Microwave hydrothermal synthesis of high performance tin–graphene nanocomposites for lithium ion batteries
Tin–graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio between tin and graphene nanosheets has critical influences on their morphologies and electrochemical performances. Field emission scanning e...
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| Published in | Journal of power sources Vol. 216; pp. 22 - 27 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
Amsterdam
Elsevier B.V
15.10.2012
Elsevier |
| Subjects | |
| Online Access | Get full text |
| ISSN | 0378-7753 1873-2755 |
| DOI | 10.1016/j.jpowsour.2012.05.051 |
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| Abstract | Tin–graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio between tin and graphene nanosheets has critical influences on their morphologies and electrochemical performances. Field emission scanning electron microscope (FESEM) and transmission electron microscope (TEM) analysis confirm the homogeneous distribution of tin nanoparticles on the surface of graphene nanosheets. When applied as an anode material in lithium ion batteries, tin–graphene nanocomposite exhibits a high lithium storage capacity of 1407 mAh g−1. The as-prepared tin–graphene nanocomposite also demonstrates an excellent high rate capacity and a stable cycle performance. The superior electrochemical performance could be attributed to the synergistic effect of the three-dimensional nanoarchitecture, in which tin nanoparticles are sandwiched between highly conductive and flexible graphene nanosheets.
► Sn–GNS were prepared by a microwave hydrothermal synthesis and a one-step H2 reduction. ► Sn nanoparticles are homogenously sandwiched between highly conductive and flexible GNS. ► Altering the ratio between tin and graphene had critical influences on their morphologies. ► Sn–GNS exhibited a high lithium storage capacity of 1407 mAh g−1. |
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| AbstractList | Tin-graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio between tin and graphene nanosheets has critical influences on their morphologies and electrochemical performances. Field emission scanning electron microscope (FESEM) and transmission electron microscope (TEM) analysis confirm the homogeneous distribution of tin nanoparticles on the surface of graphene nanosheets. When applied as an anode material in lithium ion batteries, tin-graphene nanocomposite exhibits a high lithium storage capacity of 1407 mAh ga1. The as-prepared tin-graphene nanocomposite also demonstrates an excellent high rate capacity and a stable cycle performance. The superior electrochemical performance could be attributed to the synergistic effect of the three-dimensional nanoarchitecture, in which tin nanoparticles are sandwiched between highly conductive and flexible graphene nanosheets. Tin–graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio between tin and graphene nanosheets has critical influences on their morphologies and electrochemical performances. Field emission scanning electron microscope (FESEM) and transmission electron microscope (TEM) analysis confirm the homogeneous distribution of tin nanoparticles on the surface of graphene nanosheets. When applied as an anode material in lithium ion batteries, tin–graphene nanocomposite exhibits a high lithium storage capacity of 1407 mAh g−1. The as-prepared tin–graphene nanocomposite also demonstrates an excellent high rate capacity and a stable cycle performance. The superior electrochemical performance could be attributed to the synergistic effect of the three-dimensional nanoarchitecture, in which tin nanoparticles are sandwiched between highly conductive and flexible graphene nanosheets. ► Sn–GNS were prepared by a microwave hydrothermal synthesis and a one-step H2 reduction. ► Sn nanoparticles are homogenously sandwiched between highly conductive and flexible GNS. ► Altering the ratio between tin and graphene had critical influences on their morphologies. ► Sn–GNS exhibited a high lithium storage capacity of 1407 mAh g−1. |
| Author | Chen, Shuangqiang Ahn, Hyojun Wang, Guoxiu Wang, Yong |
| Author_xml | – sequence: 1 givenname: Shuangqiang surname: Chen fullname: Chen, Shuangqiang organization: School of Environmental and Chemical Engineering, Shanghai University, Shangda Road 99, Shanghai 200444, PR China – sequence: 2 givenname: Yong surname: Wang fullname: Wang, Yong email: yongwang@shu.edu.cn organization: School of Environmental and Chemical Engineering, Shanghai University, Shangda Road 99, Shanghai 200444, PR China – sequence: 3 givenname: Hyojun surname: Ahn fullname: Ahn, Hyojun organization: School of Materials Science and Engineering, Gyeongsang National University, 900 Gazwa-dong, Jinju, Gyeongnam 660-701, Republic of Korea – sequence: 4 givenname: Guoxiu surname: Wang fullname: Wang, Guoxiu email: Guoxiu.wang@uts.edu.au organization: Centre for Clean Energy Technology, School of Chemistry and Forensic Science, University of Technology Sydney, Broadway, Sydney, NSW 2007, Australia |
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| Keywords | Lithium ion batteries Graphene nanosheets Microwave hydrothermal synthesis Tin nanoparticles Hydrogen reduction Performance evaluation Nanosheet Anode Hydrogen Nanoparticle Alkaline storage battery Lithium Field emission Electrode material Synergism Electrochemical characteristic Storage capacity Nanocomposite High performance Scanning electron microscopy Transmission microscope Sandwich structure Secondary cell Electron microscopy Field emission microscopy Lithium battery Three dimensional model Transmission electron microscopy Hydrothermal synthesis Graphene Morphology Nanostructured materials |
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| Snippet | Tin–graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio... Tin-graphene nanocomposites are prepared by a combination of microwave hydrothermal synthesis and a one-step hydrogen gas reduction. Altering the weight ratio... |
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| SubjectTerms | Applied sciences Direct energy conversion and energy accumulation Electrical engineering. Electrical power engineering Electrical power engineering Electrochemical conversion: primary and secondary batteries, fuel cells Exact sciences and technology Graphene Graphene nanosheets Hydrogen reduction Lithium ion batteries Materials Microwave hydrothermal synthesis Nanocomposites Nanomaterials Nanostructure Scanning electron microscopy Synthesis Tin Tin nanoparticles |
| Title | Microwave hydrothermal synthesis of high performance tin–graphene nanocomposites for lithium ion batteries |
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