Synthesis and characterization of poly(hydroxyethyl methacrylate- N-methacryloyl-( l)-glutamic acid) copolymer beads for removal of lead ions

N-methacryloyl-( l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or comonomer. MAGA was characterized by FTIR and NMR. Spherical beads with an average diameter of 150–200 μm were obtained by suspension polymerizati...

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Published inMaterials Science & Engineering C Vol. 25; no. 4; pp. 448 - 454
Main Authors Denizli, Adil, Garipcan, Bora, Karabakan, Abdülkerim, Senöz, Hülya
Format Journal Article
LanguageEnglish
Published Elsevier B.V 01.06.2005
Subjects
Glutamic acid
Lead removal
Metal-chelating beads
Metal-chelating beads
Lead removal
Glutamic acid
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Abstract N-methacryloyl-( l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or comonomer. MAGA was characterized by FTIR and NMR. Spherical beads with an average diameter of 150–200 μm were obtained by suspension polymerization of MAGA and 2-hydroxyethyl methacrylate (HEMA) performed in an aqueous dispersion medium. Poly(HEMA-MAGA) beads were characterized by swelling studies, surface area measurements and elemental analysis. Poly(HEMA-MAGA) beads have a specific surface area of 56.7 m 2/g. Poly(HEMA-MAGA) beads were used in the removal studies of Pb 2+ ions. Adsorption equilibrium was achieved in about 60 min. The adsorption of Pb 2+ ions onto PHEMA beads was negligible (0.38 mg/g). The MAGA incorporation into the polymer structure significantly increased the lead adsorption capacity (348 mg/g). The adsorption of Pb 2+ ions increased with increasing pH and reached a plateau value at around pH 5.0. Competitive adsorption of heavy metal ions from synthetic wastewater was also studied. The adsorption capacities are 42.5 mg/g for Pb 2+, 26.8 mg/g for Hg 2+ and 17.6 mg/g for Cd 2+ at 0.5 mmol/l metal concentration. Consecutive adsorption and elution operations showed the feasibility of repeated use for poly(HEMA-MAGA) chelating beads.
AbstractList N-methacryloyl-(l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or comonomer. MAGA was characterized by FTIR and NMR. Spherical beads with an average diameter of 150-200 mu m were obtained by suspension polymerization of MAGA and 2-hydroxyethyl methacrylate (HEMA) performed in an aqueous dispersion medium. Poly(HEMA-MAGA) beads were characterized by swelling studies, surface area measurements and elemental analysis. Poly(HEMA-MAGA) beads have a specific surface area of 56.7 m super(2)/g. Poly(HEMA-MAGA) beads were used in the removal studies of Pb super(2+) ions. Adsorption equilibrium was achieved in about 60 min. The adsorption of Pb super(2+) ions onto PHEMA beads was negligible (0.38 mg/g). The MAGA incorporation into the polymer structure significantly increased the lead adsorption capacity (348 mg/g). The adsorption of Pb super(2+) ions increased with increasing pH and reached a plateau value at around pH 5.0. Competitive adsorption of heavy metal ions from synthetic wastewater was also studied. The adsorption capacities are 42.5 mg/g for Pb super(2+), 26.8 mg/g for Hg super(2+) and 17.6 mg/g for Cd super(2+) at 0.5 mmol/l metal concentration. Consecutive adsorption and elution operations showed the feasibility of repeated use for poly(HEMA-MAGA) chelating beads.
N-methacryloyl-( l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or comonomer. MAGA was characterized by FTIR and NMR. Spherical beads with an average diameter of 150–200 μm were obtained by suspension polymerization of MAGA and 2-hydroxyethyl methacrylate (HEMA) performed in an aqueous dispersion medium. Poly(HEMA-MAGA) beads were characterized by swelling studies, surface area measurements and elemental analysis. Poly(HEMA-MAGA) beads have a specific surface area of 56.7 m 2/g. Poly(HEMA-MAGA) beads were used in the removal studies of Pb 2+ ions. Adsorption equilibrium was achieved in about 60 min. The adsorption of Pb 2+ ions onto PHEMA beads was negligible (0.38 mg/g). The MAGA incorporation into the polymer structure significantly increased the lead adsorption capacity (348 mg/g). The adsorption of Pb 2+ ions increased with increasing pH and reached a plateau value at around pH 5.0. Competitive adsorption of heavy metal ions from synthetic wastewater was also studied. The adsorption capacities are 42.5 mg/g for Pb 2+, 26.8 mg/g for Hg 2+ and 17.6 mg/g for Cd 2+ at 0.5 mmol/l metal concentration. Consecutive adsorption and elution operations showed the feasibility of repeated use for poly(HEMA-MAGA) chelating beads.
Author Garipcan, Bora
Denizli, Adil
Karabakan, Abdülkerim
Senöz, Hülya
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Lead removal
Glutamic acid
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Snippet N-methacryloyl-( l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or...
N-methacryloyl-(l)-glutamic acid (MAGA) was synthesized using methacryloyl chloride and l-glutamic acid methyl ester as a metal-complexing ligand and/or...
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SubjectTerms Glutamic acid
Lead removal
Metal-chelating beads
Title Synthesis and characterization of poly(hydroxyethyl methacrylate- N-methacryloyl-( l)-glutamic acid) copolymer beads for removal of lead ions
URI https://dx.doi.org/10.1016/j.msec.2004.12.001
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