Synthesis of reduced graphene oxide nanoscrolls embedded in polypyrrole matrix for supercapacitor applications

[Display omitted] •Reduced graphene oxide nanoscrolls have been synthesized in the presence of pyrrole, under acidic medium.•Reduced graphene oxide nanoscrolls embedded polypyrrole thin films have been fabricated in the presence of sulphuric acid and ammonium persulfate.•Samples have been characteri...

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Published inSynthetic metals Vol. 227; pp. 21 - 28
Main Authors Atri, Priyanka, Tiwari, Dinesh Chandra, Sharma, Rishi
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 01.05.2017
Elsevier BV
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Abstract [Display omitted] •Reduced graphene oxide nanoscrolls have been synthesized in the presence of pyrrole, under acidic medium.•Reduced graphene oxide nanoscrolls embedded polypyrrole thin films have been fabricated in the presence of sulphuric acid and ammonium persulfate.•Samples have been characterized by FESEM, TEM, FTIR, UV–vis, Raman and TGA analysis.•The synthesized thin films of reduced graphene oxide nanoscrolls embedded polypyrrole have been used for supercapacitor applications.•Supercapacitor electrode shows good cyclic stability by retaining 88% of the specific capacitance even after 200 cycles. Reduced graphene oxide (rGO) nanoscrolls are synthesized in the presence of pyrrole (Py) by using oxidative polymerization method in the presence of sulphuric acid and ammonium persulfate. We report a simple method for the synthesis of rGO nanoscrolls in the presence of pyrrole, and this composite material is used for the supercapacitor applications. Supercapacitor electrodes show good cyclic stability by retaining 88% of the specific capacitance even after 200 cycles. Polypyrrole – reduced graphene oxide (PPy-rGO nanoscrolls) is characterized by Raman, TEM, FESEM, EDX, FTIR, TGA and UV–vis spectroscopy techniques.
AbstractList [Display omitted] •Reduced graphene oxide nanoscrolls have been synthesized in the presence of pyrrole, under acidic medium.•Reduced graphene oxide nanoscrolls embedded polypyrrole thin films have been fabricated in the presence of sulphuric acid and ammonium persulfate.•Samples have been characterized by FESEM, TEM, FTIR, UV–vis, Raman and TGA analysis.•The synthesized thin films of reduced graphene oxide nanoscrolls embedded polypyrrole have been used for supercapacitor applications.•Supercapacitor electrode shows good cyclic stability by retaining 88% of the specific capacitance even after 200 cycles. Reduced graphene oxide (rGO) nanoscrolls are synthesized in the presence of pyrrole (Py) by using oxidative polymerization method in the presence of sulphuric acid and ammonium persulfate. We report a simple method for the synthesis of rGO nanoscrolls in the presence of pyrrole, and this composite material is used for the supercapacitor applications. Supercapacitor electrodes show good cyclic stability by retaining 88% of the specific capacitance even after 200 cycles. Polypyrrole – reduced graphene oxide (PPy-rGO nanoscrolls) is characterized by Raman, TEM, FESEM, EDX, FTIR, TGA and UV–vis spectroscopy techniques.
Reduced graphene oxide (rGO) nanoscrolls are synthesized in the presence of pyrrole (Py) by using oxidative polymerization method in the presence of sulphuric acid and ammonium persulfate. We report a simple method for the synthesis of rGO nanoscrolls in the presence of pyrrole, and this composite material is used for the supercapacitor applications. Supercapacitor electrodes show good cyclic stability by retaining 88% of the specific capacitance even after 200 cycles. Polypyrrole-reduced graphene oxide (PPy-rGO nanoscrolls) is characterized by Raman, TEM, FESEM, EDX, FTIR, TGA and UV-vis spectroscopy techniques.
Author Tiwari, Dinesh Chandra
Sharma, Rishi
Atri, Priyanka
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  givenname: Dinesh Chandra
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  organization: MEMS and Microsensors Group, CSIR-Central Electronics Engineering Research Institute (CEERI), Pilani 333031, Raj., India, India
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Graphene nanoscrolls
Polypyrrole
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Snippet [Display omitted] •Reduced graphene oxide nanoscrolls have been synthesized in the presence of pyrrole, under acidic medium.•Reduced graphene oxide nanoscrolls...
Reduced graphene oxide (rGO) nanoscrolls are synthesized in the presence of pyrrole (Py) by using oxidative polymerization method in the presence of sulphuric...
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SubjectTerms Ammonium peroxodisulfate
Chemical synthesis
Composite materials
Electrodes
Fourier transforms
Graphene
Graphene nanoscrolls
Polymerization
Polypyrrole
Spectrum analysis
Sulfuric acid
Supercapacitor
Supercapacitors
Title Synthesis of reduced graphene oxide nanoscrolls embedded in polypyrrole matrix for supercapacitor applications
URI https://dx.doi.org/10.1016/j.synthmet.2017.03.002
https://www.proquest.com/docview/1954364449
Volume 227
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