Stimuli-responsive poly(phenyl acetylene) microparticles with tunable chirality

[Display omitted] •Helical dendronized poly(phenyl acetylene) microparticles were fabricated.•Thermally-induced dehydration induced reversible chirality transitions.•Solution pH show significant effect on helical conformation.•OEG dendrons provide shielding effect for coordination of metal ions. Chi...

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Published inEuropean polymer journal Vol. 118; pp. 275 - 279
Main Authors Zhao, Yuanbo, Zhang, Xiacong, Li, Wen, Zhang, Afang
Format Journal Article
LanguageEnglish
Published Oxford Elsevier Ltd 01.09.2019
Elsevier BV
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Abstract [Display omitted] •Helical dendronized poly(phenyl acetylene) microparticles were fabricated.•Thermally-induced dehydration induced reversible chirality transitions.•Solution pH show significant effect on helical conformation.•OEG dendrons provide shielding effect for coordination of metal ions. Chiral polymeric microparticles combine the characteristics of chirality and spherical morphology in one matter, which may provide confined microenvironments to switch chirality and to promote conformation transition. Here we report on fabrication of chiral polymeric microparticles (CMPs) from dendronized copolymers, and investigation of their tunable chirality upon external stimuli, such as temperature, pH, metal ion complexation and solvents. These polymeric microparticles were constructed via one-pot approach through precipitation copolymerization of phenylacetylene derivatives. The monomers contain dendritic oligoethylene glycol (OEG) to afford copolymers thermoresponsiveness and alkynyl groups for polymerization and crosslinking. Chirality of the polymeric microparticles was afforded by intrinsic chirality from the amino acid moieties. Furthermore, thermoresponsiveness of these microparticles paves a novel route to switch their chirality and mediate their responsive behavior to metal ion coordination.
AbstractList Chiral polymeric microparticles combine the characteristics of chirality and spherical morphology in one matter, which may provide confined microenvironments to switch chirality and to promote conformation transition. Here we report on fabrication of chiral polymeric microparticles (CMPs) from dendronized copolymers, and investigation of their tunable chirality upon external stimuli, such as temperature, pH, metal ion complexation and solvents. These polymeric microparticles were constructed via one-pot approach through precipitation copolymerization of phenylacetylene derivatives. The monomers contain dendritic oligoethylene glycol (OEG) to afford copolymers thermoresponsiveness and alkynyl groups for polymerization and crosslinking. Chirality of the polymeric microparticles was afforded by intrinsic chirality from the amino acid moieties. Furthermore, thermoresponsiveness of these microparticles paves a novel route to switch their chirality and mediate their responsive behavior to metal ion coordination.
[Display omitted] •Helical dendronized poly(phenyl acetylene) microparticles were fabricated.•Thermally-induced dehydration induced reversible chirality transitions.•Solution pH show significant effect on helical conformation.•OEG dendrons provide shielding effect for coordination of metal ions. Chiral polymeric microparticles combine the characteristics of chirality and spherical morphology in one matter, which may provide confined microenvironments to switch chirality and to promote conformation transition. Here we report on fabrication of chiral polymeric microparticles (CMPs) from dendronized copolymers, and investigation of their tunable chirality upon external stimuli, such as temperature, pH, metal ion complexation and solvents. These polymeric microparticles were constructed via one-pot approach through precipitation copolymerization of phenylacetylene derivatives. The monomers contain dendritic oligoethylene glycol (OEG) to afford copolymers thermoresponsiveness and alkynyl groups for polymerization and crosslinking. Chirality of the polymeric microparticles was afforded by intrinsic chirality from the amino acid moieties. Furthermore, thermoresponsiveness of these microparticles paves a novel route to switch their chirality and mediate their responsive behavior to metal ion coordination.
Author Zhang, Xiacong
Zhao, Yuanbo
Li, Wen
Zhang, Afang
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Keywords Helical polymer
Poly(phenyl acetylene)
Stimuli-responsiveness
Thermoresponsiveness
Chirality
Polymeric microparticle
Language English
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SSID ssj0007363
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Snippet [Display omitted] •Helical dendronized poly(phenyl acetylene) microparticles were fabricated.•Thermally-induced dehydration induced reversible chirality...
Chiral polymeric microparticles combine the characteristics of chirality and spherical morphology in one matter, which may provide confined microenvironments...
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SubjectTerms Antifreeze solutions
Chirality
Copolymerization
Copolymers
Crosslinking
Crosslinking polymerization
Helical polymer
Metal ions
Microparticles
Morphology
Nanoparticles
Poly(phenyl acetylene)
Polymeric microparticle
Polyphenylacetylene
Stimuli
Stimuli-responsiveness
Thermoresponsiveness
Title Stimuli-responsive poly(phenyl acetylene) microparticles with tunable chirality
URI https://dx.doi.org/10.1016/j.eurpolymj.2019.05.054
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