The effect of aromatic and aliphatic amines on copper electrowinning from acidic sulphate electrolyte
Copper electrodeposition in the presence of various types of aromatic and aliphatic amines was studied. The effects of operating variables including organic additives concentrations and temperature on the limiting current were investigated by the potentio-dynamic polarization technique. The effects...
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| Published in | Hydrometallurgy Vol. 104; no. 2; pp. 169 - 177 |
|---|---|
| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
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Amsterdam
Elsevier B.V
01.09.2010
Elsevier |
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| Abstract | Copper electrodeposition in the presence of various types of aromatic and aliphatic amines was studied. The effects of operating variables including organic additives concentrations and temperature on the limiting current were investigated by the potentio-dynamic polarization technique. The effects of amines on the surface tensions of the solutions were measured; the results showed that amines reduce solution surface tension. The adsorption of all inhibitors on copper cathode was found to obey Temkin, Flory–Huggin and kinetic adsorption isotherm. The calculated free energy of adsorption (ΔG
ads.) of inhibitor on copper surface indicated that the adsorption reactions were spontaneous (ΔG
ads.
<
0). The thermodynamic activation parameters (E
a, ΔH*, ΔS* and ΔG*) were estimated and discussed. It was found that activation energy values for copper electrodeposition in the inhibited solutions were higher than that for the uninhibited solution. The high inhibitor efficiency was discussed in terms of the strong adsorption of inhibitor molecules on the copper surface. |
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| AbstractList | Copper electrodeposition in the presence of various types of aromatic and aliphatic amines was studied. The effects of operating variables including organic additives concentrations and temperature on the limiting current were investigated by the potentio-dynamic polarization technique. The effects of amines on the surface tensions of the solutions were measured; the results showed that amines reduce solution surface tension. The adsorption of all inhibitors on copper cathode was found to obey Temkin, Flory–Huggin and kinetic adsorption isotherm. The calculated free energy of adsorption (ΔG
ads.) of inhibitor on copper surface indicated that the adsorption reactions were spontaneous (ΔG
ads.
<
0). The thermodynamic activation parameters (E
a, ΔH*, ΔS* and ΔG*) were estimated and discussed. It was found that activation energy values for copper electrodeposition in the inhibited solutions were higher than that for the uninhibited solution. The high inhibitor efficiency was discussed in terms of the strong adsorption of inhibitor molecules on the copper surface. Copper electrodeposition in the presence of various types of aromatic and aliphatic amines was studied. The effects of operating variables including organic additives concentrations and temperature on the limiting current were investigated by the potentio-dynamic polarization technique. The effects of amines on the surface tensions of the solutions were measured; the results showed that amines reduce solution surface tension. The adsorption of all inhibitors on copper cathode was found to obey Temkin, Flory-Huggin and kinetic adsorption isotherm. The calculated free energy of adsorption ( Delta Gads.) of inhibitor on copper surface indicated that the adsorption reactions were spontaneous ( Delta Gads. <0). The thermodynamic activation parameters (Ea, Delta H*, Delta S* and Delta G*) were estimated and discussed. It was found that activation energy values for copper electrodeposition in the inhibited solutions were higher than that for the uninhibited solution. The high inhibitor efficiency was discussed in terms of the strong adsorption of inhibitor molecules on the copper surface. |
| Author | Ahmed, A.M. Abdel-Rahman, H.H. Harfoush, A.A. Moustafa, A.H.E. |
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| CitedBy_id | crossref_primary_10_1007_s11771_013_1712_7 crossref_primary_10_1080_03719553_2015_1109183 crossref_primary_10_1021_ie400160x crossref_primary_10_1080_01496395_2015_1081943 crossref_primary_10_1016_S1452_3981_23_15761_0 crossref_primary_10_5796_electrochemistry_80_226 crossref_primary_10_1016_S1452_3981_23_13413_4 |
| Cites_doi | 10.1016/j.apsusc.2007.03.045 10.1016/S0304-386X(03)00030-6 10.1002/ceat.200700158 10.1016/j.jhazmat.2005.06.030 10.1016/j.colsurfa.2007.06.035 10.1155/2009/107807 10.1149/1.2404128 10.1016/j.corsci.2005.09.017 10.1016/j.matchemphys.2003.12.027 10.1016/j.jcis.2004.01.031 10.1016/j.electacta.2006.06.025 10.1016/j.jhazmat.2007.05.055 10.1590/S0103-50532006000400011 10.1002/cjce.5450670612 10.1007/BF00618990 10.1016/j.biortech.2008.11.016 10.1016/j.jelechem.2008.04.006 10.1016/S0169-4332(02)00553-6 10.1016/0013-4686(72)80067-7 10.1016/j.corsci.2008.04.015 10.1016/j.matchemphys.2008.09.065 10.1016/0300-9467(89)80003-6 10.1016/j.jhazmat.2006.05.051 10.1016/S0010-938X(03)00174-4 10.1016/j.electacta.2008.09.052 10.1016/j.electacta.2006.04.047 10.1016/S0013-4686(02)00833-2 |
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| Keywords | Mass transfer in electrolysis Copper electrodeposition Amines Adsorption Surface morphology Surface treatment Mass transfer Metal coating Amine Electrolytic separation Electrolyte Morphology Electrodeposition Acid medium Hydrometallurgy |
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| SubjectTerms | ACIDS ACTIVATION ENERGY ADSORPTION Aliphatic amines AMINES Applied sciences Copper Copper electrodeposition CORROSION INHIBITORS ELECTRODEPOSITION ELECTROLYTES ELECTROWINNING Exact sciences and technology Inhibition Mass transfer in electrolysis Metallic coatings Metals. Metallurgy Production of metals Production techniques Surface chemistry Surface morphology SURFACE TENSION Surface treatment |
| Title | The effect of aromatic and aliphatic amines on copper electrowinning from acidic sulphate electrolyte |
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