Super adsorption capability of rhombic dodecahedral Ca-Al layered double oxides for Congo red removal

In this work, a novel rhombic dodecahedral structure of Ca-Al-layered double hydroxides (Ca-Al-LDHs) was synthesized by a two-phase solvothermal method. Subsequently, Ca-Al layered double oxides (Ca-Al-LDOs) were obtained by calcinating Ca-Al-LDHs at 600 °C which maintained the rhombic dodecahedral...

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Published inJournal of alloys and compounds Vol. 768; pp. 572 - 581
Main Authors Zhang, Heng, Chen, Hang, Azat, Seytkhan, Mansurov, Zulkhair A., Liu, Xueming, Wang, Jide, Su, Xintai, Wu, Ronglan
Format Journal Article
LanguageEnglish
Published Lausanne Elsevier B.V 05.11.2018
Elsevier BV
Subjects
Adsorption
Alloys
Ca-Al layered double oxides
Chemical bonds
Congo red
Energy dispersive X ray spectroscopy
Hydrogen bonding
Hydroxides
Infrared spectra
Ion exchange
Morphology
Quantum theory
Rhombic dodecahedral structure
Scanning electron microscopy
Solid phases
Thermodynamics
Transmission electron microscopy
Water treatment
X ray spectra
X-ray diffraction
Zinc oxides
Ca-Al layered double oxides
Congo red
Adsorption
Rhombic dodecahedral structure
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Abstract In this work, a novel rhombic dodecahedral structure of Ca-Al-layered double hydroxides (Ca-Al-LDHs) was synthesized by a two-phase solvothermal method. Subsequently, Ca-Al layered double oxides (Ca-Al-LDOs) were obtained by calcinating Ca-Al-LDHs at 600 °C which maintained the rhombic dodecahedral structures well. The morphologies of as-obtained samples were characterized by both transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The phase structure and elemental composition were analyzed by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS), respectively. Fourier transformed infrared (FT-IR) spectra were performed to confirm the existence of LDH structures. The Ca-Al-LDOs exhibited high adsorption rates and superb adsorption capacities for removal of Congo red (CR) from aqueous solution. The maximum adsorption capacities of Ca-Al-LDOs towards CR reached to 1536.1 mg g−1, which is extremely higher than most of hydrotalcite-like materials. The adsorption process of Ca-Al-LDHs and Ca-Al-LDOs were described by the Langmuir isotherm model and pseudo-second-order model well. The adsorption mechanisms mainly dominated by electrostatic adsorption, ion exchange process, hydrogen bonding interactions and surface complexation. This general strategy afforded a wide possibility to prepare a novel and advanced LDOs adsorption material for water treatment. [Display omitted] •Ca-Al-LDHs were synthesized via a two-phase solvothermal method.•Ca-Al-LDHs and Ca-Al-LDOs with rhombic dodecahedral morphology.•The Ca-Al-LDOs has the maximum adsorption capacity of 1536.1 mg g−1.
AbstractList In this work, a novel rhombic dodecahedral structure of Ca-Al-layered double hydroxides (Ca-Al-LDHs) was synthesized by a two-phase solvothermal method. Subsequently, Ca-Al layered double oxides (Ca-Al-LDOs) were obtained by calcinating Ca-Al-LDHs at 600 °C which maintained the rhombic dodecahedral structures well. The morphologies of as-obtained samples were characterized by both transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The phase structure and elemental composition were analyzed by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS), respectively. Fourier transformed infrared (FT-IR) spectra were performed to confirm the existence of LDH structures. The Ca-Al-LDOs exhibited high adsorption rates and superb adsorption capacities for removal of Congo red (CR) from aqueous solution. The maximum adsorption capacities of Ca-Al-LDOs towards CR reached to 1536.1 mg g−1, which is extremely higher than most of hydrotalcite-like materials. The adsorption process of Ca-Al-LDHs and Ca-Al-LDOs were described by the Langmuir isotherm model and pseudo-second-order model well. The adsorption mechanisms mainly dominated by electrostatic adsorption, ion exchange process, hydrogen bonding interactions and surface complexation. This general strategy afforded a wide possibility to prepare a novel and advanced LDOs adsorption material for water treatment.
In this work, a novel rhombic dodecahedral structure of Ca-Al-layered double hydroxides (Ca-Al-LDHs) was synthesized by a two-phase solvothermal method. Subsequently, Ca-Al layered double oxides (Ca-Al-LDOs) were obtained by calcinating Ca-Al-LDHs at 600 °C which maintained the rhombic dodecahedral structures well. The morphologies of as-obtained samples were characterized by both transmission electron microscopy (TEM) and scanning electron microscopy (SEM). The phase structure and elemental composition were analyzed by X-ray diffraction (XRD) and energy dispersive X-ray spectroscopy (EDS), respectively. Fourier transformed infrared (FT-IR) spectra were performed to confirm the existence of LDH structures. The Ca-Al-LDOs exhibited high adsorption rates and superb adsorption capacities for removal of Congo red (CR) from aqueous solution. The maximum adsorption capacities of Ca-Al-LDOs towards CR reached to 1536.1 mg g−1, which is extremely higher than most of hydrotalcite-like materials. The adsorption process of Ca-Al-LDHs and Ca-Al-LDOs were described by the Langmuir isotherm model and pseudo-second-order model well. The adsorption mechanisms mainly dominated by electrostatic adsorption, ion exchange process, hydrogen bonding interactions and surface complexation. This general strategy afforded a wide possibility to prepare a novel and advanced LDOs adsorption material for water treatment. [Display omitted] •Ca-Al-LDHs were synthesized via a two-phase solvothermal method.•Ca-Al-LDHs and Ca-Al-LDOs with rhombic dodecahedral morphology.•The Ca-Al-LDOs has the maximum adsorption capacity of 1536.1 mg g−1.
Author Chen, Hang
Liu, Xueming
Azat, Seytkhan
Su, Xintai
Wang, Jide
Wu, Ronglan
Zhang, Heng
Mansurov, Zulkhair A.
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  givenname: Zulkhair A.
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  organization: Institute of Combustion Problems, Almaty 050012, Kazakhstan
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  givenname: Xueming
  surname: Liu
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  fullname: Wang, Jide
  organization: Ministry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, China
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  givenname: Xintai
  orcidid: 0000-0001-6615-5273
  surname: Su
  fullname: Su, Xintai
  email: suxintai827@163.com
  organization: Ministry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, China
– sequence: 8
  givenname: Ronglan
  surname: Wu
  fullname: Wu, Ronglan
  email: wuronglan@163.com
  organization: Ministry Key Laboratory of Oil and Gas Fine Chemicals, College of Chemistry and Chemical Engineering, Xinjiang University, Urumqi 830046, China
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Keywords Ca-Al layered double oxides
Congo red
Adsorption
Rhombic dodecahedral structure
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Snippet In this work, a novel rhombic dodecahedral structure of Ca-Al-layered double hydroxides (Ca-Al-LDHs) was synthesized by a two-phase solvothermal method....
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SubjectTerms Adsorption
Alloys
Ca-Al layered double oxides
Chemical bonds
Congo red
Energy dispersive X ray spectroscopy
Hydrogen bonding
Hydroxides
Infrared spectra
Ion exchange
Morphology
Quantum theory
Rhombic dodecahedral structure
Scanning electron microscopy
Solid phases
Thermodynamics
Transmission electron microscopy
Water treatment
X ray spectra
X-ray diffraction
Zinc oxides
Title Super adsorption capability of rhombic dodecahedral Ca-Al layered double oxides for Congo red removal
URI https://dx.doi.org/10.1016/j.jallcom.2018.07.241
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