Edge-enriched MoS2 nanosheets modified porous nanosheet-assembled hierarchical In2O3 microflowers for room temperature detection of NO2 with ultrahigh sensitivity and selectivity

Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO2 sensors. Herein, the edge-enriched MoS2 nanosheets modified porous nanoshee...

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Published inJournal of hazardous materials Vol. 434; p. 128836
Main Authors Zhang, Yajie, Jiang, Yadong, Duan, Zaihua, Wu, Yingwei, Zhao, Qiuni, Liu, Bohao, Huang, Qi, Yuan, Zhen, Li, Xian, Tai, Huiling
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.07.2022
Subjects
ambient temperature
Edge activity
Heterojunction
High selectivity
human health
In2O3/MoS2
nanosheets
nitrogen dioxide
NO2 sensor
synergism
toxicity
NO2 sensor
High selectivity
In2O3/MoS2
Edge activity
Heterojunction
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Abstract Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO2 sensors. Herein, the edge-enriched MoS2 nanosheets modified porous nanosheets-assembled three-dimensional (3D) In2O3 microflowers have been synthesized to improve the sensitivity and selectivity of NO2 detection at RT. The results show that the In2O3/MoS2 composite sensor exhibits a response as high as 343.09–5 ppm NO2, which is 309 and 72.5 times higher than the sensors based on the pristine MoS2 and In2O3. The composite sensor also shows short recovery time (37 s), excellent repeatability and long-term stability. Furthermore, the response of the In2O3/MoS2 sensor to NO2 is at least 30 times higher than that of other gases, proving the ultrahigh selectivity of the sensor. The outstanding sensing performance of the In2O3/MoS2 sensor can be attributed to the synergistic effect and abundant active sites originating from the p-n heterojunction, exposed edge structures and the designed 2D/3D hybrid structure. The strategy proposed herein is expected to provide a useful reference for the development of high-performance RT NO2 sensors. [Display omitted] •3D porous hierarchical In2O3/MoS2 microflowers were prepared via mechanical mixing.•The In2O3/MoS2 sensor exhibited a response as high as 343.09–5 ppm NO2 at RT.•The In2O3/MoS2 sensor showed short recovery time and ultrahigh selectivity to NO2.•The enhanced properties are due to the n-p heterojunction and increased active sites.
AbstractList Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO2 sensors. Herein, the edge-enriched MoS2 nanosheets modified porous nanosheets-assembled three-dimensional (3D) In2O3 microflowers have been synthesized to improve the sensitivity and selectivity of NO2 detection at RT. The results show that the In2O3/MoS2 composite sensor exhibits a response as high as 343.09-5 ppm NO2, which is 309 and 72.5 times higher than the sensors based on the pristine MoS2 and In2O3. The composite sensor also shows short recovery time (37 s), excellent repeatability and long-term stability. Furthermore, the response of the In2O3/MoS2 sensor to NO2 is at least 30 times higher than that of other gases, proving the ultrahigh selectivity of the sensor. The outstanding sensing performance of the In2O3/MoS2 sensor can be attributed to the synergistic effect and abundant active sites originating from the p-n heterojunction, exposed edge structures and the designed 2D/3D hybrid structure. The strategy proposed herein is expected to provide a useful reference for the development of high-performance RT NO2 sensors.Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO2 sensors. Herein, the edge-enriched MoS2 nanosheets modified porous nanosheets-assembled three-dimensional (3D) In2O3 microflowers have been synthesized to improve the sensitivity and selectivity of NO2 detection at RT. The results show that the In2O3/MoS2 composite sensor exhibits a response as high as 343.09-5 ppm NO2, which is 309 and 72.5 times higher than the sensors based on the pristine MoS2 and In2O3. The composite sensor also shows short recovery time (37 s), excellent repeatability and long-term stability. Furthermore, the response of the In2O3/MoS2 sensor to NO2 is at least 30 times higher than that of other gases, proving the ultrahigh selectivity of the sensor. The outstanding sensing performance of the In2O3/MoS2 sensor can be attributed to the synergistic effect and abundant active sites originating from the p-n heterojunction, exposed edge structures and the designed 2D/3D hybrid structure. The strategy proposed herein is expected to provide a useful reference for the development of high-performance RT NO2 sensors.
Nitrogen dioxide (NO₂) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO₂ sensors. Herein, the edge-enriched MoS₂ nanosheets modified porous nanosheets-assembled three-dimensional (3D) In₂O₃ microflowers have been synthesized to improve the sensitivity and selectivity of NO₂ detection at RT. The results show that the In₂O₃/MoS₂ composite sensor exhibits a response as high as 343.09–5 ppm NO₂, which is 309 and 72.5 times higher than the sensors based on the pristine MoS₂ and In₂O₃. The composite sensor also shows short recovery time (37 s), excellent repeatability and long-term stability. Furthermore, the response of the In₂O₃/MoS₂ sensor to NO₂ is at least 30 times higher than that of other gases, proving the ultrahigh selectivity of the sensor. The outstanding sensing performance of the In₂O₃/MoS₂ sensor can be attributed to the synergistic effect and abundant active sites originating from the p-n heterojunction, exposed edge structures and the designed 2D/3D hybrid structure. The strategy proposed herein is expected to provide a useful reference for the development of high-performance RT NO₂ sensors.
Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor selectivity at room temperature (RT) restrain the application of NO2 sensors. Herein, the edge-enriched MoS2 nanosheets modified porous nanosheets-assembled three-dimensional (3D) In2O3 microflowers have been synthesized to improve the sensitivity and selectivity of NO2 detection at RT. The results show that the In2O3/MoS2 composite sensor exhibits a response as high as 343.09–5 ppm NO2, which is 309 and 72.5 times higher than the sensors based on the pristine MoS2 and In2O3. The composite sensor also shows short recovery time (37 s), excellent repeatability and long-term stability. Furthermore, the response of the In2O3/MoS2 sensor to NO2 is at least 30 times higher than that of other gases, proving the ultrahigh selectivity of the sensor. The outstanding sensing performance of the In2O3/MoS2 sensor can be attributed to the synergistic effect and abundant active sites originating from the p-n heterojunction, exposed edge structures and the designed 2D/3D hybrid structure. The strategy proposed herein is expected to provide a useful reference for the development of high-performance RT NO2 sensors. [Display omitted] •3D porous hierarchical In2O3/MoS2 microflowers were prepared via mechanical mixing.•The In2O3/MoS2 sensor exhibited a response as high as 343.09–5 ppm NO2 at RT.•The In2O3/MoS2 sensor showed short recovery time and ultrahigh selectivity to NO2.•The enhanced properties are due to the n-p heterojunction and increased active sites.
ArticleNumber 128836
Author Huang, Qi
Yuan, Zhen
Liu, Bohao
Li, Xian
Jiang, Yadong
Wu, Yingwei
Zhao, Qiuni
Zhang, Yajie
Duan, Zaihua
Tai, Huiling
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  surname: Jiang
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  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
– sequence: 3
  givenname: Zaihua
  surname: Duan
  fullname: Duan, Zaihua
  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
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  surname: Wu
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  surname: Zhao
  fullname: Zhao, Qiuni
  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
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  surname: Liu
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  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
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  surname: Huang
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  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
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  surname: Yuan
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  surname: Tai
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  email: taitai1980@uestc.edu.cn
  organization: State Key Laboratory of Electronic Thin Films and Integrated Devices, School of Optoelectronic Science and Engineering, University of Electronic Science and Technology of China (UESTC), Chengdu 610054, PR China
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Keywords NO2 sensor
High selectivity
In2O3/MoS2
Edge activity
Heterojunction
Language English
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crossref_citationtrail_10_1016_j_jhazmat_2022_128836
elsevier_sciencedirect_doi_10_1016_j_jhazmat_2022_128836
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  year: 2022
  text: 2022-07-15
  day: 15
PublicationDecade 2020
PublicationTitle Journal of hazardous materials
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Snippet Nitrogen dioxide (NO2) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor...
Nitrogen dioxide (NO₂) is one of the most hazardous toxic pollutants to human health and the environment. However, deficiencies of low sensitivity and poor...
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SubjectTerms ambient temperature
Edge activity
Heterojunction
High selectivity
human health
In2O3/MoS2
nanosheets
nitrogen dioxide
NO2 sensor
synergism
toxicity
Title Edge-enriched MoS2 nanosheets modified porous nanosheet-assembled hierarchical In2O3 microflowers for room temperature detection of NO2 with ultrahigh sensitivity and selectivity
URI https://dx.doi.org/10.1016/j.jhazmat.2022.128836
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