Synthesis and characterization of novel waterborne polyurethane nanocomposites with magnetic and electrical properties
The novel nanocomposites derived from waterborne polyurethane and nano-Fe3O4 (WPU/Fe3O4) have been successfully synthesized by in situ polymerization progress. The nano-Fe3O4 particles prepared by co-precipitation method were modified by using oleic acid (OA) to improve their compatibility with mono...
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| Published in | Composites. Part A, Applied science and manufacturing Vol. 55; pp. 94 - 101 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Kidlington
Elsevier Ltd
01.12.2013
Elsevier |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The novel nanocomposites derived from waterborne polyurethane and nano-Fe3O4 (WPU/Fe3O4) have been successfully synthesized by in situ polymerization progress. The nano-Fe3O4 particles prepared by co-precipitation method were modified by using oleic acid (OA) to improve their compatibility with monomers. The chemical structures, morphology, thermal behavior, mechanical properties, magnetic properties and electrical properties of the WPU/Fe3O4 nanocomposites were investigated by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray diffraction (XRD), atomic force microscope (AFM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), dynamic mechanical thermal analysis (DMA), vibrating sample magnetometer (VSM) and high resistance meter respectively. The results indicated that the Fe3O4 nanoparticles modified by oleic acid could be homogeneously dispersed in the WPU and the introduction of ones was obviously improving the thermal properties, magnetic properties and electrical properties of WPU/Fe3O4 nanocomposites. The resulting WPU/Fe3O4 nanocomposites would be having the potential applications in microwave absorption. |
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| AbstractList | The novel nanocomposites derived from waterborne polyurethane and nano-Fe3O4 (WPU/Fe3O4) have been successfully synthesized by in situ polymerization progress. The nano-Fe3O4 particles prepared by co-precipitation method were modified by using oleic acid (OA) to improve their compatibility with monomers. The chemical structures, morphology, thermal behavior, mechanical properties, magnetic properties and electrical properties of the WPU/Fe3O4 nanocomposites were investigated by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray diffraction (XRD), atomic force microscope (AFM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), dynamic mechanical thermal analysis (DMA), vibrating sample magnetometer (VSM) and high resistance meter respectively. The results indicated that the Fe3O4 nanoparticles modified by oleic acid could be homogeneously dispersed in the WPU and the introduction of ones was obviously improving the thermal properties, magnetic properties and electrical properties of WPU/Fe3O4 nanocomposites. The resulting WPU/Fe3O4 nanocomposites would be having the potential applications in microwave absorption. The novel nanocomposites derived from waterborne polyurethane and nano-Fe₃O₄ (WPU/Fe₃O₄) have been successfully synthesized by in situ polymerization progress. The nano-Fe₃O₄ particles prepared by co-precipitation method were modified by using oleic acid (OA) to improve their compatibility with monomers. The chemical structures, morphology, thermal behavior, mechanical properties, magnetic properties and electrical properties of the WPU/Fe₃O₄ nanocomposites were investigated by Fourier transform infrared spectroscopy (FT-IR), scanning electron microscopy (SEM), X-ray diffraction (XRD), atomic force microscope (AFM), thermogravimetric analysis (TGA), differential scanning calorimetry (DSC), dynamic mechanical thermal analysis (DMA), vibrating sample magnetometer (VSM) and high resistance meter respectively. The results indicated that the Fe₃O₄ nanoparticles modified by oleic acid could be homogeneously dispersed in the WPU and the introduction of ones was obviously improving the thermal properties, magnetic properties and electrical properties of WPU/Fe₃O₄ nanocomposites. The resulting WPU/Fe₃O₄ nanocomposites would be having the potential applications in microwave absorption. |
| Author | Chen, Suli Li, Quanfang Hou, Ke Peng, Lanqin Zhang, Sidi Li, Yanfeng |
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| Keywords | B. Electrical properties A. Polymer–matrix composites (PMCs) B. Magnetic properties A. Particle-reinforcement Electrical conductivity Iron oxide Electrical properties A. Polymer―matrix composites (PMCs) Mechanical properties Dispersion reinforced material Experimental study Polyaddition Thermal stability Surface treatment Thermal properties Microwave absorption Magnetic material Oleic acid Morphology Preparation Polyurethane Nanocomposite Aqueous dispersion Magnetic properties |
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| Snippet | The novel nanocomposites derived from waterborne polyurethane and nano-Fe3O4 (WPU/Fe3O4) have been successfully synthesized by in situ polymerization progress.... The novel nanocomposites derived from waterborne polyurethane and nano-Fe₃O₄ (WPU/Fe₃O₄) have been successfully synthesized by in situ polymerization progress.... |
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| SubjectTerms | A. Particle-reinforcement A. Polymer–matrix composites (PMCs) absorption Applied sciences B. Electrical properties B. Magnetic properties chemical structure Composites coprecipitation differential scanning calorimetry electrical properties Exact sciences and technology Forms of application and semi-finished materials Fourier transform infrared spectroscopy iron oxides magnetic properties mechanical properties nanocomposites nanoparticles oleic acid particles Polymer industry, paints, wood polymerization polyurethanes scanning electron microscopy Technology of polymers thermal analysis thermal properties thermogravimetry X-ray diffraction |
| Title | Synthesis and characterization of novel waterborne polyurethane nanocomposites with magnetic and electrical properties |
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