Relationship between the physicochemical properties of sludge-based carbons and the adsorption capacity of dissolved organic matter in advanced wastewater treatment: Effects of chemical conditioning

Pyrolysis carbonisation is a promising technology to convert organic waste into valuable carbon-based materials. However, sludge is generally highly compressible and difficult to dewater because of its high concentrations of biopolymers; the bound water of sludge is trapped in a network composed of...

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Published inChemosphere (Oxford) Vol. 243; p. 125333
Main Authors Li, Lanfeng, Ai, Jing, Zhang, Weijun, Peng, Sainan, Dong, Tianyi, Deng, Yun, Cui, Yanping, Wang, Dongsheng
Format Journal Article
LanguageEnglish
Published England Elsevier Ltd 01.03.2020
Subjects
Adsorption
Biopolymers
Carbon
Chemical conditioning
DOMs fractionation
Ferric Compounds
Flocculation
Hydrogen Peroxide
Hydrogen-Ion Concentration
Iron
Organic Chemicals
Pyrolysis
Sewage - chemistry
Sludge-based carbons
Waste Disposal, Fluid - methods
Waste Water
Water - chemistry
Pyrolysis
Sludge-based carbons
DOMs fractionation
Adsorption
Chemical conditioning
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Abstract Pyrolysis carbonisation is a promising technology to convert organic waste into valuable carbon-based materials. However, sludge is generally highly compressible and difficult to dewater because of its high concentrations of biopolymers; the bound water of sludge is trapped in a network composed of biopolymers. Therefore, chemical conditioning is an indispensable step for improving sludge dewaterability performance. In the present work, the effects of different chemical conditioning agents (polymeric aluminium chloride (PACl), iron(III) chloride (FeCl3), KMnO4–Fe(II) and Fenton’s reagent) on the physicochemical properties of sludge-based carbons (SBCs) were systematically studied and the SBCs were further used in advanced wastewater treatment. The adsorption mechanisms of dissolved organic matters (DOMs) by different SBCs were also investigated. The results showed that conditioning with KMnO4–Fe(II) and Fenton’s reagent improved the specific surface area of the SBCs, whereas inorganic salt flocculation conditioning reduced the porosity of the SBCs. In addition, we found that the Fenton-SBC and Mn/Fe-SBC performed better than the other investigated SBCs in the removal of organic compounds from secondary effluent and that the pseudo-second-order kinetic model could better describe the process of DOMs adsorption by all of the investigated SBCs. Moreover, three-dimensional fluorescence excitation–emission matrix spectroscopy in combination with an analysis of the physical and chemical fractionation of DOMs showed that all of the SBCs performed well in the adsorption of aromatic substances, hydrophobic acids and hydrophobic neutrals, whereas the Mn/Fe-SBC and Fenton-SBC performed better than the other SBCs in the removal of weakly hydrophobic acids. [Display omitted] •Fenton’s reagent and KMnO4–Fe(II) conditioning improved porosity of SBCs.•Fenton-SBC and Mn/Fe-SBC performed better in DOMs removal.•SBCs were effective in removing aromatic and high molecular weight of substances.•Pore structure and carbon content affected the adsorption capacities of SBCs.
AbstractList Pyrolysis carbonisation is a promising technology to convert organic waste into valuable carbon-based materials. However, sludge is generally highly compressible and difficult to dewater because of its high concentrations of biopolymers; the bound water of sludge is trapped in a network composed of biopolymers. Therefore, chemical conditioning is an indispensable step for improving sludge dewaterability performance. In the present work, the effects of different chemical conditioning agents (polymeric aluminium chloride (PACl), iron(III) chloride (FeCl ), KMnO -Fe(II) and Fenton's reagent) on the physicochemical properties of sludge-based carbons (SBCs) were systematically studied and the SBCs were further used in advanced wastewater treatment. The adsorption mechanisms of dissolved organic matters (DOMs) by different SBCs were also investigated. The results showed that conditioning with KMnO -Fe(II) and Fenton's reagent improved the specific surface area of the SBCs, whereas inorganic salt flocculation conditioning reduced the porosity of the SBCs. In addition, we found that the Fenton-SBC and Mn/Fe-SBC performed better than the other investigated SBCs in the removal of organic compounds from secondary effluent and that the pseudo-second-order kinetic model could better describe the process of DOMs adsorption by all of the investigated SBCs. Moreover, three-dimensional fluorescence excitation-emission matrix spectroscopy in combination with an analysis of the physical and chemical fractionation of DOMs showed that all of the SBCs performed well in the adsorption of aromatic substances, hydrophobic acids and hydrophobic neutrals, whereas the Mn/Fe-SBC and Fenton-SBC performed better than the other SBCs in the removal of weakly hydrophobic acids.
Pyrolysis carbonisation is a promising technology to convert organic waste into valuable carbon-based materials. However, sludge is generally highly compressible and difficult to dewater because of its high concentrations of biopolymers; the bound water of sludge is trapped in a network composed of biopolymers. Therefore, chemical conditioning is an indispensable step for improving sludge dewaterability performance. In the present work, the effects of different chemical conditioning agents (polymeric aluminium chloride (PACl), iron(III) chloride (FeCl3), KMnO4–Fe(II) and Fenton’s reagent) on the physicochemical properties of sludge-based carbons (SBCs) were systematically studied and the SBCs were further used in advanced wastewater treatment. The adsorption mechanisms of dissolved organic matters (DOMs) by different SBCs were also investigated. The results showed that conditioning with KMnO4–Fe(II) and Fenton’s reagent improved the specific surface area of the SBCs, whereas inorganic salt flocculation conditioning reduced the porosity of the SBCs. In addition, we found that the Fenton-SBC and Mn/Fe-SBC performed better than the other investigated SBCs in the removal of organic compounds from secondary effluent and that the pseudo-second-order kinetic model could better describe the process of DOMs adsorption by all of the investigated SBCs. Moreover, three-dimensional fluorescence excitation–emission matrix spectroscopy in combination with an analysis of the physical and chemical fractionation of DOMs showed that all of the SBCs performed well in the adsorption of aromatic substances, hydrophobic acids and hydrophobic neutrals, whereas the Mn/Fe-SBC and Fenton-SBC performed better than the other SBCs in the removal of weakly hydrophobic acids. [Display omitted] •Fenton’s reagent and KMnO4–Fe(II) conditioning improved porosity of SBCs.•Fenton-SBC and Mn/Fe-SBC performed better in DOMs removal.•SBCs were effective in removing aromatic and high molecular weight of substances.•Pore structure and carbon content affected the adsorption capacities of SBCs.
ArticleNumber 125333
Author Ai, Jing
Dong, Tianyi
Cui, Yanping
Zhang, Weijun
Deng, Yun
Peng, Sainan
Li, Lanfeng
Wang, Dongsheng
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Keywords Pyrolysis
Sludge-based carbons
DOMs fractionation
Adsorption
Chemical conditioning
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Snippet Pyrolysis carbonisation is a promising technology to convert organic waste into valuable carbon-based materials. However, sludge is generally highly...
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StartPage 125333
SubjectTerms Adsorption
Biopolymers
Carbon
Chemical conditioning
DOMs fractionation
Ferric Compounds
Flocculation
Hydrogen Peroxide
Hydrogen-Ion Concentration
Iron
Organic Chemicals
Pyrolysis
Sewage - chemistry
Sludge-based carbons
Waste Disposal, Fluid - methods
Waste Water
Water - chemistry
Title Relationship between the physicochemical properties of sludge-based carbons and the adsorption capacity of dissolved organic matter in advanced wastewater treatment: Effects of chemical conditioning
URI https://dx.doi.org/10.1016/j.chemosphere.2019.125333
https://www.ncbi.nlm.nih.gov/pubmed/31734596
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