Effect of Yb2O3 doping on the grain boundary of NiFe2O4-10NiO-based cermets after sintering

xYb2O3-15（20Ni-Cu）/（85 -x）（NiFe2O4-10NiO）（x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0） cermets for aluminum electrolysis were prepared to investigate the effect ofYb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with in...

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Published in	International journal of minerals, metallurgy and materials Vol. 22; no. 12; pp. 1334 - 1341
Main Author	He, Han-bing
Format	Journal Article
Language	English
Published	Beijing University of Science and Technology Beijing 01.12.2015 Springer Nature B.V School of Metal urgy and Environment, Central South University, Changsha 410083, China
Subjects	Aluminum Ceramics Cermets Characterization and Evaluation of Materials Chemistry and Materials Science Composites Corrosion and Coatings Corrosion resistance Decomposition reactions Doping Electrical resistivity Electrolysis Electron probe microanalysis Fe2O3 Glass Grain boundaries Materials Science Metallic Materials Microstructural analysis Natural Materials Nickel ferrites Phase composition Sintering Specific gravity Surfaces and Interfaces Thin Films Tribology X-ray diffraction X-ray spectroscopy X射线光谱仪 Yb2O3 扫描电子显微镜掺杂晶界金属陶瓷陶瓷烧结 doping aluminum electrolysis grain boundaries cermets ytterbium oxide
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Abstract	xYb2O3-15（20Ni-Cu）/（85 -x）（NiFe2O4-10NiO）（x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0） cermets for aluminum electrolysis were prepared to investigate the effect ofYb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb2O3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction （XRD）, scanning electron microscopy with energy dispersive X-ray spectroscopy （SEM/EDX）, and electron probe microanalysis （EPMA）, YbFeO3 was produced along the grain boundary. The YbFeO3 was concluded to not only have formed from the interaction between the NiFe2O4 or Fe2O3 component and Yb2O3 at the grain boundary of the cermets, but also from the decomposition of NiFe2O4 into NiO and Fe2O3 and the subsequent reaction of Fe2O3 with Yb2O3. Thus, the production of YbFeO3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance.
AbstractList	xYb2O3–15(20Ni–Cu)/(85 − x)(NiFe2O4–10NiO) (x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to investigate the effect of Yb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb2O3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction (XRD), scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM/EDX), and electron probe microanalysis (EPMA), YbFeO3 was produced along the grain boundary. The YbFeO3 was concluded to not only have formed from the interaction between the NiFe2O4 or Fe2O3 component and Yb2O3 at the grain boundary of the cermets, but also from the decomposition of NiFe2O4 into NiO and Fe2O3 and the subsequent reaction of Fe2O3 with Yb2O3. Thus, the production of YbFeO3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance. xYb2O3–15(20Ni–Cu)/(85?x)(NiFe2O4–10NiO) (x=0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to investigate the effect of Yb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb2O3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction (XRD), scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM/EDX), and electron probe microanalysis (EPMA), YbFeO3 was produced along the grain boundary. The YbFeO3 was concluded to not only have formed from the interaction between the NiFe2O4 or Fe2O3 component and Yb2O3 at the grain boundary of the cermets, but also from the decomposition of NiFe2O4 into NiO and Fe2O3 and the subsequent reaction of Fe2O3 with Yb2O3. Thus, the pro-duction of YbFeO3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance. xYb2O3-15（20Ni-Cu）/（85 -x）（NiFe2O4-10NiO）（x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0） cermets for aluminum electrolysis were prepared to investigate the effect ofYb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb2O3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction （XRD）, scanning electron microscopy with energy dispersive X-ray spectroscopy （SEM/EDX）, and electron probe microanalysis （EPMA）, YbFeO3 was produced along the grain boundary. The YbFeO3 was concluded to not only have formed from the interaction between the NiFe2O4 or Fe2O3 component and Yb2O3 at the grain boundary of the cermets, but also from the decomposition of NiFe2O4 into NiO and Fe2O3 and the subsequent reaction of Fe2O3 with Yb2O3. Thus, the production of YbFeO3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance. x Yb 2 O 3 –15(20Ni–Cu)/(85 − x )(NiFe 2 O 4 –10NiO) ( x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to investigate the effect of Yb 2 O 3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb 2 O 3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction (XRD), scanning electron microscopy with energy dispersive X-ray spectroscopy (SEM/EDX), and electron probe microanalysis (EPMA), YbFeO 3 was produced along the grain boundary. The YbFeO 3 was concluded to not only have formed from the interaction between the NiFe 2 O 4 or Fe 2 O 3 component and Yb 2 O 3 at the grain boundary of the cermets, but also from the decomposition of NiFe 2 O 4 into NiO and Fe 2 O 3 and the subsequent reaction of Fe 2 O 3 with Yb 2 O 3 . Thus, the production of YbFeO 3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance.
Author	Han-bing He
AuthorAffiliation	School of Metallurgy and Environment, Central South University, Changsha 410083, China Department of Metallurgical Engineering, University of Utah, Salt Lake City, UT 84112, USA
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Cites_doi	10.1111/jace.12080 10.1007/s11771-007-0120-2 10.1111/j.1551-2916.2012.05305.x 10.4028/www.scientific.net/AMM.508.61 10.1007/s11837-009-0067-x 10.1007/BF02915044 10.1016/j.ceramint.2012.06.006 10.1023/A:1003464304488 10.1016/S1003-6326(11)60752-8 10.1016/S1003-6326(08)60194-6 10.1016/j.solidstatesciences.2011.05.004 10.1016/S1003-6326(13)62934-9 10.1023/A:1003460220418
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Copyright	University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2015 University of Science and Technology Beijing and Springer-Verlag Berlin Heidelberg 2015. Copyright © Wanfang Data Co. Ltd. All Rights Reserved.
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Keywords	doping aluminum electrolysis grain boundaries cermets ytterbium oxide
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Notes	xYb2O3-15（20Ni-Cu）/（85 -x）（NiFe2O4-10NiO）（x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0） cermets for aluminum electrolysis were prepared to investigate the effect ofYb2O3 doping on the grain boundary of the cermets after sintering. The results showed that each interface was very clear and that with increasing Yb2O3 content, most of the Yb was evenly distributed at the grain boundary. Moreover, according to the phase composition and microstructural analysis by X-ray diffraction （XRD）, scanning electron microscopy with energy dispersive X-ray spectroscopy （SEM/EDX）, and electron probe microanalysis （EPMA）, YbFeO3 was produced along the grain boundary. The YbFeO3 was concluded to not only have formed from the interaction between the NiFe2O4 or Fe2O3 component and Yb2O3 at the grain boundary of the cermets, but also from the decomposition of NiFe2O4 into NiO and Fe2O3 and the subsequent reaction of Fe2O3 with Yb2O3. Thus, the production of YbFeO3 resulted in a cermet with high relative density, good electrical conductivity, and good corrosion resistance. cermets; ytterbium oxide; doping; grain boundaries; aluminum electrolysis 11-5787/TF
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PublicationTitle	International journal of minerals, metallurgy and materials
PublicationTitleAbbrev	Int J Miner Metall Mater
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PublicationTitle_FL	International Journal of Minerals, Metallurgy and Materials
PublicationYear	2015
Publisher	University of Science and Technology Beijing Springer Nature B.V School of Metal urgy and Environment, Central South University, Changsha 410083, China
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Snippet	xYb2O3-15（20Ni-Cu）/（85 -x）（NiFe2O4-10NiO）（x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0） cermets for aluminum electrolysis were prepared to investigate the... x Yb 2 O 3 –15(20Ni–Cu)/(85 − x )(NiFe 2 O 4 –10NiO) ( x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to... xYb2O3–15(20Ni–Cu)/(85 − x)(NiFe2O4–10NiO) (x = 0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to investigate the... xYb2O3–15(20Ni–Cu)/(85?x)(NiFe2O4–10NiO) (x=0, 0.25, 0.5, 0.75, 1.0, 2.0, and 10.0) cermets for aluminum electrolysis were prepared to investigate the effect...
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SubjectTerms	Aluminum Ceramics Cermets Characterization and Evaluation of Materials Chemistry and Materials Science Composites Corrosion and Coatings Corrosion resistance Decomposition reactions Doping Electrical resistivity Electrolysis Electron probe microanalysis Fe2O3 Glass Grain boundaries Materials Science Metallic Materials Microstructural analysis Natural Materials Nickel ferrites Phase composition Sintering Specific gravity Surfaces and Interfaces Thin Films Tribology X-ray diffraction X-ray spectroscopy X射线光谱仪 Yb2O3 扫描电子显微镜掺杂晶界金属陶瓷陶瓷烧结
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Title	Effect of Yb2O3 doping on the grain boundary of NiFe2O4-10NiO-based cermets after sintering
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