The fracture toughness of alumina coatings plasma-sprayed at different in situ temperatures
Alumina coatings were prepared by atmospheric plasma spraying through controlling the surface temperature of the coatings during spraying. Both the polished and fractured cross-section microstructures of the coatings were characterized by scanning electron microscopy (SEM). The phase structures of t...
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| Published in | Ceramics international Vol. 38; no. 6; pp. 4661 - 4667 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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Elsevier Ltd
01.08.2012
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| Abstract | Alumina coatings were prepared by atmospheric plasma spraying through controlling the surface temperature of the coatings during spraying. Both the polished and fractured cross-section microstructures of the coatings were characterized by scanning electron microscopy (SEM). The phase structures of the coatings and the feedstock were analyzed by X-ray diffraction technique (XRD). The microstructure and phase structure of the coatings prepared at different substrate temperatures were examined. SEM observations show that the intersplat bonding within the coatings was significantly improved by increasing the substrate temperature. The fracture toughness of the deposits was measured by indentation methods. For the coatings prepared at low substrate temperatures, the fracture toughness increased with the substrate temperature due to the improvement in the intersplat bonding. However, a significant decrease in the fracture toughness was found for the coatings prepared at high substrate temperatures. The change in phase structure of the coatings suggested that the residual tensile stress mainly resulted from phase transformation from γ-alumina to α-alumina at high substrate temperature should answer for the decline in the fracture toughness. |
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| AbstractList | Alumina coatings were prepared by atmospheric plasma spraying by controlling the surface temperature of the coatings during spraying. Both the polished and fractured cross-sectional microstructures of the coatings were characterised by SEM. The phase structures of the coatings and the feedstock were analysed by XRD. The microstructure and phase structure of the coatings prepared at different substrate temperatures were examined. SEM showed that the intersplat bonding within the coatings was improved by increasing the substrate temperature. The fracture toughness of the deposits was measured by indentation methods. For the coatings prepared at low substrate temperatures, the fracture toughness increased with the substrate temperature due to the improvement in the intersplat bonding. However, a significant decrease in the fracture toughness was found for the coatings prepared at high substrate temperatures. The change in phase structure of the coatings suggested that the residual tensile stress mainly resulted from phase transformation from gamma-alumina to alpha-alumina at high substrate temperatures was the reason for the decline in the fracture toughness. Alumina coatings were prepared by atmospheric plasma spraying through controlling the surface temperature of the coatings during spraying. Both the polished and fractured cross-section microstructures of the coatings were characterized by scanning electron microscopy (SEM). The phase structures of the coatings and the feedstock were analyzed by X-ray diffraction technique (XRD). The microstructure and phase structure of the coatings prepared at different substrate temperatures were examined. SEM observations show that the intersplat bonding within the coatings was significantly improved by increasing the substrate temperature. The fracture toughness of the deposits was measured by indentation methods. For the coatings prepared at low substrate temperatures, the fracture toughness increased with the substrate temperature due to the improvement in the intersplat bonding. However, a significant decrease in the fracture toughness was found for the coatings prepared at high substrate temperatures. The change in phase structure of the coatings suggested that the residual tensile stress mainly resulted from phase transformation from γ-alumina to α-alumina at high substrate temperature should answer for the decline in the fracture toughness. |
| Author | Hao, Jian-Min Xing, Ya-Zhe Wei, Qiu-Lan |
| Author_xml | – sequence: 1 givenname: Ya-Zhe surname: Xing fullname: Xing, Ya-Zhe email: xingyz@chd.edu.cn organization: School of Materials Science and Engineering, Chang’an University, Xi’an, Shaanxi 710064, China – sequence: 2 givenname: Qiu-Lan surname: Wei fullname: Wei, Qiu-Lan organization: Department of Automotive Engineering, Shaanxi College of Communication Technology, Xi’an, Shaanxi 710018, China – sequence: 3 givenname: Jian-Min surname: Hao fullname: Hao, Jian-Min organization: School of Materials Science and Engineering, Chang’an University, Xi’an, Shaanxi 710064, China |
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| Keywords | Phase transformation Plasma spraying Alumina Fracture toughness |
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| SubjectTerms | Alumina Aluminum oxide Atmospherics Bonding Coatings Fracture toughness Microstructure Phase transformation Plasma spraying Scanning electron microscopy Solid phases |
| Title | The fracture toughness of alumina coatings plasma-sprayed at different in situ temperatures |
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