Nickel coated on beech wood by electroless nickel coating: effects of complexing agent concentrations on nickel film properties
In order to obtain beech wood substrates with new functions as conductive materials and to develop their utilities in industrial fields, the technique of electroless nickel coating on the beech wood substrate was employed. The influence of complexing agent concentration [Na 2 EDTA·2H 2 O] on the nic...
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Published in | Composite interfaces Vol. 21; no. 8; pp. 659 - 669 |
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Main Authors | , |
Format | Journal Article |
Language | English |
Published |
Taylor & Francis
01.01.2014
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Abstract | In order to obtain beech wood substrates with new functions as conductive materials and to develop their utilities in industrial fields, the technique of electroless nickel coating on the beech wood substrate was employed. The influence of complexing agent concentration [Na
2
EDTA·2H
2
O] on the nickel surface resistivity was studied. The process conditions were Ni(CH
3
COO)
2
·4H
2
O 0.103 mol/L, CH
3
CHOCOOH 18.18 mL/L, N
2
H
5
OH 54.54 mL/L, NaOH 0.193 mol/L, pH value of 9.5, temperature of 75 °C, and the complexing agent concentration varied between 0.012 and 0.061 mol/L. By means of XRD, EDXRF, and SEM, the chemical composition and morphology of the prepared films were investigated. The results showed that when the complexing agent concentration increased from 0.012 to 0.061 mol/L in the electroless nickel coating baths, the gained nickel mass on the beech wood substrate decreased from 17.04 to 9.03 mg/cm
2
, the nickel crystallite sizes reduced from 16.1 to 1.41 nm and the electric measurements demonstrated that the nickel surface resistivity rose from 0.004 to 192.16 kΩ/cm
2
. |
---|---|
AbstractList | In order to obtain beech wood substrates with new functions as conductive materials and to develop their utilities in industrial fields, the technique of electroless nickel coating on the beech wood substrate was employed. The influence of complexing agent concentration [Na
2
EDTA·2H
2
O] on the nickel surface resistivity was studied. The process conditions were Ni(CH
3
COO)
2
·4H
2
O 0.103 mol/L, CH
3
CHOCOOH 18.18 mL/L, N
2
H
5
OH 54.54 mL/L, NaOH 0.193 mol/L, pH value of 9.5, temperature of 75 °C, and the complexing agent concentration varied between 0.012 and 0.061 mol/L. By means of XRD, EDXRF, and SEM, the chemical composition and morphology of the prepared films were investigated. The results showed that when the complexing agent concentration increased from 0.012 to 0.061 mol/L in the electroless nickel coating baths, the gained nickel mass on the beech wood substrate decreased from 17.04 to 9.03 mg/cm
2
, the nickel crystallite sizes reduced from 16.1 to 1.41 nm and the electric measurements demonstrated that the nickel surface resistivity rose from 0.004 to 192.16 kΩ/cm
2
. |
Author | Amer, Jamal Al-Khawaja, Sameer |
Author_xml | – sequence: 1 givenname: Jamal surname: Amer fullname: Amer, Jamal email: cscientific@aec.org.sy organization: Department of Chemistry, Atomic Energy Commission of Syria – sequence: 2 givenname: Sameer surname: Al-Khawaja fullname: Al-Khawaja, Sameer organization: Department of Physics, Atomic Energy Commission of Syria |
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CitedBy_id | crossref_primary_10_1016_j_ijhydene_2015_08_017 crossref_primary_10_1080_03067319_2021_1984443 crossref_primary_10_1080_09276440_2021_1913899 crossref_primary_10_3390_ma16114101 crossref_primary_10_1002_sia_6034 |
Cites_doi | 10.1016/j.surfcoat.2009.10.032 10.1021/cm034554n 10.1016/j.surfcoat.2006.03.023 10.1080/15685543.2014.854615 10.1016/j.surfcoat.2005.04.021 10.1007/BF02856822 10.1007/s00226-010-0303-0 10.1023/A:1004161707536 10.1023/A:1009692232398 10.1016/j.apsusc.2010.08.060 10.1016/S0257-8972(98)00553-2 10.4028/www.scientific.net/AMR.183-185.1563 10.1016/j.proeng.2011.11.2533 10.1007/s11676-006-0013-5 10.1016/j.jallcom.2013.03.107 10.1016/S0254-0584(02)00101-3 10.1016/j.materresbull.2012.04.146 10.1007/s00226-012-0466-y |
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Title | Nickel coated on beech wood by electroless nickel coating: effects of complexing agent concentrations on nickel film properties |
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