fourier transform in- frared spectroscopy, matrix-assisted laser desorption ionization-time of flight mas...
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| Published in | Chinese journal of chemistry Vol. 30; no. 5; pp. 1097 - 1101 |
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| Main Author | |
| Format | Journal Article |
| Language | English |
| Published |
Weinheim
WILEY-VCH Verlag
01.05.2012
WILEY‐VCH Verlag Wiley Wiley Subscription Services, Inc |
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| Abstract | Four novel [60]fullerene pyrrolidines containing trifluoromethyl （--CF3） group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been characterized by UV-Vis spectroscopy, fourier transform in- frared spectroscopy, matrix-assisted laser desorption ionization-time of flight mass spectroscopy, and IH, 13C, 19F nuclear magnetic resonance spectrometer （IH NMR, 13C NMR, 19F NMR）. Their optical and electrochemical prop- erties have been studied, and the results show that those fulleropyrrolidines containing --CF3 group have good fluo- rescence and electrochemical properties. Compared with C60, they have negative shifts in varying degrees for half-wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital （LUMO） levels are close to that of [6,6]-phenyl-C6：butyric acid methyl ester. |
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| AbstractList | Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF3) group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been characterized by UV-Vis spectroscopy, fourier transform infrared spectroscopy, matrix-assisted laser desorption ionization-time of flight mass spectroscopy, and 1H, 13C, 19F nuclear magnetic resonance spectrometer (1H NMR, 13C NMR, 19F NMR). Their optical and electrochemical properties have been studied, and the results show that those fulleropyrrolidines containing CF3 group have good fluorescence and electrochemical properties. Compared with C60, they have negative shifts in varying degrees for half-wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital (LUMO) levels are close to that of [6,6]-phenyl-C61-butyric acid methyl ester. Four novel [60]fullerene pyrrolidines containing trifluoromethyl （--CF3） group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been characterized by UV-Vis spectroscopy, fourier transform in- frared spectroscopy, matrix-assisted laser desorption ionization-time of flight mass spectroscopy, and IH, 13C, 19F nuclear magnetic resonance spectrometer （IH NMR, 13C NMR, 19F NMR）. Their optical and electrochemical prop- erties have been studied, and the results show that those fulleropyrrolidines containing --CF3 group have good fluo- rescence and electrochemical properties. Compared with C60, they have negative shifts in varying degrees for half-wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital （LUMO） levels are close to that of [6,6]-phenyl-C6：butyric acid methyl ester. Abstract Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF 3 ) group have been synthesized via 1,3‐dipolar cycloaddition reaction, which have been characterized by UV‐Vis spectroscopy, fourier transform infrared spectroscopy, matrix‐assisted laser desorption ionization‐time of flight mass spectroscopy, and 1 H, 13 C, 19 F nuclear magnetic resonance spectrometer ( 1 H NMR, 13 C NMR, 19 F NMR). Their optical and electrochemical properties have been studied, and the results show that those fulleropyrrolidines containing CF 3 group have good fluorescence and electrochemical properties. Compared with C 60 , they have negative shifts in varying degrees for half‐wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital (LUMO) levels are close to that of [6,6]‐phenyl‐C 61 ‐butyric acid methyl ester. Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF3) group have been synthesized via 1,3‐dipolar cycloaddition reaction, which have been characterized by UV‐Vis spectroscopy, fourier transform infrared spectroscopy, matrix‐assisted laser desorption ionization‐time of flight mass spectroscopy, and 1H, 13C, 19F nuclear magnetic resonance spectrometer (1H NMR, 13C NMR, 19F NMR). Their optical and electrochemical properties have been studied, and the results show that those fulleropyrrolidines containing CF3 group have good fluorescence and electrochemical properties. Compared with C60, they have negative shifts in varying degrees for half‐wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital (LUMO) levels are close to that of [6,6]‐phenyl‐C61‐butyric acid methyl ester. Four novel [60]fullerene pyrrolidines containing CF3 group have been synthesized, and their optical and electrochemical properties were also studied. |
| Author | Yu, Rui Fang, Shu Wei, Xianwen Li, Xiangzi |
| AuthorAffiliation | College of Chemistry and Materials Science, Key Laboratory of Functional Molecular Solids, the Ministry of Education, Anhui Laboratory of Molecule-based Materials, Anhui Normal University, Wuhu, Anhui 241000, China Department of Chemistry, Wannan Medical College, Wuhu, Anhui 241002, China |
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| Keywords | electrochemistry pyrrolidine PERFORMANCE AZOMETHINE YLIDES fullerenes trifluoromethyl group CONJUGATED POLYMERS RESONANCE fluorescence LIMITING PROPERTIES FULLERENE 1,3-DIPOLAR CYCLOADDITION C-60 DERIVATIVES |
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| Notes | 31-1547/O6 Four novel [60]fullerene pyrrolidines containing trifluoromethyl （--CF3） group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been characterized by UV-Vis spectroscopy, fourier transform in- frared spectroscopy, matrix-assisted laser desorption ionization-time of flight mass spectroscopy, and IH, 13C, 19F nuclear magnetic resonance spectrometer （IH NMR, 13C NMR, 19F NMR）. Their optical and electrochemical prop- erties have been studied, and the results show that those fulleropyrrolidines containing --CF3 group have good fluo- rescence and electrochemical properties. Compared with C60, they have negative shifts in varying degrees for half-wave potentials, and may have potential applications for photovoltaic conversion materials since their lowest unoccupied molecular orbital （LUMO） levels are close to that of [6,6]-phenyl-C6：butyric acid methyl ester. Li Xiangzi,Yu Rui,Fang Shu, Wei Xianwen（a College of Chemistry and Materials Science, Key Laboratory of Functional Molecular Solids, the Ministry of Education Anhui Laboratory of Molecule-based Materials, Anhui Normal University, Wuhu, Anhui 241000, China h Department of Chemistry, Wannan Medical College, Wuhu, Anhui 241002, China） fullerenes, trifluoromethyl group, pyrrolidine, fluorescence, electrochemistry istex:0AB853964C393BEB82F6C98D24074BB9B431DA48 the State Education Ministry of China - No. EYTP, SRF for ROCS, SRFDP 20070370001 the Natural Science Foundation of the Anhui Higher Education Institutions of China - No. KJ2010B250, 2006KJ006TD, 2008Z028 the Doctoral Research Initial Foundation of Wannan Medical College the Research Culture Founds of Anhui Normal University - No. 2010rcpy040 the Natural Science Foundation of Anhui Province, China - No. 1208085QE102 ArticleID:CJOC201100444 the National Natural Science Foundation of China - No. 21071005, 20671002, 20490217 ark:/67375/WNG-DMQ91FJG-3 |
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| SSID | ssj0027726 |
| Score | 1.9297245 |
| Snippet | Four novel [60]fullerene pyrrolidines containing trifluoromethyl （--CF3） group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been... Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF3) group have been synthesized via 1,3‐dipolar cycloaddition reaction, which have been... Four novel [60]fullerene pyrrolidines containing trifluoromethyl (?CF3) group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been... Abstract Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF 3 ) group have been synthesized via 1,3‐dipolar cycloaddition reaction, which... Four novel [60]fullerene pyrrolidines containing trifluoromethyl (CF3) group have been synthesized via 1,3-dipolar cycloaddition reaction, which have been... |
| Source | Web of Science |
| SourceID | proquest crossref webofscience wiley istex chongqing |
| SourceType | Aggregation Database Enrichment Source Index Database Publisher |
| StartPage | 1097 |
| SubjectTerms | Chemistry Chemistry, Multidisciplinary Desorption electrochemistry fluorescence fullerenes NMR Nuclear magnetic resonance Physical Sciences pyrrolidine Science & Technology Spectrum analysis trifluoromethyl group 三氟甲基 偶极环加成反应 光学 合成 基质辅助激光解吸电离 核磁共振波谱仪 电化学性质 紫外可见光谱 |
| Title | Synthesis, Characterization, Optical and Electrochemical Properties of Fulleropyrrolidines Containing Trifluoromethyl Group |
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