Synthesis of sinteractive single-phase microstructure yttrium disilicate precursor powder using hydrothermal processing
This paper is the first report of the synthesis of a sinteractive single-phase microstructure yttrium disilicate precursor powder using hydrothermal processing. The effect of the pH of the precursor chemicals on the ease of formation of a single-phase material was investigated using x-ray diffractio...
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| Published in | Journal of materials research Vol. 13; no. 11; pp. 3135 - 3143 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
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New York, USA
Cambridge University Press
01.11.1998
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| Abstract | This paper is the first report of the synthesis of a sinteractive single-phase microstructure yttrium disilicate precursor powder using hydrothermal processing. The effect of the pH of the precursor chemicals on the ease of formation of a single-phase material was investigated using x-ray diffraction, TEM, and SEM. Under very acidic conditions (pH 1), the formation of yttrium chloride, in addition to the yttrium disilicate precursors, produced a powder that absorbed moisture, did not sinter well, and produced a two-phase interpenetrating microstructure after sintering. At pH 6, yttrium chloride no longer formed, but the interpenetrating network persisted after sintering. Only under basic conditions (pH 10) did single-phase yttrium disilicate form after sintering. This work is noteworthy because the calcination time of 1 h required for the formation of this ceramic at 1050 °C is over an order of magnitude lower than the calcination times of over 100 h required when calcined in the temperature range 900 °C to 1150 °C, as reported previously by other workers. |
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| AbstractList | This paper is the first report of the synthesis of a sinteractive single-phase microstructure yttrium disilicate precursor powder using hydrothermal processing. The effect of the pH of the precursor chemicals on the ease of formation of a single-phase material was investigated using x-ray diffraction, TEM, and SEM. Under very acidic conditions (pH 1), the formation of yttrium chloride, in addition to the yttrium disilicate precursors, produced a powder that absorbed moisture, did not sinter well, and produced a two-phase interpenetrating microstructure after sintering. At pH 6, yttrium chloride no longer formed, but the interpenetrating network persisted after sintering. Only under basic conditions (pH 10) did single-phase yttrium disilicate form after sintering. This work is noteworthy because the calcination time of 1 h required for the formation of this ceramic at 1050 deg C is over an order of magnitude lower than the calcination times of over 100 h required when calcined in the temperature range 900-1150 deg C, as reported previously by other workers. (Authors' goal is to synthesize nanosized single-phase yttrium silicate powder to be used as a matrix for composites. They expect the material to have potential high performance characteristics; melting point for the silicate is 1775 deg C.) This paper is the first report of the synthesis of a sinteractive single-phase microstructure yttrium disilicate precursor powder using hydrothermal processing. The effect of the pH of the precursor chemicals on the ease of formation of a single-phase material was investigated using x-ray diffraction, TEM, and SEM. Under very acidic conditions (pH 1), the formation of yttrium chloride, in addition to the yttrium disilicate precursors, produced a powder that absorbed moisture, did not sinter well, and produced a two-phase interpenetrating microstructure after sintering. At pH 6, yttrium chloride no longer formed, but the interpenetrating network persisted after sintering. Only under basic conditions (pH 10) did single-phase yttrium disilicate form after sintering. This work is noteworthy because the calcination time of 1 h required for the formation of this ceramic at 1050 °C is over an order of magnitude lower than the calcination times of over 100 h required when calcined in the temperature range 900 °C to 1150 °C, as reported previously by other workers. The effect of the pH of the precursor chemicals on the ease of formation of a single-phase material was investigated using XRD, TEM, and SEM. Under very acidic conditions (pH 1), the formation of yttrium chloride, in addition to the yttrium disilicate precursors, produced a powder that absorbed moisture, did not sinter well, and produced a two-phase interpenetrating microstructure after sintering. At pH 6, yttrium chloride no longer formed, but the interpenetrating network persisted after sintering. Only under basic conditions (pH 10) did single-phase yttrium disilicate form after sintering. The calcination time of 1 h required for the formation of this ceramic at 1050 C is over an order of magnitude lower than the calcination times of over 100 h required when calcined in the temperature range 900 C to 1150 C, as reported previously. 21 refs. |
| Author | Ponton, C. B. Chan, K. C. Trusty, P. A. |
| Author_xml | – sequence: 1 givenname: P. A. surname: Trusty fullname: Trusty, P. A. organization: IRC in Materials for High Performance Applications, The University of Birmingham, Edgbaston, Birmingham B15 2TT, United Kingdom – sequence: 2 givenname: K. C. surname: Chan fullname: Chan, K. C. organization: School of Metallurgy & Materials, The University of Birmingham, Edgbaston, Birmingham B15 2TT, United Kingdom – sequence: 3 givenname: C. B. surname: Ponton fullname: Ponton, C. B. organization: School of Metallurgy & Materials and IRC in Materials for High Performance Applications, The University of Birmingham, Edgbaston, Birmingham B15 2TT, United Kingdom |
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| Cites_doi | 10.1016/0022-5088(70)90159-1 10.1557/JMR.1994.0436 10.1111/j.1151-2916.1995.tb08499.x 10.1111/j.1151-2916.1978.tb09251.x 10.1111/j.1151-2916.1975.tb11488.x 10.1080/10426919508935103 10.1111/j.1151-2916.1987.tb05695.x 10.1002/9780470310502.ch28 |
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| References | Levin (S0884291400046604_ref008) 1969 Trusty (S0884291400046604_ref019) 1994 Bondar (S0884291400046604_ref007) 1969; 33 Trusty (S0884291400046604_ref018) 1994 Bondar (S0884291400046604_ref002) 1967; 2 Leskelä (S0884291400046604_ref020) 1982 S0884291400046604_ref009 S0884291400046604_ref017 S0884291400046604_ref006 S0884291400046604_ref005 S0884291400046604_ref003 S0884291400046604_ref013 Ito (S0884291400046604_ref014) 1968; 53 S0884291400046604_ref012 Bataliyeva (S0884291400046604_ref016) 1967; 173 S0884291400046604_ref011 Nekrasov (S0884291400046604_ref015) 1976; 231 Warshaw (S0884291400046604_ref001) 1964; 1 S0884291400046604_ref010 S0884291400046604_ref021 Liddell (S0884291400046604_ref004) 1986; 85 |
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