Structural investigation of Te-based chalcogenide glasses using Raman spectroscopy
► Firstly study the structural change of metal and metal halide modified GeTe4 glass. ► The 124cm−1and 140cm−1 bands (Ge–Te, Te–Te) are insensitive to composition change. ► Zn, In and Sb will open up the chain structures of Ge–Te and Te–Te. ► Both Ga and metal halide (iodine) ultimately act as glass...
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Published in | Infrared physics & technology Vol. 55; no. 4; pp. 316 - 319 |
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Main Authors | , , , , , , , , |
Format | Journal Article |
Language | English |
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Elsevier B.V
01.07.2012
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Abstract | ► Firstly study the structural change of metal and metal halide modified GeTe4 glass. ► The 124cm−1and 140cm−1 bands (Ge–Te, Te–Te) are insensitive to composition change. ► Zn, In and Sb will open up the chain structures of Ge–Te and Te–Te. ► Both Ga and metal halide (iodine) ultimately act as glass network stabilizer.
Structural changes of metals (Zn, Sb, In, Ga) and metal halides (AgI, ZnI2, CdI2, PbI2, BiI3) modified GeTe4 glasses were investigated with the aid of Raman spectroscopy. The Raman spectra of these glasses in the frequency region between 100cm−1 and 300cm−1 display four main bands at about 124, 140, 159 and 275cm−1 which are contributed by Ge–Te, Te–Te, Te–Te and Ge–Ge vibration modes. The intensity of 159cm−1 and 275cm−1 bands vary with the addition of different glass modifiers. While the relative intensity of the 124cm−1 and 140cm−1 bands are insensitive to composition changes. Glass modifiers like Zn, In and Sb act as glass network unstabilizer which will disorganize the glass network by opening up the chain structures of Ge–Te and Te–Te. In the case of Ga and metal halides, Ga can open up Ge–(Te–Te)4/2 tetrahedra and form Ga–(Te–Te)3/2 triangle. Iodine can form covalent bonds with tellurium and decrease the tendency of microcrystal formation. Thus both Ga and iodine ultimately act as glass network stabilizer. |
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AbstractList | Structural changes of metals (Zn, Sb, In, Ga) and metal halides (AgI, ZnI2, CdI2, PbI2, BiI3) modified GeTe4 glasses were investigated with the aid of Raman spectroscopy. The Raman spectra of these glasses in the frequency region between 100 cma1 and 300 cma1 display four main bands at about 124, 140, 159 and 275 cma1 which are contributed by GeaTe, TeaTe, TeaTe and GeaGe vibration modes. The intensity of 159 cma1 and 275 cma1 bands vary with the addition of different glass modifiers. While the relative intensity of the 124 cma1 and 140 cma1 bands are insensitive to composition changes. Glass modifiers like Zn, In and Sb act as glass network unstabilizer which will disorganize the glass network by opening up the chain structures of GeaTe and TeaTe. In the case of Ga and metal halides, Ga can open up Gea(TeaTe)4/2 tetrahedra and form Gaa(TeaTe)3/2 triangle. Iodine can form covalent bonds with tellurium and decrease the tendency of microcrystal formation. Thus both Ga and iodine ultimately act as glass network stabilizer. ► Firstly study the structural change of metal and metal halide modified GeTe4 glass. ► The 124cm−1and 140cm−1 bands (Ge–Te, Te–Te) are insensitive to composition change. ► Zn, In and Sb will open up the chain structures of Ge–Te and Te–Te. ► Both Ga and metal halide (iodine) ultimately act as glass network stabilizer. Structural changes of metals (Zn, Sb, In, Ga) and metal halides (AgI, ZnI2, CdI2, PbI2, BiI3) modified GeTe4 glasses were investigated with the aid of Raman spectroscopy. The Raman spectra of these glasses in the frequency region between 100cm−1 and 300cm−1 display four main bands at about 124, 140, 159 and 275cm−1 which are contributed by Ge–Te, Te–Te, Te–Te and Ge–Ge vibration modes. The intensity of 159cm−1 and 275cm−1 bands vary with the addition of different glass modifiers. While the relative intensity of the 124cm−1 and 140cm−1 bands are insensitive to composition changes. Glass modifiers like Zn, In and Sb act as glass network unstabilizer which will disorganize the glass network by opening up the chain structures of Ge–Te and Te–Te. In the case of Ga and metal halides, Ga can open up Ge–(Te–Te)4/2 tetrahedra and form Ga–(Te–Te)3/2 triangle. Iodine can form covalent bonds with tellurium and decrease the tendency of microcrystal formation. Thus both Ga and iodine ultimately act as glass network stabilizer. Structural changes of metals (Zn, Sb, In, Ga) and metal halides (AgI, ZnI2, CdI2, PbI2, BiI3) modified GeTe4 glasses were investigated with the aid of Raman spectroscopy. The Raman spectra of these glasses in the frequency region between 100 cm−1 and 300 cm−1 display four main bands at about 124, 140, 159 and 275 cm−1 which are contributed by Ge-Te, Te-Te, Te-Te and Ge-Ge vibration modes. The intensity of 159 cm−1 and 275 cm−1 bands vary with the addition of different glass modifiers. While the relative intensity of the 124 cm−1 and 140 cm−1 bands are insensitive to composition changes. Glass modifiers like Zn, In and Sb act as glass network unstabilizer which will disorganize the glass network by opening up the chain structures of Ge-Te and Te-Te. In the case of Ga and metal halides, Ga can open up Ge-(Te-Te)4/2 tetrahedra and form Ga-(Te-Te)3/2 triangle. Iodine can form covalent bonds with tellurium and decrease the tendency of microcrystal formation. Thus both Ga and iodine ultimately act as glass network stabilizer. |
Author | Dai, Shixun Boussard, Catherine Conseil, Clément Zhang, Xianghua Wang, Xunsi Ma, Hongli Nie, Qiuhua Sun, Jie Bureau, Bruno |
Author_xml | – sequence: 1 givenname: Jie surname: Sun fullname: Sun, Jie organization: College of Information Science and Engineering, Ningbo University, Ningbo 31521, China – sequence: 2 givenname: Qiuhua surname: Nie fullname: Nie, Qiuhua organization: College of Information Science and Engineering, Ningbo University, Ningbo 31521, China – sequence: 3 givenname: Xunsi surname: Wang fullname: Wang, Xunsi email: xunsiwang@siom.ac.cn organization: College of Information Science and Engineering, Ningbo University, Ningbo 31521, China – sequence: 4 givenname: Shixun surname: Dai fullname: Dai, Shixun organization: College of Information Science and Engineering, Ningbo University, Ningbo 31521, China – sequence: 5 givenname: Xianghua surname: Zhang fullname: Zhang, Xianghua organization: Laboratory of Glasses and Ceramics, UMR 6226 CNRS, University of Rennes 1, Rennes Cedex 135042, France – sequence: 6 givenname: Bruno surname: Bureau fullname: Bureau, Bruno organization: Laboratory of Glasses and Ceramics, UMR 6226 CNRS, University of Rennes 1, Rennes Cedex 135042, France – sequence: 7 givenname: Catherine surname: Boussard fullname: Boussard, Catherine organization: Laboratory of Glasses and Ceramics, UMR 6226 CNRS, University of Rennes 1, Rennes Cedex 135042, France – sequence: 8 givenname: Clément surname: Conseil fullname: Conseil, Clément organization: Laboratory of Glasses and Ceramics, UMR 6226 CNRS, University of Rennes 1, Rennes Cedex 135042, France – sequence: 9 givenname: Hongli surname: Ma fullname: Ma, Hongli organization: Laboratory of Glasses and Ceramics, UMR 6226 CNRS, University of Rennes 1, Rennes Cedex 135042, France |
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Keywords | Te Chalcogenide glass Raman spectra |
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Snippet | ► Firstly study the structural change of metal and metal halide modified GeTe4 glass. ► The 124cm−1and 140cm−1 bands (Ge–Te, Te–Te) are insensitive to... Structural changes of metals (Zn, Sb, In, Ga) and metal halides (AgI, ZnI2, CdI2, PbI2, BiI3) modified GeTe4 glasses were investigated with the aid of Raman... |
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SubjectTerms | Antimony Chalcogenide glass Chemical Sciences Material chemistry Raman spectra |
Title | Structural investigation of Te-based chalcogenide glasses using Raman spectroscopy |
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