Sensitive and selective detection of chromium (VI) based on two-dimensional luminescence metal organic framework nanosheets via the mechanism integrating chemical oxidation-reduction and inner filter effect
Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH2-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium...
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| Published in | Journal of hazardous materials Vol. 419; p. 126443 |
|---|---|
| Main Authors | , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
05.10.2021
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| Abstract | Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH2-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium Cr (VI). The nanosheets possess stable fluorescence with the maximum emission wavelength of 436 nm at excitation of 338 nm that can be effectively quenched by hexavalent chromium Cr (VI). The NH2-CuMOFs nanosheets show superior advantage over the linker of NH2-BDC for the excellent selectivity to Cr (Ⅵ) without the interferences of other metal ions. The mechanism investigation suggested that the sensitive detection of Cr (VI) was attributed to the chemical oxidation-reduction (redox) reaction and internal filtration effect (IFE) between Cr (VI) and NH2-CuMOFs nanosheets. Based on this mechanism, the quantitation of Cr (VI) was realized in the linear range of 0.1–20 μM with a detection limit of 18 nM. Moreover, the detection of Cr (VI) in real samples was also conducted with good recovery. This work provides an optical sensing nanoplatform for heavy metal ions based on two-dimensional LMOFs via a novel mechanism integrating chemical redox reaction and IFE, which may promise broad application prospect for two-dimensional luminescence nanosheets.
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•2D luminescence metal organic framework (LMOF) nanosheet was synthesized.•NH2-CuMOFs served as a superior sensitive fluorescent nanoplatform for chromium (Ⅵ).•NH2-CuMOFs show excellent selectivity to Cr (Ⅵ) over NH2-BDC.•A new mechanism integrated with redox reaction and internal filtration effect was proposed.•The quantitative of Cr (Ⅵ) based on NH2-CuMOFs nanosheets was realized. |
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| AbstractList | Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH₂-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH₂-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium Cr (VI). The nanosheets possess stable fluorescence with the maximum emission wavelength of 436 nm at excitation of 338 nm that can be effectively quenched by hexavalent chromium Cr (VI). The NH₂-CuMOFs nanosheets show superior advantage over the linker of NH₂-BDC for the excellent selectivity to Cr (Ⅵ) without the interferences of other metal ions. The mechanism investigation suggested that the sensitive detection of Cr (VI) was attributed to the chemical oxidation-reduction (redox) reaction and internal filtration effect (IFE) between Cr (VI) and NH₂-CuMOFs nanosheets. Based on this mechanism, the quantitation of Cr (VI) was realized in the linear range of 0.1–20 μM with a detection limit of 18 nM. Moreover, the detection of Cr (VI) in real samples was also conducted with good recovery. This work provides an optical sensing nanoplatform for heavy metal ions based on two-dimensional LMOFs via a novel mechanism integrating chemical redox reaction and IFE, which may promise broad application prospect for two-dimensional luminescence nanosheets. Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH2-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium Cr (VI). The nanosheets possess stable fluorescence with the maximum emission wavelength of 436 nm at excitation of 338 nm that can be effectively quenched by hexavalent chromium Cr (VI). The NH2-CuMOFs nanosheets show superior advantage over the linker of NH2-BDC for the excellent selectivity to Cr (Ⅵ) without the interferences of other metal ions. The mechanism investigation suggested that the sensitive detection of Cr (VI) was attributed to the chemical oxidation-reduction (redox) reaction and internal filtration effect (IFE) between Cr (VI) and NH2-CuMOFs nanosheets. Based on this mechanism, the quantitation of Cr (VI) was realized in the linear range of 0.1-20 μM with a detection limit of 18 nM. Moreover, the detection of Cr (VI) in real samples was also conducted with good recovery. This work provides an optical sensing nanoplatform for heavy metal ions based on two-dimensional LMOFs via a novel mechanism integrating chemical redox reaction and IFE, which may promise broad application prospect for two-dimensional luminescence nanosheets.Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH2-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium Cr (VI). The nanosheets possess stable fluorescence with the maximum emission wavelength of 436 nm at excitation of 338 nm that can be effectively quenched by hexavalent chromium Cr (VI). The NH2-CuMOFs nanosheets show superior advantage over the linker of NH2-BDC for the excellent selectivity to Cr (Ⅵ) without the interferences of other metal ions. The mechanism investigation suggested that the sensitive detection of Cr (VI) was attributed to the chemical oxidation-reduction (redox) reaction and internal filtration effect (IFE) between Cr (VI) and NH2-CuMOFs nanosheets. Based on this mechanism, the quantitation of Cr (VI) was realized in the linear range of 0.1-20 μM with a detection limit of 18 nM. Moreover, the detection of Cr (VI) in real samples was also conducted with good recovery. This work provides an optical sensing nanoplatform for heavy metal ions based on two-dimensional LMOFs via a novel mechanism integrating chemical redox reaction and IFE, which may promise broad application prospect for two-dimensional luminescence nanosheets. Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively charged 2-aminoterephthalic acid (NH2-BDC) via a bottom-up strategy, which were first used as the fluorescent probes for the detection of chromium Cr (VI). The nanosheets possess stable fluorescence with the maximum emission wavelength of 436 nm at excitation of 338 nm that can be effectively quenched by hexavalent chromium Cr (VI). The NH2-CuMOFs nanosheets show superior advantage over the linker of NH2-BDC for the excellent selectivity to Cr (Ⅵ) without the interferences of other metal ions. The mechanism investigation suggested that the sensitive detection of Cr (VI) was attributed to the chemical oxidation-reduction (redox) reaction and internal filtration effect (IFE) between Cr (VI) and NH2-CuMOFs nanosheets. Based on this mechanism, the quantitation of Cr (VI) was realized in the linear range of 0.1–20 μM with a detection limit of 18 nM. Moreover, the detection of Cr (VI) in real samples was also conducted with good recovery. This work provides an optical sensing nanoplatform for heavy metal ions based on two-dimensional LMOFs via a novel mechanism integrating chemical redox reaction and IFE, which may promise broad application prospect for two-dimensional luminescence nanosheets. [Display omitted] •2D luminescence metal organic framework (LMOF) nanosheet was synthesized.•NH2-CuMOFs served as a superior sensitive fluorescent nanoplatform for chromium (Ⅵ).•NH2-CuMOFs show excellent selectivity to Cr (Ⅵ) over NH2-BDC.•A new mechanism integrated with redox reaction and internal filtration effect was proposed.•The quantitative of Cr (Ⅵ) based on NH2-CuMOFs nanosheets was realized. |
| ArticleNumber | 126443 |
| Author | Zhang, Youyu Hu, Xiaojun Chen, Chao Ma, Zhangyan Zhu, Xiaohua Liu, Meiling Li, Haitao Qiu, Linjie Li, Peipei Yao, Shouzhuo |
| Author_xml | – sequence: 1 givenname: Linjie surname: Qiu fullname: Qiu, Linjie organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 2 givenname: Zhangyan surname: Ma fullname: Ma, Zhangyan organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 3 givenname: Peipei surname: Li fullname: Li, Peipei organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 4 givenname: Xiaojun surname: Hu fullname: Hu, Xiaojun organization: Hunan Institute of Food Quality Supervision Inspection and Research, PR China – sequence: 5 givenname: Chao surname: Chen fullname: Chen, Chao email: chenchao840103@163.com organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 6 givenname: Xiaohua surname: Zhu fullname: Zhu, Xiaohua organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 7 givenname: Meiling surname: Liu fullname: Liu, Meiling email: liumeilingww@126.com, liuml@hunnu.edu.cn organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 8 givenname: Youyu surname: Zhang fullname: Zhang, Youyu organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 9 givenname: Haitao surname: Li fullname: Li, Haitao organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China – sequence: 10 givenname: Shouzhuo surname: Yao fullname: Yao, Shouzhuo organization: Key Laboratory of Chemical Biology & Traditional Chinese Medicine Research (Ministry of Education, China), College of Chemistry and Chemical Engineering, Hunan Normal University, Changsha 410081, PR China |
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| Copyright | 2021 Elsevier B.V. Copyright © 2021 Elsevier B.V. All rights reserved. |
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| Keywords | Two-dimensional nanomaterial Fluorescence probe Cr (Ⅵ) Internal filtration effect Luminescence metal organic framework (LMOF) Redox reaction |
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| Snippet | Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH2-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively... Two-dimensional luminescence metal organic framework nanosheets (LMOF) named NH₂-CuMOFs were synthesized using Cu (II) nodes coordinated with negatively... |
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| SubjectTerms | chromium coordination polymers Cr (Ⅵ) detection limit filtration fluorescence Fluorescence probe heavy metals Internal filtration effect Luminescence metal organic framework (LMOF) nanosheets Redox reaction redox reactions Two-dimensional nanomaterial wavelengths |
| Title | Sensitive and selective detection of chromium (VI) based on two-dimensional luminescence metal organic framework nanosheets via the mechanism integrating chemical oxidation-reduction and inner filter effect |
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