New ecdysteroids from Serratula tinctoria

Six new ecdysteroids have been isolated from Serratula tinctoria; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone, 3-epi-poststerone, 3-epi-rubrosterone, and 22-oxo-20-hydroxyecdysone. These minor compounds were found together with the known ecdysteroids, 20...

Full description

Saved in:
Bibliographic Details
Published inPlanta medica Vol. 58; no. 4; p. 358
Main Authors Rudel, D. (Centre National de la Recherche Scientifique, Ecole Normale Superieure, Paris (France). Dept. de Biologie, Lab. de Biochimie et Physiologie du Developpement), Bathori, M, Gharbi, J, Girault, J.P, Racz, I, Melis, K, Szendrei, K, Lafont, R
Format Journal Article
LanguageEnglish
Published Germany 01.08.1992
Subjects
Online AccessGet more information

Cover

Loading…
Abstract Six new ecdysteroids have been isolated from Serratula tinctoria; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone, 3-epi-poststerone, 3-epi-rubrosterone, and 22-oxo-20-hydroxyecdysone. These minor compounds were found together with the known ecdysteroids, 20-hydroxyecdysone, its 2-, 3-, and 22-monoacetates, rubrosterone, poststerone, polypodine B (5beta,20-dihydroxyecdysone), pterosterone (25-deoxy-20,24- dihvdroxyecdysone), and makisterone C (24-ethyl-20-- hydroxvecdysone). All these ecdysteroids were isolated by a combination of several chromatographic techniques (liquid chromatography on alumina, DCCC, and HPLC), then identified using standard mass spectrometric and 2D(1)H-NMR techniques.
AbstractList Six new ecdysteroids have been isolated from SERRATULA TINCTORIA; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone, 3-epi-poststerone, 3-epi-rubrosterone, and 22-oxo-20-hydroxyecdysone. These minor compounds were found together with the known ecdysteroids, 20-hydroxyecdysone, its 2-, 3-, and 22-monoacetates, rubrosterone, poststerone, polypodine B (5beta,20-dihydroxyecdysone), pterosterone (25-deoxy-20,24-dihydroxyecdysone), and makisterone C (24-ethyl-20-hydroxyecdysone). All these ecdysteroids were isolated by a combination of several chromatographic techniques (liquid chromatography on alumina, DCCC, and HPLC), then identified using standard mass spectrometric and 2D (1)H-NMR techniques.
Six new ecdysteroids have been isolated from Serratula tinctoria; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone, 3-epi-poststerone, 3-epi-rubrosterone, and 22-oxo-20-hydroxyecdysone. These minor compounds were found together with the known ecdysteroids, 20-hydroxyecdysone, its 2-, 3-, and 22-monoacetates, rubrosterone, poststerone, polypodine B (5beta,20-dihydroxyecdysone), pterosterone (25-deoxy-20,24- dihvdroxyecdysone), and makisterone C (24-ethyl-20-- hydroxvecdysone). All these ecdysteroids were isolated by a combination of several chromatographic techniques (liquid chromatography on alumina, DCCC, and HPLC), then identified using standard mass spectrometric and 2D(1)H-NMR techniques.
Author Rudel, D. (Centre National de la Recherche Scientifique, Ecole Normale Superieure, Paris (France). Dept. de Biologie, Lab. de Biochimie et Physiologie du Developpement)
Girault, J.P
Lafont, R
Gharbi, J
Bathori, M
Szendrei, K
Melis, K
Racz, I
Author_xml – sequence: 1
  fullname: Rudel, D. (Centre National de la Recherche Scientifique, Ecole Normale Superieure, Paris (France). Dept. de Biologie, Lab. de Biochimie et Physiologie du Developpement)
– sequence: 2
  fullname: Bathori, M
– sequence: 3
  fullname: Gharbi, J
– sequence: 4
  fullname: Girault, J.P
– sequence: 5
  fullname: Racz, I
– sequence: 6
  fullname: Melis, K
– sequence: 7
  fullname: Szendrei, K
– sequence: 8
  fullname: Lafont, R
BackLink https://www.ncbi.nlm.nih.gov/pubmed/17226485$$D View this record in MEDLINE/PubMed
BookMark eNo1zj1PwzAUhWELFdG0MLIwoKwMhnv9FXuEUj6kCgZgjpz4BgU1SWWnqvrvqVSYzvLo6J2xST_0xNglwi2C1neJCwDDnUFl9QnLUEnHQQicsAxACg5OySmbpfQDgMoBnLEpFkKYg8_YzRvtcqrDPo0UhzakvIlDl39QjH7crn0-tn09DrH15-y08etEF387Z19Py8_FC1-9P78u7le8loUeuTbYCFMYT9IqUzTaBLIWvaqC0ap2CM5KlGidIxlEFdAD-doiUAGCUMzZ9fF3s606CuUmtp2P-_K_-QCujqDxQ-m_Y5vKx6WTD6gQxC_voUsk
CitedBy_id crossref_primary_10_1007_s10600_018_2300_8
crossref_primary_10_1016_S0031_9422_98_00447_6
crossref_primary_10_1135_cccc20020124
crossref_primary_10_1248_cpb_58_690
crossref_primary_10_1016_S0039_128X_99_00096_3
crossref_primary_10_1016_S0031_9422_03_00021_9
crossref_primary_10_1016_0021_9673_94_85206_5
crossref_primary_10_1002_arch_10060
crossref_primary_10_1016_0021_9673_94_85205_7
crossref_primary_10_3390_separations9120448
crossref_primary_10_1556_JPC_17_2004_5_3
crossref_primary_10_1021_np970124y
crossref_primary_10_1081_JLC_100101452
crossref_primary_10_1016_j_phytol_2020_04_017
crossref_primary_10_1016_S0305_1978_97_00003_3
crossref_primary_10_1016_j_steroids_2011_07_007
crossref_primary_10_1002_mrc_2581
crossref_primary_10_1002__SICI_1520_6327_1997_35_1_2_227__AID_ARCH21_3_0_CO_2_C
crossref_primary_10_1007_BF01928896
crossref_primary_10_1016_S0731_7085_97_00051_4
crossref_primary_10_1021_acs_jafc_5b02570
crossref_primary_10_1016_S0021_9673_01_00992_X
crossref_primary_10_1007_BF02128751
crossref_primary_10_1016_0040_4020_96_00589_3
crossref_primary_10_14258_jcprm_2018022017
crossref_primary_10_1016_0965_1748_94_90078_7
crossref_primary_10_1038_s41598_019_53090_9
crossref_primary_10_1086_499991
crossref_primary_10_1016_0965_1748_93_90098_D
crossref_primary_10_1111_1365_2745_12824
crossref_primary_10_1021_np070037y
crossref_primary_10_1134_S1068162019070094
crossref_primary_10_1016_j_jchromb_2017_03_043
crossref_primary_10_14258_jcprm_2017042016
crossref_primary_10_1016_0965_1748_94_90122_8
crossref_primary_10_1016_S0305_1978_97_00130_0
crossref_primary_10_1016_0040_4020_95_00635_L
crossref_primary_10_1002_cbdv_200590025
crossref_primary_10_1016_S0040_4020_97_00245_7
crossref_primary_10_1016_S0965_1748_01_00106_0
ContentType Journal Article
DBID FBQ
NPM
DOI 10.1055/s-2006-961485
DatabaseName AGRIS
PubMed
DatabaseTitle PubMed
DatabaseTitleList PubMed

Database_xml – sequence: 1
  dbid: NPM
  name: PubMed
  url: https://proxy.k.utb.cz/login?url=http://www.ncbi.nlm.nih.gov/entrez/query.fcgi?db=PubMed
  sourceTypes: Index Database
– sequence: 2
  dbid: FBQ
  name: AGRIS
  url: http://www.fao.org/agris/Centre.asp?Menu_1ID=DB&Menu_2ID=DB1&Language=EN&Content=http://www.fao.org/agris/search?Language=EN
  sourceTypes: Publisher
DeliveryMethod no_fulltext_linktorsrc
Discipline Pharmacy, Therapeutics, & Pharmacology
Botany
EISSN 1439-0221
ExternalDocumentID 17226485
DE93B1410
Genre Journal Article
GroupedDBID ---
-~X
.GJ
0R~
123
1UC
4.4
53G
5~~
AAMFZ
AAWTL
AAYOK
ABCQX
ABJNI
ABOCM
ABPTK
ABTAH
ACGFS
AEDKO
AEMDM
AENEX
AEUVB
AFFNX
AFZED
AHRAW
ALMA_UNASSIGNED_HOLDINGS
BXHMU
CS3
DU5
EBS
EJD
EWXKU
F5P
FBQ
IY8
L7B
N9A
O9-
QTC
RIG
RN7
ROL
RTC
ZGI
ZY4
~KM
AECCQ
AEIGU
AEILP
AIZAD
H13
NPM
ID FETCH-LOGICAL-c375t-561f2676ae38467f56de881a4bd654c910983131899e3d2bd1a0eac810e702e12
ISSN 0032-0943
IngestDate Sat Sep 28 07:57:29 EDT 2024
Wed Dec 27 19:20:34 EST 2023
IsPeerReviewed true
IsScholarly true
Issue 4
Language English
LinkModel OpenURL
MergedId FETCHMERGED-LOGICAL-c375t-561f2676ae38467f56de881a4bd654c910983131899e3d2bd1a0eac810e702e12
Notes F60
93B1410
PMID 17226485
ParticipantIDs pubmed_primary_17226485
fao_agris_DE93B1410
PublicationCentury 1900
PublicationDate 1992-08-01
PublicationDateYYYYMMDD 1992-08-01
PublicationDate_xml – month: 08
  year: 1992
  text: 1992-08-01
  day: 01
PublicationDecade 1990
PublicationPlace Germany
PublicationPlace_xml – name: Germany
PublicationTitle Planta medica
PublicationTitleAlternate Planta Med
PublicationYear 1992
SSID ssj0014900
Score 1.588512
Snippet Six new ecdysteroids have been isolated from Serratula tinctoria; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone,...
Six new ecdysteroids have been isolated from SERRATULA TINCTORIA; these are: the 2,22- and 3,22-diacetates of 20-hydroxyecdysone, 5beta-hydroxyrubrosterone,...
SourceID pubmed
fao
SourceType Index Database
Publisher
StartPage 358
SubjectTerms COMPOSICION QUIMICA
Compositae
COMPOSITION CHIMIQUE
Ecdysteroids
ESTRUCTURA QUIMICA
FITOALEXINA
INSECTICIDAS
INSECTICIDE
PHYTOALEXINE
PLANTAS MEDICINALES
PLANTE MEDICINALE
Serratula
SERRATULA TINCTORIA
STRUCTURE CHIMIQUE
Title New ecdysteroids from Serratula tinctoria
URI https://www.ncbi.nlm.nih.gov/pubmed/17226485
Volume 58
hasFullText
inHoldings 1
isFullTextHit
isPrint
link http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwnV3PT9swFLYo7MBlgo4BGyAfENIE2fLDduwjhQKaNMSmInGrHNuBSNCgNhy6v57n2E0DbBJwiSq7ipL3vbx88XvvM0K7TEVGyQyiX0TTgHBDA27yJABXyJgSJmR1k9ivc3Z2SX5e0avZRuO-u6TKvqu__-wreQ-qMAa42i7ZNyDbnBQG4DfgC0dAGI6vwtgWJ_aVtmLM47LQE9csAo-_FUq-lftVMbJr8oVsU1C7TVElXVK9icl_HrRL1zcFwD2ghqVrQ5-L6N_IcVY8SSadFmP5cOsSGr5XTPumuripYGviYgJjwgkmzeIi5S38SSvIJW7mRfANqdWpmAT1KoWwCqO0_T-w3f1djQSQJltY94rZZ1rYs6kO6qTcRrVzuzbjc0ZE-IYjfy9eURWu6seTa7I6sf48QChyWT77oqiZxWAFffSfBPjQ4buKFsyoiz70SqDt0y7au3Di4tMDPJj3yk0O8B6-mMuOTz-hb-ANuO0N2HoDbrwBN96whi5P-oOjs8BvhBGoJKVVABw3j1nKpEksXcwp04bzSJJMM0oUMD7BkwiisxAm0XGmIxnCC5VHoUnD2ETxZ7Q4KkdmA2ESkTxOGfBQpUnOwE6piXPFCE0FD4nZRF2wyFBewytmeNwXSc8WAm-idWeh4b3TQBnOLPjlvzNf0fLc1bbQUg4PndkGBldlO6hz0vu9U8P3CJlNPWA
link.rule.ids 783
linkProvider National Library of Medicine
openUrl ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=New+Ecdysteroids+from+Serratula+tinctoria&rft.jtitle=Planta+medica&rft.au=Rudel%2C+D&rft.au=Bathori%2C+M&rft.au=Gharbi%2C+J&rft.au=Girault%2C+J+P&rft.date=1992-08-01&rft.issn=0032-0943&rft.volume=58&rft.issue=4&rft.spage=358&rft_id=info:doi/10.1055%2Fs-2006-961485&rft_id=info%3Apmid%2F17226485&rft_id=info%3Apmid%2F17226485&rft.externalDocID=17226485
thumbnail_l http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=0032-0943&client=summon
thumbnail_m http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=0032-0943&client=summon
thumbnail_s http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=0032-0943&client=summon