Production of porous activated carbons from Caesalpinia ferrea seed pod wastes: Highly efficient removal of captopril from aqueous solutions

Porous activated carbons (ACs) prepared from a lignocellulosic waste, Caesalpinia ferrea seed pod wastes (CF) were utilised for removing captopril pharmaceutical from synthetic hospital effluents and aqueous effluents. Chemical activation using ZnCl2 was performed. It was utilised the following prop...

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Published inJournal of cleaner production Vol. 197; no. 1; pp. 919 - 929
Main Authors Kasperiski, Fernando M., Lima, Eder C., Umpierres, Cibele S., dos Reis, Glaydson S., Thue, Pascal Silas, Lima, Diana Ramos, Dias, Silvio L.P., Saucier, Caroline, da Costa, Janaina B.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.10.2018
Elsevier
Subjects
Activated carbon
Adsorption
Caesalpinia ferrea
Captopril
Chemical Sciences
Emerging contaminant
Pharmaceutical
Emerging contaminant
Pharmaceutical
Adsorption
Captopril
Activated carbon
Caesalpinia ferrea
TRAITEMENT DE L&apos
ACTIVATED CARBON
PHARMACEUTICAL
EMERGING CONTAMINANT
HOPITAL
EAU
CONTAMINATION
INHIBITEUR
ADSORPTION
CAPTOPRIL
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Abstract Porous activated carbons (ACs) prepared from a lignocellulosic waste, Caesalpinia ferrea seed pod wastes (CF) were utilised for removing captopril pharmaceutical from synthetic hospital effluents and aqueous effluents. Chemical activation using ZnCl2 was performed. It was utilised the following proportions CF-Biomass: ZnCl2 (1: 0.5, 1:1 and 1:1.5, obtaining CFAC.0.5, CFAC.1.0, and CFAC.1.5 activated carbons. These mixtures were pyrolysed at 600 °C in a conventional furnace. The ACs were characterised by FTIR, hydrophobic/hydrophilic ratio (HI), CHN/O elemental analysis, Boehm titration, surface areas (SBET), total pore volumes, and pore size distribution. These analyses show that the ACs presents several functional groups on AC surfaces and there is a predominance of hydrophilic surfaces. All the activated carbons prepared presented surface area 1050–1480 m2 g−1. Regarding the adsorption process, the kinetics data were fitted to General-order kinetic model and equilibrium of adsorption data were well represented by and Liu isotherm model. The maximum adsorption capacity of 535.5 mg g−1 was obtained at 25 °C for the sample CFAC.1.5. The thermodynamic studies have shown that the adsorption process of captopril is spontaneous and favourable. The employment of the ACs for treating simulated effluents, with different emerging contaminants, showed an excellent removal (up to 97.67%). This result is evidence that Caesalpinia ferrea seed pod wastes were a high-efficiency precursor for AC preparation and that such activated carbons could be used for treating hospital effluents containing pharmaceuticals. •Caesalpinia ferrea seed pods were used as carbon source for preparation of activated carbon.•Efficient removal of captopril pharmaceutical from hospital effluents was obtained.•Maximum captopril sorption capacity of 776.2 mg g−1.•The several functional groups of ACs surface leads to a hydrophilic surface of ACs.
AbstractList Porous activated carbons (ACs) prepared from a lignocellulosic waste, Caesalpinia ferrea seed pod wastes (CF) were utilised for removing captopril pharmaceutical from synthetic hospital effluents and aqueous effluents. Chemical activation using ZnCl2 was performed. It was utilised the following proportions CF-Biomass: ZnCl2 (1: 0.5, 1:1 and 1:1.5, obtaining CFAC.0.5, CFAC.1.0, and CFAC.1.5 activated carbons. These mixtures were pyrolysed at 600 °C in a conventional furnace. The ACs were characterised by FTIR, hydrophobic/hydrophilic ratio (HI), CHN/O elemental analysis, Boehm titration, surface areas (SBET), total pore volumes, and pore size distribution. These analyses show that the ACs presents several functional groups on AC surfaces and there is a predominance of hydrophilic surfaces. All the activated carbons prepared presented surface area 1050–1480 m2 g−1. Regarding the adsorption process, the kinetics data were fitted to General-order kinetic model and equilibrium of adsorption data were well represented by and Liu isotherm model. The maximum adsorption capacity of 535.5 mg g−1 was obtained at 25 °C for the sample CFAC.1.5. The thermodynamic studies have shown that the adsorption process of captopril is spontaneous and favourable. The employment of the ACs for treating simulated effluents, with different emerging contaminants, showed an excellent removal (up to 97.67%). This result is evidence that Caesalpinia ferrea seed pod wastes were a high-efficiency precursor for AC preparation and that such activated carbons could be used for treating hospital effluents containing pharmaceuticals. •Caesalpinia ferrea seed pods were used as carbon source for preparation of activated carbon.•Efficient removal of captopril pharmaceutical from hospital effluents was obtained.•Maximum captopril sorption capacity of 776.2 mg g−1.•The several functional groups of ACs surface leads to a hydrophilic surface of ACs.
Porous activated carbons (ACs) prepared from a lignocellulosic waste, Caesalpinia ferrea seed pod wastes (CF) were utilised for removing captopril pharmaceutical from synthetic hospital effluents and aqueous effluents. Chemical activation using ZnCl2 was performed. It was utilised the following proportions CFBiomass: ZnCl2 (1: 0.5, 1:1 and 1:1.5, obtaining CFAC.0.5, CFAC.1.0, and CFAC.1.5 activated carbons. These mixtures were pyrolysed at 600 °C in a conventional furnace. The ACs were characterised by FTIR, hydrophobic/hydrophilic ratio (HI), CHN/O elemental analysis, Boehm titration, surface areas (SBET), total pore volumes, and pore size distribution. These analyses show that the ACs presents several functional groups on AC surfaces and there is a predominance of hydrophilic surfaces. All the activated carbons prepared presented surface area 1050-1480m2 g-1. Regarding the adsorption process, the kinetics data were fitted to General-order kinetic model and equilibrium of adsorption data were well represented by and Liu isotherm model. The maximum adsorption capacity of 535.5 mg g-1 was obtained at 25 °C for the sample CFAC.1.5. The thermodynamic studies have shown that the adsorption process of captopril is spontaneous and favourable. The employment of the ACs for treating simulated effluents, with different emerging contaminants, showed an excellent removal (up to 97.67%). This result is evidence that Caesalpinia ferrea seed pod wastes were a high-efficiency precursor for AC preparation and that such activated carbons could be used for treating hospital effluents containing pharmaceuticals.
Author Thue, Pascal Silas
Kasperiski, Fernando M.
Dias, Silvio L.P.
Saucier, Caroline
Lima, Diana Ramos
dos Reis, Glaydson S.
da Costa, Janaina B.
Umpierres, Cibele S.
Lima, Eder C.
Author_xml – sequence: 1
  givenname: Fernando M.
  surname: Kasperiski
  fullname: Kasperiski, Fernando M.
  organization: Graduate Program in Metallurgical, Mine and Materials Engineering (PPGE3M), School of Engineering, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, Porto Alegre, RS, Brazil
– sequence: 2
  givenname: Eder C.
  surname: Lima
  fullname: Lima, Eder C.
  email: eder.lima@ufrgs.br, profederlima@gmail.com
  organization: Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, P.O. Box 15003, 91501-970, Porto Alegre, RS, Brazil
– sequence: 3
  givenname: Cibele S.
  surname: Umpierres
  fullname: Umpierres, Cibele S.
  organization: Graduate Program in Science of Materials (PGCIMAT), Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, Porto Alegre, RS, Brazil
– sequence: 4
  givenname: Glaydson S.
  surname: dos Reis
  fullname: dos Reis, Glaydson S.
  organization: Graduate Program in Metallurgical, Mine and Materials Engineering (PPGE3M), School of Engineering, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, Porto Alegre, RS, Brazil
– sequence: 5
  givenname: Pascal Silas
  surname: Thue
  fullname: Thue, Pascal Silas
  organization: Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, P.O. Box 15003, 91501-970, Porto Alegre, RS, Brazil
– sequence: 6
  givenname: Diana Ramos
  surname: Lima
  fullname: Lima, Diana Ramos
  organization: Graduate Program in Metallurgical, Mine and Materials Engineering (PPGE3M), School of Engineering, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, Porto Alegre, RS, Brazil
– sequence: 7
  givenname: Silvio L.P.
  surname: Dias
  fullname: Dias, Silvio L.P.
  organization: Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, P.O. Box 15003, 91501-970, Porto Alegre, RS, Brazil
– sequence: 8
  givenname: Caroline
  surname: Saucier
  fullname: Saucier, Caroline
  organization: Graduate Program in Chemistry (PPGQ), Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, Porto Alegre, RS, Brazil
– sequence: 9
  givenname: Janaina B.
  surname: da Costa
  fullname: da Costa, Janaina B.
  organization: Institute of Chemistry, Federal University of Rio Grande Do Sul (UFRGS), Av. Bento Gonçalves 9500, P.O. Box 15003, 91501-970, Porto Alegre, RS, Brazil
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Issue 1
Keywords Emerging contaminant
Pharmaceutical
Adsorption
Captopril
Activated carbon
Caesalpinia ferrea
TRAITEMENT DE L&apos
ACTIVATED CARBON
PHARMACEUTICAL
EMERGING CONTAMINANT
HOPITAL
EAU
CONTAMINATION
INHIBITEUR
ADSORPTION
CAPTOPRIL
Language English
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SSID ssj0017074
Score 2.612137
Snippet Porous activated carbons (ACs) prepared from a lignocellulosic waste, Caesalpinia ferrea seed pod wastes (CF) were utilised for removing captopril...
SourceID hal
crossref
elsevier
SourceType Open Access Repository
Aggregation Database
Publisher
StartPage 919
SubjectTerms Activated carbon
Adsorption
Caesalpinia ferrea
Captopril
Chemical Sciences
Emerging contaminant
Pharmaceutical
Title Production of porous activated carbons from Caesalpinia ferrea seed pod wastes: Highly efficient removal of captopril from aqueous solutions
URI https://dx.doi.org/10.1016/j.jclepro.2018.06.146
https://hal.science/hal-02974324
Volume 197
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