Syntheses and fluorescent properties of complexes of Eu(III) with HTTA, TPPO and benzoic acid
A series of Eu(III) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic acid(PTA) and p-methoxybenzoic acid(POA) were synthesized and were characterized with elemental analysis, IR spectroscopy, scanning electronic mic...
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| Published in | Journal of rare earths Vol. 27; no. 3; pp. 368 - 371 |
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| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Elsevier B.V
01.06.2009
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| Subjects | |
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| Abstract | A series of Eu(III) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives,
p-toluic acid(PTA) and
p-methoxybenzoic acid(POA) were synthesized and were characterized with elemental analysis, IR spectroscopy, scanning electronic microscopy and fluorescent spectra. The complexes were revealed to be Eu(BA)(TTA)
2TPPO
2, Eu(PTA)(TTA)
2TPPO
2 and Eu(POA)(TTA)
2TPPO
2. The excitation and absorption spectra of the complex Eu(POA)(TTA)
2TPPO
2 in MeOH solution were investigated in detail. The experimental result showed that relatively cheap materials with sharp red luminescence could be prepared, when benzoic acid or its two derivatives were added in Eu(III) complexes of α-thenoyltrifluoroacetone with trioctylphosphine oxide. The relative fluorescence intensity of the Eu(III) complexes decreased in the following order: Eu(POA)(TTA)
2TPPO
2> Eu(PTA)(TTA)
2TPPO
2>Eu(BA)(TTA)
2TPPO
2. |
|---|---|
| AbstractList | A series of Eu(III) complexes of a-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic acid(PTA) and p-methoxybenzoic acid(POA) were synthesized and were characterized with elemental analysis, IR spectroscopy, scanning electronic microscopy and fluorescent spectra. The complexes were revealed to be Eu(BA)(TTA)(2)TPPO(2), Eu(PTA)(TTA)(2)TPPO(2) and Eu(POA)(TTA)(2)TPPO(2). The excitation and absorption spectra of the complex Eu(POA)(TTA)(2)TPPO(2) in MeOH solution were investigated in detail. The experimental result showed that relatively cheap materials with sharp red luminescence could be prepared, when benzoic acid or its two derivatives were added in Eu(III) complexes of a-thenoyltrifluoroacetone with trioctylphosphine oxide. The relative fluorescence intensity of the Eu(III) complexes decreased in the following order: Eu(POA)(TTA)(2)TPPO(2) > Eu(PTA)(TTA)(2)TPPO(2) > Eu(BA)(TTA)(2)TPPO(2). O6; A series of Eu(Ⅲ) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic acid(PTA) and p-methoxybenzoic acid(POA) were synthesized and were characterized with elemental analysis, IR spectroscopy, scanning electronic microscopy and fluorescent spectra. The complexes were revealed to be Eu(BA)(TTA)2TPPO2, Eu(PTA)(TTA)2TPPO2 and Eu(POA)(TTA)2TPPO2. The excitation and absorption spectra of the complex Eu(POA)(TTA)2TPPO2 in MeOH solution were investigated in detail. The experimental result showed that relatively cheap materials with sharp red luminescence could be pre-pared, when benzoic acid or its two derivatives were added in Eu(Ⅲ) complexes of α-thenoyltdfluoroacetone with trioctylphosphine oxide. The relative fluorescence intensity of the Eu(Ⅲ) complexes decreased in the following order: Eu(POA)(TTA)2TPPO2> Eu(PTA)(TTA)2TPPO2>Eu(BA)(TTA)2TPPO2. A series of Eu(III) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic acid(PTA) and p-methoxybenzoic acid(POA) were synthesized and were characterized with elemental analysis, IR spectroscopy, scanning electronic microscopy and fluorescent spectra. The complexes were revealed to be Eu(BA)(TTA) 2TPPO 2, Eu(PTA)(TTA) 2TPPO 2 and Eu(POA)(TTA) 2TPPO 2. The excitation and absorption spectra of the complex Eu(POA)(TTA) 2TPPO 2 in MeOH solution were investigated in detail. The experimental result showed that relatively cheap materials with sharp red luminescence could be prepared, when benzoic acid or its two derivatives were added in Eu(III) complexes of α-thenoyltrifluoroacetone with trioctylphosphine oxide. The relative fluorescence intensity of the Eu(III) complexes decreased in the following order: Eu(POA)(TTA) 2TPPO 2> Eu(PTA)(TTA) 2TPPO 2>Eu(BA)(TTA) 2TPPO 2. |
| Author | ZHAN, Xuehui ZHOU, Suian ZHAO, Xuehui XIAO, Zhongliang ZHAN, Hanhui LI, Fei |
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| Cites_doi | 10.1016/S1002-0721(07)60565-1 10.1016/S0040-6090(96)09273-5 10.1007/s11771-003-0036-4 10.1016/j.jallcom.2006.07.094 10.1007/s00894-005-0280-7 10.1016/j.optmat.2006.07.014 10.1016/S0010-8545(00)80455-5 10.1016/S1002-0721(07)60563-8 10.1016/j.jphotochem.2006.12.020 10.1007/s11771-007-0013-4 10.1016/S1002-0721(07)60447-5 |
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| Keywords | fluorescent properties α-thenoyltrifluoroacetone benzoic acid europium rare earths |
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| Snippet | A series of Eu(III) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives,
p-toluic... A series of Eu(III) complexes of a-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic... O6; A series of Eu(Ⅲ) complexes of α-thenoyltrifluoroacetone(HTTA) with trioctylphosphine oxide(TPPO) and benzoic acid(BA) or its two derivatives, p-toluic... |
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| Title | Syntheses and fluorescent properties of complexes of Eu(III) with HTTA, TPPO and benzoic acid |
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