Green surface modification and nano-multifunctionalization of denim fabric
Eco-friendly multifunctional denim products using environmentally sound technologies are still a challenge. In current study, enzymatic pretreatments of denim fabric using acid pectinases, laccases, and acid cellulases individually and in admixtures were carried out followed by post-nanocoating of b...
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| Published in | Cellulose (London) Vol. 25; no. 10; pp. 6207 - 6220 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Dordrecht
Springer Netherlands
01.10.2018
Springer Nature B.V |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0969-0239 1572-882X |
| DOI | 10.1007/s10570-018-1985-y |
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| Abstract | Eco-friendly multifunctional denim products using environmentally sound technologies are still a challenge. In current study, enzymatic pretreatments of denim fabric using acid pectinases, laccases, and acid cellulases individually and in admixtures were carried out followed by post-nanocoating of bio-treated fabric samples with ZnO- and TiO
2
-NPs along with citric acid/sodium hypophosphite as ester-crosslinking/binding system using the pad-dry-microwave fixation technique. The impacts of enzymatic and subsequent nano-treatments on some physico-chemical, color change, anti-microbial and UV-blocking properties were assessed. Also, surface modification and nano-metal oxides immobilization were observed and confirmed using scan electron microscope and energy dispersive X-ray spectroscopy analysis. The experimental results revealed that the degree of surface modification and subsequent multifunctionalization are governed by type of enzyme or hybrid enzyme as well as kind of nano-metal oxide and its extent of fixation onto the modified/ester-crosslinked denim fabric structure. The synergistic effect and positive impacts of enzymatic treatment followed by nanofinishing especially in case of using ZnO-NPs on imparting better and durable performance and multifunctional properties without adversely affecting the coloration properties of denim fabric samples are confirmed and discussed. Mode of interactions was also suggested.
Graphical abstract |
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| AbstractList | Eco-friendly multifunctional denim products using environmentally sound technologies are still a challenge. In current study, enzymatic pretreatments of denim fabric using acid pectinases, laccases, and acid cellulases individually and in admixtures were carried out followed by post-nanocoating of bio-treated fabric samples with ZnO- and TiO2-NPs along with citric acid/sodium hypophosphite as ester-crosslinking/binding system using the pad-dry-microwave fixation technique. The impacts of enzymatic and subsequent nano-treatments on some physico-chemical, color change, anti-microbial and UV-blocking properties were assessed. Also, surface modification and nano-metal oxides immobilization were observed and confirmed using scan electron microscope and energy dispersive X-ray spectroscopy analysis. The experimental results revealed that the degree of surface modification and subsequent multifunctionalization are governed by type of enzyme or hybrid enzyme as well as kind of nano-metal oxide and its extent of fixation onto the modified/ester-crosslinked denim fabric structure. The synergistic effect and positive impacts of enzymatic treatment followed by nanofinishing especially in case of using ZnO-NPs on imparting better and durable performance and multifunctional properties without adversely affecting the coloration properties of denim fabric samples are confirmed and discussed. Mode of interactions was also suggested.Graphical abstract Eco-friendly multifunctional denim products using environmentally sound technologies are still a challenge. In current study, enzymatic pretreatments of denim fabric using acid pectinases, laccases, and acid cellulases individually and in admixtures were carried out followed by post-nanocoating of bio-treated fabric samples with ZnO- and TiO 2 -NPs along with citric acid/sodium hypophosphite as ester-crosslinking/binding system using the pad-dry-microwave fixation technique. The impacts of enzymatic and subsequent nano-treatments on some physico-chemical, color change, anti-microbial and UV-blocking properties were assessed. Also, surface modification and nano-metal oxides immobilization were observed and confirmed using scan electron microscope and energy dispersive X-ray spectroscopy analysis. The experimental results revealed that the degree of surface modification and subsequent multifunctionalization are governed by type of enzyme or hybrid enzyme as well as kind of nano-metal oxide and its extent of fixation onto the modified/ester-crosslinked denim fabric structure. The synergistic effect and positive impacts of enzymatic treatment followed by nanofinishing especially in case of using ZnO-NPs on imparting better and durable performance and multifunctional properties without adversely affecting the coloration properties of denim fabric samples are confirmed and discussed. Mode of interactions was also suggested. Graphical abstract Eco-friendly multifunctional denim products using environmentally sound technologies are still a challenge. In current study, enzymatic pretreatments of denim fabric using acid pectinases, laccases, and acid cellulases individually and in admixtures were carried out followed by post-nanocoating of bio-treated fabric samples with ZnO- and TiO₂-NPs along with citric acid/sodium hypophosphite as ester-crosslinking/binding system using the pad-dry-microwave fixation technique. The impacts of enzymatic and subsequent nano-treatments on some physico-chemical, color change, anti-microbial and UV-blocking properties were assessed. Also, surface modification and nano-metal oxides immobilization were observed and confirmed using scan electron microscope and energy dispersive X-ray spectroscopy analysis. The experimental results revealed that the degree of surface modification and subsequent multifunctionalization are governed by type of enzyme or hybrid enzyme as well as kind of nano-metal oxide and its extent of fixation onto the modified/ester-crosslinked denim fabric structure. The synergistic effect and positive impacts of enzymatic treatment followed by nanofinishing especially in case of using ZnO-NPs on imparting better and durable performance and multifunctional properties without adversely affecting the coloration properties of denim fabric samples are confirmed and discussed. Mode of interactions was also suggested. |
| Author | Eid, Basma M. Ibrahim, Nabil A. Abdel Aziz, Mohamed S. Hamdy, Soha M. Abd Allah, Safaa E. |
| Author_xml | – sequence: 1 givenname: Nabil A. orcidid: 0000-0002-8531-9461 surname: Ibrahim fullname: Ibrahim, Nabil A. email: nabibrahim49@yahoo.co.uk organization: Textile Research Division, National Research Centre – sequence: 2 givenname: Basma M. surname: Eid fullname: Eid, Basma M. organization: Textile Research Division, National Research Centre – sequence: 3 givenname: Mohamed S. surname: Abdel Aziz fullname: Abdel Aziz, Mohamed S. organization: Microbial Chemistry Department, National Research Center – sequence: 4 givenname: Soha M. surname: Hamdy fullname: Hamdy, Soha M. organization: Chemistry Department, Faculty of Science, Fayoum University – sequence: 5 givenname: Safaa E. surname: Abd Allah fullname: Abd Allah, Safaa E. organization: Textile Research Division, National Research Centre |
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| Keywords | Denim fabric Multifunctional properties Nano-coating Potential applications Bio-processing |
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| SubjectTerms | Admixtures Antiinfectives and antibacterials Bioorganic Chemistry cellulases cellulose Ceramics Chemistry Chemistry and Materials Science Citric acid color Composites Crosslinking Denim Energy dispersive X ray spectroscopy energy-dispersive X-ray analysis enzymatic treatment Enzymes Fabric structures Fixation Glass laccase Metal oxides Microorganisms Natural Materials Organic Chemistry Original Paper Pectinase Physical Chemistry Polymer Sciences Properties (attributes) sodium Sustainable Development sustainable technology synergism Synergistic effect Titanium dioxide Zinc oxide |
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